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1. 发明专利

JPH03255047A SUBSTITUTED BICYCLOHEPTADIONE DERIVATIVE, ITS PREPARATION AND HERBICIDE 失效
公开(公告)号：JPH03255047A
公开(公告)日：1991-11-13
申请号：JP17442190
申请日：1990-07-03
申请人： NIPPON SODA CO
发明人： UEDA AKIYOSHI , SUGA SHIGEMI , ADACHI HIROYUKI , AIHARA TOSHIO , TOMITA KAZUYUKI , YAMAGISHI HIDEKI , HOSAKA HIDEO
IPC分类号： C07D239/26 , A01N31/06 , A01N35/06 , A01N37/18 , A01N37/34 , A01N37/42 , A01N41/06 , A01N41/08 , A01N41/10 , A01N43/40 , A01N43/54 , A01N43/56 , A01N43/76 , A01N43/78 , C07C20060101 , C07C45/67 , C07C49/323 , C07C49/433 , C07C49/477 , C07C49/517 , C07C49/733 , C07C49/747 , C07C49/792 , C07C49/813 , C07C49/83 , C07C49/84 , C07C65/36 , C07C67/30 , C07C69/76 , C07C201/12 , C07C205/45 , C07C205/46 , C07C253/30 , C07C255/56 , C07C309/86 , C07C317/24 , C07C317/44 , C07C323/22 , C07C323/52 , C07D213/50 , C07D213/61 , C07D213/70 , C07D231/16 , C07D239/34 , C07D239/38 , C07D239/52 , C07D239/56 , C07D239/58 , C07D277/24 , C07D277/34 , C07D521/00
摘要： NEW MATERIAL:A substituted bicycloheptadione derivative of formula I [R is alkyl, (substituted) phenyl, (substituted) aralkyl, (substituted) heterocyclic group; R is halogen, alkoxy, alkylthio, alkynylsulfonyl, alkyl, alkoxyalkyl, alkoxyalkyl, alkoxycarbonyl; (n) is 0-4; R , R are H or alkyl] or a salt thereof. EXAMPLE:3-(2-Nitro-4-cyclobenzoyl)bicyclo[4,1,0]hepta-2,4-dione. USE:A herbicide which can be profitably synthesized, exhibits a sure activity in a small chemical amount, is highly safe and has good selectivity to crops. PREPARATION:A compound of formula II (Q is a releasable group) is subjected to a ring-closing reaction in the presence of a base to provide the compound of formula I.

2. 发明专利

JP2000212171A MOLECULAR COMPOUND HAVING DIHYDROXYTRIAZINE DERIVATIVE AS COMPONENT COMPOUND 失效
公开(公告)号：JP2000212171A
公开(公告)日：2000-08-02
申请号：JP985499
申请日：1999-01-18
申请人： NIPPON SODA CO
发明人： SUGA SHIGEMI , AOKI IZUO
IPC分类号： C07D275/02 , A01N25/22 , A61L9/01 , C07D213/16 , C07D233/58 , C07D251/34 , C07D275/03 , C07D307/06 , C07D319/12
摘要： PROBLEM TO BE SOLVED: To obtain the subject compound, showing excellent functions in various technical areas, e.g. selective separation of useful materials, being chemically stabilized, made non-volatile, released slowly or easily powdered, by including a specific dihydroxytriazine as the component compound. SOLUTION: This molecular compound comprises (A) a component compound of dihydroxytriazine derivative shown by the formula [R1 to R7 are each H, a halogen, OH, mercapto, amino, (saturated) 1-8C alkyl or the like; X is an unsubstituted group, sulfonyl, sulfinyl, thio, oxy or the like; and Y is oxy, thio or imino] and (B) a compound which can form a molecular compound with the component compound (A), e.g. toluene. A molecular compound means a compound composed of two or more component compounds, each of which can stably exist as a compound, bound to each other via a relatively weak interaction (e.g. hydrogen bonding or van der Waals force) other than covalent bond. Examples of these compounds include hydrates, solvates, adducts and clathrate compounds.

