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1. 发明专利

JP2003192596A NEW ANTICOCCIDIAL AGENT INCLUDING ORGANIC BORON COMPOUND 审中-公开
公开(公告)号：JP2003192596A
公开(公告)日：2003-07-09
申请号：JP2001397612
申请日：2001-12-27
申请人： SHIONOGI & CO , NITTO KASEI CO LTD
发明人： HAYASE YOSHIO , KAWAGUCHI YOSUKE , TANIGUCHI HISASHI , TABUCHI HITOSHI
IPC分类号： A61K31/69 , A61P33/02
摘要： PROBLEM TO BE SOLVED: To provide a new anticoccidial agent that includes an organic boron compound. SOLUTION: The medicinal composition for mammalians except humans, the antiprotozoal agent and the anticoccidial agent of this invention include a compound represented by general formula (I), their salts or their solvates. COPYRIGHT: (C)2003,JPO

2. 发明专利

JP2002255973A METHOD FOR MANUFACTURING TRIPHENYLBORANEAMINE COMPLEX COMPOUND 失效
公开(公告)号：JP2002255973A
公开(公告)日：2002-09-11
申请号：JP2001048856
申请日：2001-02-23
申请人： NITTO KASEI CO LTD
发明人： TANIGUCHI HISASHI , TAKESAWA TOSHIYUKI , TABUCHI HITOSHI
IPC分类号： C07C209/00 , C07C211/65 , C07F5/02
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a triphenylboraneamine complex compound by an economically effective process from stable easily handleable starting materials. SOLUTION: The method for manufacturing a triphenylboraneamine complex compound expressed by general formula (1) (wherein, R is a 1-18C linear or branched alkylene; and Y is H, a halogen, or a 1-18C linear or branched alkoxy) comprises reacting a tetraphenylborate magnesium halide expressed by general formula (2) (wherein, X is a halogen) with a primary amine salt expressed by general formula (3) (wherein, R and Y are same as defined above; and Z is a halogen).

3. 发明专利

JPH0812728A RESIN FOR ANTIFOULING COATING MATERIAL 失效
公开(公告)号：JPH0812728A
公开(公告)日：1996-01-16
申请号：JP12431495
申请日：1995-04-24
申请人： NITTO KASEI CO LTD
发明人： MORI KIYOMI , TAKESAWA TOSHIYUKI , INADA AKIHIRO , TANIGUCHI HISASHI
IPC分类号： C08F220/26 , C08F20/26 , C09D5/16 , C09D133/04 , C09D133/14
摘要： PURPOSE:To obtain a resin which gives an antifouling coating material which forms an antifouling coating film excellent in physical properties, adheres well to a substrate, facilitates the pretreatment of a substrate, etc., and manifests long-lasting antifouling effects. CONSTITUTION:This resin comprising a copolymer formed from 30-99.9wt.% etherified (meth)acrylate unit of formula I (where R is H or methyl; R is a 2-10C alkylene, phenylene, or benzylene; or benzylene; and X is a 1-12C alkoxy or phenoxy), 0.1-30wt.% hydroxylated (meth)acrylate unit of formula II (wherein R is H or methyl; and R is a 2-10C alkylene), and 0-50wt.% ethylenically unsatd. monomer.

4. 发明专利

JPH0459709A ATTACHING-INHIBITING AGENT TO MARINE ORGANISM 失效
公开(公告)号：JPH0459709A
公开(公告)日：1992-02-26
申请号：JP16766090
申请日：1990-06-25
申请人： NITTO KASEI CO LTD
发明人： FUJINO JUNJI , TABUCHI HITOSHI , TANIGUCHI HISASHI , MOTOTANI SHIGEO , TAKESAWA TOSHIYUKI
IPC分类号： A01N47/12 , A01N47/20 , A01N47/22
摘要： PURPOSE:To obtain the subject inhibiting agent exhibiting excellent killing effect to stain substance having excellent safety with low toxicity to human body, etc., without containing heavy metal containing a thiocarbamic acid compound readily obtained in high yield as an active ingredient. CONSTITUTION:The aimed attaching-inhibiting agent to marine organism contains a thiocarbamic acid compound (e.g. a compound having S as the X, O as the Y, CH3 as the R1 and Ch3CH2 as the R2 in formula I) expressed by formula I [R1 and R2 are alkyl, hydroxyalkyl, cycloalkyl, alkenyl, aralkyl, naphthyl or expressed by formula II (Z is H, halogen, alkyl, halogenated alkyl, alkoxy or nitro; m is 1 or 2); Y is S for X is O, or Y is O for X is S] as an active ingredient. Said inhibiting agent is safe and has low toxicity to human body without containing heavy metal and also exhibits excellent killing effect to stain substance.

