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1. 发明专利

JP2002069064A METHOD FOR PRODUCING gamma-BUTYROLACTONE 失效
公开(公告)号：JP2002069064A
公开(公告)日：2002-03-08
申请号：JP2000254333
申请日：2000-08-24
申请人： NEW JAPAN CHEM CO LTD , TONEN SEKIYUKAGAKU KK
发明人： MASAMI HIROSHI , YOSHIDA YASUHISA , ICHIKI TATSUMI , ISHIHARA TAKESHI , HAMASHIMA NAGATO , KOBAYASHI KENJI
IPC分类号： C07D307/33 , C07B61/00
摘要： PROBLEM TO BE SOLVED: To obtain γ-butyrolactone in a high yield productivity, efficiently and safely. SOLUTION: This method for producing γ-butyrolactone comprises (a) supplying a solution of maleic anhydride and hydrogen to a multitube type reactor charged with a Ru-supported catalyst to hydrogenate maleic anhydride and pulling out excessive hydrogen and a formed solution of succinic anhydride and (b) supplying the solution of succinic anhydride and hydrogen to a multitube type reactor charged with a catalyst supporting at least one kind of a metal of the group VIII and Re to hydrogenate succinic anhydride and pulling out excessive hydrogen, formed γ-butyrolactone and a solvent.

2. 发明专利

JP2004307392A Method for producing alicyclic group-substituted silane compound 有权
标题翻译：生产聚硅氧烷基取代的硅烷化合物的方法
公开(公告)号：JP2004307392A
公开(公告)日：2004-11-04
申请号：JP2003103162
申请日：2003-04-07
申请人： New Japan Chem Co Ltd , 新日本理化株式会社
发明人： YOSHIDA YASUHISA , HATTORI KAZUHIRO , MASAMI HIROSHI
IPC分类号： C07B61/00 , C07F7/08 , C07F7/18
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an alicyclic group-substituted silane compound efficiently and industrially advantageously.
SOLUTION: This method comprises hydrogenating a corresponding aromatic group-substituted silane compound using a ruthenium catalyst.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题：提供在工业上有利地制备脂环基取代的硅烷化合物的方法。解决方案：该方法包括使用钌催化剂氢化相应的芳基取代的硅烷化合物。版权所有（C）2005，JPO＆NCIPI

3. 发明专利

JP2004203792A 4-chloroformylcyclohexane-1, 2-dicarboxylic anhydride and method for producing the same 审中-公开
公开(公告)号：JP2004203792A
公开(公告)日：2004-07-22
申请号：JP2002375778
申请日：2002-12-26
申请人： New Japan Chem Co Ltd , 新日本理化株式会社
发明人： HATTORI KAZUHIRO , YOSHIDA YASUHISA , MASAMI HIROSHI
IPC分类号： C07D307/77
摘要： PROBLEM TO BE SOLVED: To obtain a novel highly reactive 4-chloroformylcyclohexane-1,2-dicarboxylic anhydride represented by formula (1), and to provide a method for producing the same.
SOLUTION: The method for producing 4-chloroformylcyclohexane-1,2-dicarboxylic anhydride comprises treating 4-carboxycyclohexane-1,2-dicarboxylic anhydride represented by formula (2) with a chlorinating agent.
COPYRIGHT: (C)2004,JPO&NCIPI

4. 发明专利

JP2004083917A Lubricant 有权
公开(公告)号：JP2004083917A
公开(公告)日：2004-03-18
申请号：JP2003412619
申请日：2003-12-10
申请人： New Japan Chem Co Ltd , 新日本理化株式会社
发明人： KAWAHARA YASUYUKI , SAITOU MIKIO , FUSHIMI ICHIRO , MITSUYA YUKIHISA , YOSHIDA YASUHISA , TOKASHIKI MICHIHIDE
IPC分类号： C10M105/36 , C10M101/02 , C10M101/04 , C10M105/04 , C10M105/42 , C10M107/08 , C10N30/00 , C10N40/20
摘要： PROBLEM TO BE SOLVED: To provide a lubricant having excellent hydrolytic stability even in severe working condition and usable in wide field.
SOLUTION: The lubricant (except a refrigerator lubricant containing an alicyclic polycarboxylate represented by general formula [I]) contains one or more alicyclic polycarboxylate represented by general formula [I] (wherein, A is cyclohexane ring or cyclohexene ring; R
1 is H or methyl; X is H or COOR
4 ; Y is H or COOR
5 ; R
2 , R
3 , R
4 and R
5 may be the same as or different from each other and are a 3-18C branched alkyl, a 3-10C cycloalkyl, a 1-18C straight chain alkyl or a 2-18C straight chain alkenyl).
COPYRIGHT: (C)2004,JPO