3. 发明专利

JPS6172783A Carboxyamidine derivative and herbicide 失效
标题翻译：羧甲酰胺衍生物和除草剂
公开(公告)号：JPS6172783A
公开(公告)日：1986-04-14
申请号：JP19369284
申请日：1984-09-14
申请人： Nippon Soda Co Ltd
发明人： HAYAKAWA KOICHI , SUGA SHIGEMI , ISHIKAWA HISAO , INABA HIDEO , SATO JUNJI
IPC分类号： A01N43/54 , A01N43/66 , C07D231/00 , C07D233/00 , C07D235/00 , C07D239/00 , C07D249/00 , C07D251/00 , C07D403/12 , C07D403/14
摘要： NEW MATERIAL:A compound of formula I [R
1 is imidazolyl, pyrazolyl or triazolyl which may be mono-, di- tri-substituted with halogen, nitro or lower alkyl; R
2 is formula III (x is halogen, lower alkyl; Y is lower alkyl, lower alkoxy), formula IV; R
3 is phenyl or phenoxy which is substituted with halogen or lower alkyl in its o-position]. E X A M P L E:N-(4,6-dimethylpyrimidine-2-yl)-N'-(2-methoxycarbonyl-ab-enzenesulfonyl)-1-imidazolecarboxy amidine.
USE: Herbicide: when it is applied to soil surfaces on preemergence of to foliage of weeds in their growing period on postemergence, it develops the herbicidal activity with very low doses.
PREPARATION: The reaction between a compound of formula II and a compound of the formula: R
1 H is carried out in accordance with the reaction equation to give the compound of formula I.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：新材料：式I化合物[R1为咪唑基，吡唑基或三唑基，可以被卤素，硝基或低级烷基单取代，二取代; R2是式III（x是卤素，低级烷基; Y是低级烷基，低级烷氧基），式IV; R3是在其位置被卤素或低级烷基取代的苯基或苯氧基]。 E X A M P L E：N-（4,6-二甲基嘧啶-2-基）-N' - （2-甲氧基羰基 - 联苯磺酰基）-1-咪唑基亚氨基脒。用途：除草剂：当芽后生长期对杂草叶片的出苗时施用于土壤表面时，以非常低的剂量产生除草活性。制备：式II化合物与式R1H化合物的反应按照反应方程进行，得到式Ⅰ化合物。

4. 发明专利

JP2009057299A Substituted phenoxyazabicyclooctane derivative and method for producing the same 有权
标题翻译：取代的苯氧基羰基衍生物及其制备方法
公开(公告)号：JP2009057299A
公开(公告)日：2009-03-19
申请号：JP2007224234
申请日：2007-08-30
申请人： Nippon Soda Co Ltd , 日本曹達株式会社
发明人： SUGA SHIGEMI , OOOKA HIROHITO , HIROKAWA KENICHI , IMAGAWA TSUTOMU
IPC分类号： C07D221/22
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a substituted phenoxyazabicyclooctane derivative [compound (V)] in a high yield by using readily available raw materials and to provide a new 2-halogenophenoxyazabicyclooctane derivative [compound (III) and compound (V)]. SOLUTION: The method for producing a substituted phenoxyazabicyclooctane derivative represented by the formula (V) comprises reacting an azabicyclool derivative represented by formula (I) with a halogenobenzene compound represented by the formula (II) in the presence of a base at ≤20°C to give a 2-halogenophenoxyazabicyclooctane derivative represented by the formula (III) and reacting the obtained 2-halogenophenoxyazabicyclooctane derivative represented by the formula (III) with an alcohol compound represented by the formula (IV), wherein R 1 and R 2 are each a substituent group-containing 1-20C alkyl group or the like; n is 1 or 2; R 3 is a 1-20C haloalkyl group or the like; and X is a halogen. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供通过使用容易获得的原料以高产率制备取代的苯氧基偶氮二环辛烷衍生物[化合物（V）]的方法，并提供新的2-卤代苯氧基氮杂双环辛烷衍生物[化合物（III）和化合物（V）]。解决方案：用于制备由式（Ⅴ）表示的取代的苯氧基氮杂双环辛烷衍生物的方法包括使式（I）表示的氮杂双环衍生物与式（II）表示的卤代苯化合物在碱的存在下， 20℃，得到式（III）表示的2-卤代苯氧基氮杂双环辛烷衍生物，将得到的式（III）表示的2-卤代苯氧基氮杂双环辛烷衍生物与式（IV）表示的醇化合物反应，其中R SB ＆lt; / SB＆gt;和R＆lt; SB＆gt; 2＆lt; / SB＆gt;各自为含有取代基的1-20C烷基等; n为1或2; R SB 3是1-20C卤代烷基等; X是卤素。版权所有（C）2009，JPO＆INPIT

