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1. 发明专利

JPS6259201A IMMOBILIZED GERMICIDE AND PRODUCTION THEREOF 失效
公开(公告)号：JPS6259201A
公开(公告)日：1987-03-14
申请号：JP19900185
申请日：1985-09-09
申请人： NIPPON SHEET GLASS CO LTD , WATANABE SHOICHIRO
发明人： WATANABE SHOICHIRO , UCHIBORI TAKESHI , KAWADA KAZUO , MASE SHOJI , YOSHIDA MOTOAKI , TAKIGAWA AKIO , MAEDA KOICHI , AOKI YUICHI , TAGO IKUO , HIRAYAMA NAOTO
IPC分类号： A61K31/05 , A01N25/24 , A61K31/047 , A61K47/00 , A61K47/48 , A61P31/04
摘要： PURPOSE:An immobilized germicide, obtained by immobilizing a specific compound in a polysaccharide subjected to specific treatment as a substrate, slightly liberating a drug from the polysaccharide, capable of exhibiting improved germicidal efficacy against Gram-positive and Gram-negative bacteria and useful in laboratories, etc. CONSTITUTION:An immobilized germicide obtained by treating the surface of a substrate consisting of a polysaccharide, e.g. cellulose, beta-cyclodextrin, dextrin, dextran or starch, with a silane coupling agent of a primary or secondary amine, e.g. gamma-aminopropyltriethoxysilane, and condensing the treated substrate with a compound, having at least phenolic OH group and capable of leaving the phenolic group even after reaction with the above-mentioned coupling agent, e.g. p-hydroxybenzyl alcohol, in the presence of palladium black as a catalyst in N2 atmosphere through dehydration. EFFECT:The residual property of the drug can be reduced and continuous sterilization can be carried out. Materials can be treated in a large amount by simple sterilizing operation, etc.

2. 发明专利

JPH0525299A PRODUCTION OF PLASTIC LENS 失效
公开(公告)号：JPH0525299A
公开(公告)日：1993-02-02
申请号：JP16539791
申请日：1991-07-05
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , OTANI NOBORU , YOSHIDA MOTOAKI
IPC分类号： B32B7/02 , B29D11/00 , B32B9/00 , B32B25/08 , B32B25/20 , B32B27/40 , C08G18/80 , C08J7/04 , C23C14/06 , G02B1/04 , G02B1/10 , G02B1/11 , G02B1/115 , G02B1/14
摘要： PURPOSE:To provide a lens comprising a hard coat and a reflection-preventive coat disposed thereon which is excellent in impact resistance and free from a trouble of staining a liquid for a hard coat. CONSTITUTION:The surface of a plastic lens base is coated with a primer coating contg. a blocked polyisocyanate and a polyol as the main components, which is then cured by heat to form a heat-curable polyurethane primer layer, on which a hard coat is then provided, followed by vapor deposition of an inorg. substance(s) on the surface of the hard coat to form a single or multiple reflection-preventive layers. In the foregoing process for producing a plastic lens, the blocked polyisocyanate of the primer coating which is used as a main component in combination with the polyol as another main component is blocked with a beta-diketone.

3. 发明专利

JPS62125302A PREPARATION OF PLASTIC LIGHT TRANSMITTING BODY 失效
公开(公告)号：JPS62125302A
公开(公告)日：1987-06-06
申请号：JP26684385
申请日：1985-11-27
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , YOSHIDA MOTOAKI , TAKIGAWA AKIO , MAEDA KOICHI , AOKI YUICHI , TAGO IKUO
IPC分类号： C08F2/02 , G02B6/00
摘要： PURPOSE:To obtain a light transmitting body having extremely high precision of shape and stable quality by coating the inside wall surface of a vessel with a copolymer of monomers having the highest monomer reactivity ratio or with a material having high affinity with the copolymer. CONSTITUTION:Inside wall surface of a polymn. tube 1 is coated previously with an acrylic F-contg. resin paint. The polymn. tube 1 is transferred from above downward with a fixed speed through a constant temp. chamber 2A. Thus, the monomer mixture in the tube 1 is heated and irradiated with light successively from its foot end. Copolymn. occurs at the bottom of the polymn. tube 1. Although the volume of the polymn. tube 1 is contracted by the polymn., no void is formed in the polymn. tube by the continuous feed of the monomer mixture from an unpolymerized part at the top of the polymn. tube 1. In accordance with the movement of the polymn. tube 1, the polymerizing part is transferred upward successively, and finally the whole monomer mixture in the polymn. tube 1 is solidified.