5. 发明专利

JPH0436204A MARINE ORGANISM REPELLENT 失效
公开(公告)号：JPH0436204A
公开(公告)日：1992-02-06
申请号：JP14272090
申请日：1990-05-30
申请人： NITTO KASEI CO LTD
发明人： FUJINO JUNJI , TABUCHI HITOSHI , TANIGUCHI HISASHI , MOTOTANI SHIGEO
IPC分类号： C07D231/38 , A01N47/28 , A01N47/30 , A01N47/36 , C07D213/75
摘要： PURPOSE:To obtain the subject repellent, containing a specific thiourea compound as an active ingredient and having high antifouling effects on marine fouling organisms with low toxicity to human bodies, fishes, etc. CONSTITUTION:The subject repellent containing 2-30wt.% compound [e.g. N,N'- di(4-chlorophenyl)thiourea] expressed by formula I (R is alkyl, alkenyl, aralkyl or formula II to IV; X and Y are H, halogen or alkoxy;(m) and (n) are 1 or 2). The aforementioned repellent has preventive effects on attaching of noxious marine organisms to ship bottoms, fishing nets, etc. The compound expressed by formula I as an active ingredient may be used alone or together with a well-known antifouling compound (e.g. cuprous oxide). A resin which is used in normal marine organism repellents may be used as the applicable resin. If improvement in film properties such as adhesion or flexibility is required, plasticizers are used.

6. 发明专利

JPH11279455A Antifouling coating composition 失效
标题翻译：防喷涂组合物
公开(公告)号：JPH11279455A
公开(公告)日：1999-10-12
申请号：JP8328098
申请日：1998-03-30
申请人： Nitto Kasei Co Ltd , Nof Corp , 日本油脂株式会社 , 日東化成株式会社
发明人： MORI KIYOMI , TANIGUCHI HISASHI , MASUOKA SHIGERU , ITO MASAYASU
IPC分类号： C09D5/16 , C09D7/12 , C09D143/04 , C09D201/02
摘要： PROBLEM TO BE SOLVED: To obtain the subject composition, excellent in coating film properties and resistance to water, and keeping stable antifouling performance for extended periods by including a specific organosilicon compound in a polymer containing organic silicon. SOLUTION: This composition uses, as the vehicle, (A) a polymer containing organic silicon having a tri-organosilicon ester group, shown by Formula I (R to R are each a 1-18C alkyl, aryl or the like, wherein at least one of R to R has a carbon number of 3 or more), and also contains an organosilicon compound shown by formula II [R to R are each R , wherein a total carbon number of R to R is 6 or more; R is H, hydroxyl or the like; and (n) is 0 or 1]. The component A includes (meth)acrylic ester copolymer having a group shown by formula I. The component B includes tri-n-propylsilanol, and preferably a liquid or solid having a boiling point of 150 deg.C or more at normal pressure. It is preferable to use the component B at 0.1 to 20 wt.% on the solid in the coating material.
摘要翻译：要解决的问题：为了获得涂膜性能和耐水性优异并且通过在含有机硅的聚合物中包含特定的有机硅化合物来保持长时间的稳定的防污性能的主题组合物。解决方案：该组合物作为载体使用（A）含有有机硅的聚合物，其具有式III所示的三有机硅酯基（R 1至R 3）各自为1-18C烷基，芳基或其中R 1至R 3中的至少一个具有3个或更多个碳原子数），并且还包含式II所示的有机硅化合物[R 4至R 8各自为R <1>，其中R 4至R 8的总碳数为6以上; R 9是H，羟基等; 和（n）为0或1]。组分A包括具有式I所示基团的（甲基）丙烯酸酯共聚物。组分B包括三正丙基硅烷醇，优选在常压下沸点为150℃或更高的液体或固体。对涂料中的固体，优选使用0.1〜20重量％的成分B.

7. 发明专利

JPH10212293A PRODUCTION OF POLYMERIZABLE TRIORGANOSILYL UNSATURATED CARBOXYLATE 失效
公开(公告)号：JPH10212293A
公开(公告)日：1998-08-11
申请号：JP1850797
申请日：1997-01-31
申请人： NITTO KASEI CO LTD , NOF CORP
发明人： FUJINO JUNJI , TANIGUCHI HISASHI , MORI KIYOMI , MASUOKA SHIGERU , ITO MASAYASU
IPC分类号： B01J23/44 , B01J31/24 , C07B61/00 , C07B63/04 , C07F7/18
摘要： PROBLEM TO BE SOLVED: To provide the subject high-purity compound without causing by- products in high yield by reacting an unsaturated carboxylic acid with a triorganosilane in the presence of a reducing double bond by using a dehydrogenating catalyst. SOLUTION: An unsaturated carboxylic acid of formula I (R and R are each H, methyl or COOR ; R is H, an alkyl, an aryl, an aralkyl, etc.; R is H, methyl, CH2 COOR , etc.) is reacted with a triorganosilane of formula II (R to R are each an alkyl, a cycloalkyl, an aryl or an aralkyl) in the presence of a compound of formula III (R and R are each H, methyl, aryl, etc.; R is H, methyl, etc.; R is an alkyl, an alkenyl, an aryl, etc.), and a dehydrogenating catalyst at -20 to 250 deg.C to give a compound of the formula (R and R are each H, methyl or COOR ; R is an alkyl, an aryl, a triorganosilyl, etc.; R is H, methyl, CH2 COOR , etc.). No triorganosilyl saturated carboxylate as an unfavorable by-product is formed by this method.