5. 发明专利

JP2006104197A Optically active heterocyclic compound, its preparation method, medicinal composition, and therapeutic method 审中-公开
标题翻译：光学活性杂环化合物，其制备方法，药物组合物和治疗方法
公开(公告)号：JP2006104197A
公开(公告)日：2006-04-20
申请号：JP2005262990
申请日：2005-09-09
申请人： Nippon Soda Co Ltd , 日本曹達株式会社
发明人： SUGA SHIGEMI , YAGIHARA TOMIO , OKADA KATSUMI , TAKAGI MASAE , NAGANO YASUKO
IPC分类号： C07D263/10 , A61K31/421 , A61P1/04 , A61P9/10 , A61P11/00 , A61P11/02 , A61P11/06 , A61P13/12 , A61P17/00 , A61P17/06 , A61P17/16 , A61P19/02 , A61P25/00 , A61P29/00 , A61P31/04 , A61P37/02 , A61P37/08 , A61P39/00 , A61P43/00
摘要： PROBLEM TO BE SOLVED: To provide an optically active heterocyclic compound which causes less side effects and is safer and more excellent in pharmacological activity; its preparation method; and a medicinal composition. SOLUTION: For example, a heterocyclic compound represented by formula [I] and its complex are provided. In formula [I], X is an oxygen or sulfur atom; Q 1 is -(CH 2 ) n - (wherein n is an integer of 0-3) or -CH=CH-; R 1 is an optionally substituted alkyl or phenyl group or the like; R 2 is an optionally substituted phenyl group or the like; R 3 is a hydrogen atom, an optionally substituted alkyl, alkylcarbonyl, alkoxycarbonyl or alkylsulfonyl group or the like; and R 4 and R 5 are each a hydrogen atom, a nitro, cyano or alkyl group or the like. A preparation method of the compound is also provided, together with a medicinal composition. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供导致副作用较小并且药理活性更加安全和更优异的旋光性杂环化合物; 其制备方法; 和药用组合物。解决方案：例如，提供由式[I]表示的杂环化合物及其络合物。在式[I]中，X是氧或硫原子; （其中n为0-3的整数）或-CH = CH-;其中n为0-3的整数。 R SB 1是任选取代的烷基或苯基等; R SB 2是任选取代的苯基等; R 3是氢原子，任选取代的烷基，烷基羰基，烷氧基羰基或烷基磺酰基等; R 4和R 5各自为氢原子，硝基，氰基或烷基等。还提供了化合物的制备方法以及药用组合物。版权所有（C）2006，JPO＆NCIPI

6. 发明专利

JPH03181464A NICOTINIC ACID DERIVATIVE HAVING SUBSTITUTED GROUP AND PRODUCTION THEREOF 失效
公开(公告)号：JPH03181464A
公开(公告)日：1991-08-07
申请号：JP32050689
申请日：1989-12-12
申请人： NIPPON SODA CO
发明人： UEDA AKIYOSHI , SUGA SHIGEMI
IPC分类号： C07D213/80 , A01N43/40 , C07D213/84
摘要： NEW MATERIAL:A compound expressed by formula I {R is H or alkyl; R1 is cyano or -Z-R2 [Z is 0 or -S(O)m-; R2 is alkyl, alkenyl, substitutable phenyl, benzyl, substituted heterocycle, alkoxyalkyl or alkylthioalkyl, m is 0, 1 or 2]). EXAMPLE:2-methyl-2-methylmercaptonicotinic acid ethyl ester. USE:Useful as intermediate of agricultural chemical or medical drug, especially as intermediate of herbicide. PREPARATION:A compound expressed by formula II (X is halogen or cyano) is reacted with a compound expressed by the formula R2-Z-M (M is alkali metal) in a solvent miscible to water such as DMF or lower alcohol, or a mixed solvent of the solvent and water at 0-70 deg.C, preferably at room temperature to afford the compound expressed by formula I.