4. 发明专利

JPH04366801A PLASTIC LENS 失效
公开(公告)号：JPH04366801A
公开(公告)日：1992-12-18
申请号：JP14169691
申请日：1991-06-13
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , OTANI NOBORU , YOSHIDA MOTOAKI , ISHIZUKA SATOSHI , KASHIWAGI HISAYUKI , HIRAYAMA NAOTO
IPC分类号： G02B1/04 , G02B1/10 , G02B1/115 , G02B1/14 , G02C7/02
摘要： PURPOSE:To eliminate interference fringes and to improve the impact resistance and weatherability after antireflection coating by laminating a primer layer, a hard coat layer and an antireflection layer on the surface of a base material and, using specific polyurethane as the primer layer. CONSTITUTION:The primer layer which has a refractive index np satisfying the conditions of equation I and a film thickness d satisfying the conditions of equation II is formed on the surface of the plastic lens base material having the refractive index nS within a range from 1. 50 to 1. 70. The hard coat layer and the single or multilayered antireflection layers formed by vapor deposition of an inorg. material are laminated in this order from the lens surface. The primer layer is formed of the polyurethane which contains at least one selected from halogen atoms and sulfur atoms exclusive of fluorine and has the refractive index np within a range from 1.45 to 1.60. In the equation I, nS is the refractive index of the plastic base material; nH is the refractive index of the hard coat layer ; the refractive indices are both the refractive indices to light of 550nm wavelength. In the equation II, lambda is the wavelength of visible light and is 450 to 650nm.

5. 发明专利

JPH03269507A PLASTIC LENS HAVING DIMMING PROPERTY 失效
公开(公告)号：JPH03269507A
公开(公告)日：1991-12-02
申请号：JP7089390
申请日：1990-03-20
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , OTANI NOBORU , YOSHIDA MOTOAKI
IPC分类号： G02C7/10 , G02B1/04 , G02B1/10 , G02B1/14 , G02B5/23 , G03C1/685
摘要： PURPOSE:To improve the resistance to wear, impact, weather and chemicals and the response speed of dimming by providing a primer layer consisting of thermosetting type polyurethane contg. a photochromic material on the surface of a lens base material and further providing a hard coat layer consisting of a silicone resin. CONSTITUTION:A coating material for a primer essentially consisting of block type polyisocyanate and polyol and further, contg. the photochromic material is applied on a lens and is cured by heating in order to form a primer layer. Oxazine photochromic materials, such as spirophotooxazine, 5- chlorospironaphotooxazine and spirophenanthrooxazine, are included as the examples of the photochromic material. The heard coat layer consisting of the silicone resin is provided on this polyurethane primer layer. The rate of the reaction of the photochromic material when the layer is irradiated with light is increased in this way and the response speed of dimming is increased. In addition, the deterioration of the photochromic material by oxidation is lessened.

6. 发明专利

JPH03109502A PRODUCTION OF PLASTIC LENS 失效
公开(公告)号：JPH03109502A
公开(公告)日：1991-05-09
申请号：JP32826089
申请日：1989-12-20
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , OTANI NOBORU , YOSHIDA MOTOAKI
IPC分类号： B29D11/00 , G02B1/11 , G02B1/115 , G02B1/14
摘要： PURPOSE:To improve impact resistance and to prevent the contamination of a hard coat liquid by using thermosetting polymer urethane as polyurethane for forming a primer layer. CONSTITUTION:The thermosetting polymer urethane is used as the polyurethane for forming the primer layer. The primer layer consisting of the thermosetting polymer urethane is provided between the plastic lens and the hard coat layer in this case and, therefore, even the lens formed by providing an antireflection film layer on the hard coat layer has excellent impact resistance and meets the requirements specified by FDA of the United States and has the higher impact resistance than the lens provided with the primer layer consisting of thermoplastic polyurethane. Even if the lens provided with the primer layer is immersed to the hard coat liquid, the polyurethane which is the primer component has a thermosetting property and, therefore, the primer layer does not elute in the hard coat liquid and there is no possibility that the hard coat liquid is contaminated. The homogeneous plastic lens is obtd. in such a manner.