8. 发明专利

JPH10195084A PRODUCTION OF POLYMERIZABLE TRIORGANOSILYL UNSATURATED CARBOXYLATE 失效
公开(公告)号：JPH10195084A
公开(公告)日：1998-07-28
申请号：JP446597
申请日：1997-01-14
申请人： NITTO KASEI CO LTD , NOF CORP
发明人： FUJINO JUNJI , TANIGUCHI HISASHI , MORI KIYOMI , MASUOKA SHIGERU , ITO MASAYASU
IPC分类号： B01J23/72 , B01J23/86 , B01J27/055 , B01J27/122 , B01J27/232 , B01J27/25 , B01J27/26 , B01J31/02 , B01J31/04 , B01J31/22 , C07B61/00 , C07F7/18 , C08F30/08
摘要： PROBLEM TO BE SOLVED: To obtain the subject compound in high purity and yield by reacting a specific unsaturated carboxylic acid with a specific triorganosilane in the presence of at least one kind of catalyst selected from copper and copper compounds. SOLUTION: This compound of formula III (R and R are each H, methyl, etc.; R is H, methyl, etc.) is obtained by reacting an unsaturated carboxylic acid (e.g. acrylic acid, methacrylic acid) of formula I (R and R are each H, methy, etc.; R is H, methyl, etc.) having 0.5-3 molar equivalents of carboxyl group with a triorganosilane of formula II (R and R are each an alkyl, cycloalkyl, aryl, etc.) in the presence of at least one kind of catalyst selected from among copper and copper compounds (e.g. copper oxide, copper suboxide, copper hydroxide, copper carboxylate, copper alkoxide, etc.) at 0.005-0.5mol, in terms of copper element, per mole of the organosilane at-20 to 250 deg.C, in an industrially advantageous way, with no reduction of the double bond of the polymerizable unsaturated carboxylic acid.

9. 发明专利

JPH08311083A PRODUCTION OF SILICON COMPOUND HAVING STERIC HINDRANCE 失效
公开(公告)号：JPH08311083A
公开(公告)日：1996-11-26
申请号：JP5160596
申请日：1996-03-08
申请人： NITTO KASEI CO LTD
发明人： SAKAMOTO NORIHIKO , TANIGUCHI HISASHI , INADA AKIHIRO , FUJIKAWA MASAZUMI
IPC分类号： C07F7/12
摘要： PURPOSE: To safely obtain a silicon compound having steric hindrance in high yield without removing by-products by reacting a Grignard reagent with a silicon compound in the presence of a cyano compound, etc., using a polyalkylene glycol as a solvent and distilling the reaction product. CONSTITUTION: The objective silicon compound having steric hindrance is produced in high yield by coupling a Grignard reagent expressed by formula II (R is a tertiary hydrocarbon group, a secondary hydrocarbon group or an aromatic hydrocarbon group; X is a halogen) with an organic silicon compound expressed by formula III (R is a hydrocarbon group; X is a halogen; m is an integer of 0-2) in the presence of a cyano compound, a thiocyanic acid compound or an acetylacetonate compound using a polyalkylene glycol dialkyl ether expressed by formula I (R and R are each a 1-8C alkyl; R is H or methyl; n is an integer of 1-6) as a solvent and separating and purifying a silicon compound having tertiary hydrocarbon group, a secondary hydrocarbon group or an aromatic hydrocarbon group from the reaction mixture by distillation.

10. 发明专利

JPH03258706A MARINE ANTIFOULING AGENT 失效
公开(公告)号：JPH03258706A
公开(公告)日：1991-11-19
申请号：JP5567290
申请日：1990-03-07
申请人： NITTO KASEI CO LTD
发明人： FUJINO JUNJI , TABUCHI HITOSHI , TANIGUCHI HISASHI , TAKESAWA TOSHIYUKI , MOTOTANI SHIGEO
IPC分类号： A01N51/00 , A01N47/46
摘要： PURPOSE:To obtain a marine antifouling agent having low toxicity and exhibiting antifouling effect over a long period by using N,N-dimethyl-N'-phenyl- N'-(fluorodichloromethylthio)-sulfamide and a compound such as 2,4- dichlorophenyl isothiocyanate as active components. CONSTITUTION:The objective agent is produced by using N,N-dimethyl-N'- phenyl-N'-(fluorodichloromethylthio)-sulfamide and at least one kind of compound selected from 2,4-dichlorophenyl isothiocyanate and 3,4-dichlorophenyl isothiocyanate as active components. The weight ratio of isocyanate: sulfamide is preferably 4:1 to 1:3, especially 2:1 to 1:2. The amount of the agent is preferably 5-300 pts.wt., especially

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