7. 发明专利

JPH0348635A SUBSTITUTED CYCLOHEXADIONE DERIVATIVE, ITS PRODUCTION AND HERBICIDE 失效
公开(公告)号：JPH0348635A
公开(公告)日：1991-03-01
申请号：JP18225889
申请日：1989-07-14
申请人： NIPPON SODA CO
发明人： UEDA AKIYOSHI , SUGA SHIGEMI , MIYAZAWA YASUYUKI , AIHARA TOSHIO , TOMITA KAZUYUKI , YAMAGISHI HIDEKI , HOSAKA HIDEO
IPC分类号： C07D213/50 , A01N35/06 , A01N35/10 , A01N41/10 , B01J23/02 , B01J27/138 , B01J27/18 , B01J27/232 , C07B61/00 , C07C45/38 , C07C45/42 , C07C45/51 , C07C45/72 , C07C49/417 , C07C49/517 , C07C49/657 , C07C49/683 , C07C49/693 , C07C49/697 , C07C49/713 , C07C49/723 , C07C49/743 , C07C49/747 , C07C49/753 , C07C49/757 , C07C49/792 , C07C49/798 , C07C49/835 , C07C49/84 , C07C205/45 , C07C251/40 , C07C251/42 , C07C251/52 , C07C251/60 , C07C255/56 , C07C317/24 , C07C317/32 , C07C323/22 , C07C323/47 , C07C323/52 , C07D213/57 , C07D213/61 , C07D213/63 , C07D213/70
摘要： NEW MATERIAL:A compound selected from a substituted cyclohexadione derivative of formula I [R is alkyl, phenyl, aralkyl or heterocyclic group; Y is alkylene; (m) is 0 or 1; R is H or alkyl; R is halogen, cyano, alkyl, haloalkyl, phenyl, etc.; (n) is 0-5; Z is W (W is halogen, etc.) or OR (R is alkyl); Z is SR6 (R is phenyl, etc.), OR or Z and Z together form O, etc.], its salt, enamine or its analog, acylate, sulfonate, carbamate and ether derivative. EXAMPLE:5-(alpha-Chlorophenylthiomethyl)-2-(2-nitro-4-chlorobenzoyl)cy clohexane-1,3- dione. USE:A herbicide. PREPARATION:The compound of formula III (a compound of formula I wherein Z and Z are OR ) can be produced e.g. by selectively oxidizing a compound of formula II.

8. 发明专利

JP2009298793A Host compound for clathrate compound 有权
标题翻译：主题化合物用于分离化合物
公开(公告)号：JP2009298793A
公开(公告)日：2009-12-24
申请号：JP2009179390
申请日：2009-07-31
申请人： Nippon Soda Co Ltd , 日本曹達株式会社
发明人： SUGA SHIGEMI , AOKI IZUO
IPC分类号： C07D251/32 , A01N25/00 , A01N25/22 , A01N43/80 , A01P3/00
摘要： PROBLEM TO BE SOLVED: To provide a host compound for a clathrate compound showing extremely excellent property in the technical field of selective separation of useful substance, chemical stabilization, non-volatilization, sustained-releasing, pulverization, etc. SOLUTION: This host compound for the clathrate compound comprises a dihydroxy triazine derivative represented by general formula (I) [wherein R 1 -R 7 may be mutually the same or different and represent a group selected from the group consisting of a hydrogen atom, a halogen atom, a hydroxy group, a mercapto group, an amino group, a 1-8C saturated or unsaturated alkyl group, a 1-8C saturated or unsaturated alkoxy group, a 1-8C saturated or unsaturated alkylthio group, a 1-8C saturated or unsaturated alkylamino group, a 1-8C saturated or unsaturated dialkylamino group, a 1-8C saturated or unsaturated alkylsulfonyl group, an aromatic group, an arylthio group, an arylamino group, etc., Y represents a group selected from the group consisting of an oxy group, a thio group, and an imino group]. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供在有用物质的选择性分离，化学稳定化，非挥发，持续释放，粉碎等技术领域中表现出极好的性能的笼形化合物的主体化合物。解决方案：用于包合化合物的该主体化合物包含由通式（I）表示的二羟基三嗪衍生物[其中R 1 -R 7 可以相同或不同，表示选自氢原子，卤素原子，羟基，巯基，氨基，1-8C饱和或不饱和烷基，1-8C饱和或不饱和烷氧基， 1-8C饱和或不饱和烷硫基，1-8C饱和或不饱和烷基氨基，1-8C饱和或不饱和二烷基氨基，1-8C饱和或不饱和烷基磺酰基，芳基，芳硫基，芳基氨基等，Y表示一组sel 来自由氧基，硫基和亚氨基组成的组]。版权所有（C）2010，JPO＆INPIT