7. 发明专利

JP2001051101A PRIMER COMPOSITION FOR PLASTIC LENS 失效
公开(公告)号：JP2001051101A
公开(公告)日：2001-02-23
申请号：JP2000056732
申请日：2000-03-02
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , OTANI NOBORU , YOSHIDA MOTOAKI
IPC分类号： G02B1/10 , G02B1/115 , G02B1/14
摘要： PROBLEM TO BE SOLVED: To provide a primer composition for a plastic lens suitable to manufacture the plastic lens excellent in wear resistance, impact resistance, antireflectivity, weather resistance, chemical resistance, and adhesive property of a coating film. SOLUTION: This primer composition for a plastic lens covers a plastic lens base material surface as a primer layer for forming a hardcoat layer of a silicone resin and a monolayer or multilayer antireflection film of inorganic substance on the surface of the hardcoat layer. The primer composition contains a block type polyisocyanate, a polyester polyol, a curing catalyst and a solvent.

8. 发明专利

JPH0651104A ANTIREFLECTION PLASTIC LENS 失效
公开(公告)号：JPH0651104A
公开(公告)日：1994-02-25
申请号：JP20480192
申请日：1992-07-31
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , OTANI NOBORU , YOSHIDA MOTOAKI
IPC分类号： G02B1/04 , G02B1/10 , G02B1/11
摘要： PURPOSE:To obtain an antireflection plastic lens free of interference fringes and excellent in impact resistance after being coated. CONSTITUTION:A primer layer, a siliconic hard coat layer of refractive index nH and a single or multiple-layered antireflection layer by the vapor deposition of inorg. matter are laminated in this order on the surface of a plastic lens having 1.64-1.70 refractive index nS to obtain an antireflection plastic lens. The primer layer consists of the polyurethane obtained by the reaction of a polyol with the block body of a polyisocyanate having an aromatic ring, and the antireflection plastic lens has a refractive index of nP and a thickness of (d) fulfilling the specified two conditions.

9. 发明专利

JPH0641519A ANTI-FOGGING COATING COMPOSITION 失效
公开(公告)号：JPH0641519A
公开(公告)日：1994-02-15
申请号：JP2321587
申请日：1987-02-03
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , OTANI NOBORU
IPC分类号： C08L33/26 , C08L33/24 , C09D133/04 , C09D133/26 , C09K3/18
摘要： PURPOSE:To provide the coating composition useful for a coating film, etc., having excellent scratch resistance and weather resistance, comprising a specific copolymer, a specific epoxy group-containing polymer and a specific epoxy group-organic silane compound, etc., in a specific ratio. CONSTITUTION:The coating composition comprises (A) 40-70 pts.wt. copolymer consisting of (i) 50-80wt.% repeating structural unit of formula I (each of R1 to R4 is H of a lower alkyl) and (ii) 20-50wt.% repeating structural unit of formula II (each of R5 and R6 is R1; X is a hydroxyl group-containing organic group), (B) 30-60 pts.wt. (co)polymer containing 20wt.% or more repeating structural unit of formula III (each of R7 and R8 is R1; Y is an epoxy group- containing organic group), (C) 0.3-30 pts.wt. based on 100 pts.wt. total amounts of the components A and B) epoxy group-containing organic silane compound and/or melamine skeleton-containing compound and further a curing catalyst.

10. 发明专利

JPS6298303A PREPARATION OF PLASTIC OPTICAL FIBER 失效
公开(公告)号：JPS6298303A
公开(公告)日：1987-05-07
申请号：JP23904385
申请日：1985-10-25
申请人： NIPPON SHEET GLASS CO LTD
发明人： MASE SHOJI , YOSHIDA MOTOAKI , TAKIGAWA AKIO , MAEDA KOICHI , AOKI YUICHI , TAGO IKUO
IPC分类号： D01F8/14 , C08J3/24 , D06M10/00 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/32 , G02B6/00
摘要： PURPOSE:To obtain optical fiber having superior heat resistance in the environment >=ca. 100 deg.C by forming optical fiber consisting of a core part comprising unsatd. polyester resin and a clad part comprising another unsatd. polyester resin having lower refractive index than said unsatd. polyester resin, and subjecting the fiber to heat treatment or irradiation with active rays. CONSTITUTION:Polyester resin synthesized from, for example, maleic anhydride and bisphenol A, is used as the core material. Further, polyester resin synthesized from, for example, maleic anhydride and fluorinated bisphenol A is used as the clad material. Thereafter, ca. 1% dicumyl peroxide is added to both the core material and the clad material, and melt spinning is performed at ca. 100 deg.C using a jacketted pot. Obtd. optical fiber is heat-treated at ca. 150 deg.C for ca. 2hr. Thus, three-dimensinally crosslinked optical fiber is obtd.

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