9. 发明专利

JP2001039971A MOLECULAR COMPOUND CONTAINING TRI-O-THYMOTIDES AS CONSTITUENT COMPOUND 失效
公开(公告)号：JP2001039971A
公开(公告)日：2001-02-13
申请号：JP21430599
申请日：1999-07-28
申请人： NIPPON SODA CO
发明人： SUGA SHIGEMI , SUZUKI HIROYUKI
IPC分类号： C07D323/00 , A01N37/10 , C07D213/71 , C07D213/89 , C07D341/00
摘要： PROBLEM TO BE SOLVED: To obtain a molecular compound having new useful properties such as sustained release, decrease of skin irritation, chemical stability, involatity, powderization, selective separation of useful materials or the like other than inherent properties in effective components and useful as a germicide, an antibacterial agent, an insecticide, an insect repellent, a flavor, an antifoulant and a curing agent for epoxy resins. SOLUTION: This molecular compound is obtained by reacting tri-o- thymotides represented by the formula (R1 to R12 are each independently H or a 1-6C straight chain or branched alkyl group; and X is O or S) with a germicide, an antibacterial agent, an antifungal agent, an insecticide, an insect pest-repellent, a flavor, a deodorant, an antifoulant, a curing and accelerating agent for paints, resins and adhesives, a natural essential oil, an antioxidant or a vulcanization accelerator capable of forming a molecular compound with tri-o-thymotides.

10. 发明专利

JPH0352862A SUBSTITUTED PYRIDINE DERIVATIVE, PRODUCTION THEREOF AND HERBICIDE 失效
公开(公告)号：JPH0352862A
公开(公告)日：1991-03-07
申请号：JP18594589
申请日：1989-07-20
申请人： NIPPON SODA CO
发明人： UEDA AKIYOSHI , SUGA SHIGEMI , TOMITA KAZUYUKI , HOSAKA HIDEO
IPC分类号： C07D213/50 , A01N43/40 , C07D213/84 , C07D405/08 , C07D409/08
摘要： NEW MATERIAL:A compound expressed by formula I, salt of said compound or enamine, acylate, sulfonate, carbamate and ether derivative of said compound [Y is lower alkylene; m is 0 or 1; R1 is OH, halogen, CN, NO2, heterocycle or Z-R4 (Z is O, S, SO or NH, etc.; R4 is alkyl, alkenyl, alkinyl or phenyl, etc.), etc.; R2 is halogen, CN, alkyl, alkoxycarbonyl or phenyl, etc.; l is 1-5; R3 is halogen, OH, NO2, CN, alkyl, alkenyl, monoalkylamino, alkoxycarbonyl, phenyl or heterocycle, etc.; n is 0-4]. EXAMPLE:2-(2-methyl-6-chloronicotinoyl)-5-methoxynethylcyclohexa-1,3-d ione. USE:Used as herbicide. PREPARATION:A compound expressed by formula II (Q is eliminating group) is reacted with a compound expressed by formula III in the presence of base and transformed in the presence of cyano compound and base to afford the aimed compound.

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