5. 发明专利

JP2000007595A PRODUCTION OF CYCLOHEXANEDIMETHANOL 失效
公开(公告)号：JP2000007595A
公开(公告)日：2000-01-11
申请号：JP17990698
申请日：1998-06-26
申请人： NEW JAPAN CHEM CO LTD
发明人： ITO HIROSHI , IWAMURA TAIICHIRO , YOSHIDA YASUHISA , NAKAZAWA MIKIRO
IPC分类号： B01J23/80 , B01J23/86 , C07B61/00 , C07C29/149 , C07C29/80 , C07C31/27
摘要： PROBLEM TO BE SOLVED: To obtain a high-quality cyclohexanedimethanol by keeping the content of copper in distillation liquid during distillation in a specific concentration when a reaction crude material obtained by reducing a dialkyl cyclohexanedicarboxylate in the presence of a copper-based catalyst is purified by distillation under reduced pressure. SOLUTION: When a reaction crude material contained in cyclohexanedimethanol of formula II obtained by reducing a dialkyl cyclohexanedicarboxylate of formula I (R is a 1-4C alkyl) in the presence of a copper-based catalyst (e.g. copper oxide/chromium oxide) is distilled under reduced pressure, the content of copper contained in distillation liquid during distillation is kept in the concentration of

6. 发明专利

JP2003026766A Epoxy-based reactive diluent and liquid epoxy resin composition containing the same 审中-公开
标题翻译：基于环氧的反应性稀释液和含有它的液体环氧树脂组合物
公开(公告)号：JP2003026766A
公开(公告)日：2003-01-29
申请号：JP2001213366
申请日：2001-07-13
申请人： New Japan Chem Co Ltd , 新日本理化株式会社
发明人： YOSHIMURA RIEKO , NOBE TOMIO , YOSHIDA YASUHISA , FUJITANI TSURATAKE
IPC分类号： C08G59/24 , H01L23/29 , H01L23/31
摘要： PROBLEM TO BE SOLVED: To provide a liquid epoxy resin composition which contains an epoxy- based reactive diluent and is useful as a sealing material for semiconductor package, a sealing material for a photoelectric conversion element, a conductive adhesive, a die-bonding paste, an anisotropic conductive paste, and a joint filler for viaholes, through holes, etc.
SOLUTION: This epoxy resin composition contains (A) an epoxy resin, (B) a reactive diluent, (C) a curing agent, and optionally (D) a filler. Ingredient B is a nuclear hydrogenation product of bisphenol A diglycidyl ether, has a content (obtained by GPC) of a compound represented by formula (1) of 5 wt.% or lower, a degree of nuclear hydrogenation of 80% or higher, a chlorine content of 0.2 wt.% or lower, an epoxy equivalent of 210 or lower, and a viscosity of 1,000 mPa s or lower.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供含有环氧类反应性稀释剂并可用作半导体封装用密封材料的液态环氧树脂组合物，用于光电转换元件的密封材料，导电粘合剂，芯片粘合膏，各向异性导电膏，以及用于通孔，通孔等的接合填料。解决方案：该环氧树脂组合物含有（A）环氧树脂，（B）反应性稀释剂，（C）固化剂和任选的（D）填料。成分B是双酚A二缩水甘油醚的核氢化物，具有式（1）表示的化合物的含量（GPC得到）为5重量％以下，核氢化度为80％以上的成分氯含量为0.2重量％以下，环氧当量为210以下，粘度为1000mPa·s以下。

7. 发明专利

JP2002003484A METHOD FOR PRODUCING SUCCINIC ANHYDRIDE 失效
公开(公告)号：JP2002003484A
公开(公告)日：2002-01-09
申请号：JP2000186373
申请日：2000-06-21
申请人： NEW JAPAN CHEM CO LTD
发明人： MASAMI HIROSHI , YOSHIDA YASUHISA
IPC分类号： C07D307/60 , C07B61/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing succinic anhydride in high efficiency and productivity while keeping the catalytic activity in hydrogenation reaction over a long period. SOLUTION: Succinic anhydride is produced by the catalytic hydrogenation of maleic anhydride by a fixed bed continuous reaction in a multitube reactor using a ruthenium-supporting formed catalyst as the hydrogenation catalyst. The hydrogenation reaction is carried out in a γ-butyrolactone solution.

8. 发明专利

JP2000001447A PRODUCTION OF CYCLOHEXANEDIMENTHANOL 失效
公开(公告)号：JP2000001447A
公开(公告)日：2000-01-07
申请号：JP16337798
申请日：1998-06-11
申请人： NEW JAPAN CHEM CO LTD
发明人： IWAMURA TAIICHIRO , YOSHIDA YASUHISA , ITO HIROSHI , NAKAZAWA MIKIRO
IPC分类号： B01J23/80 , C07B61/00 , C07C29/149 , C07C31/27
摘要： PROBLEM TO BE SOLVED: To provide an industrially practicable process for producing cyclohexanedimethanol by which the productivity is excellent with safety even in environmental aspects. SOLUTION: The hydrogenation is carried out in the presence of a copper- zinc-silica molded catalyst when hydrogenating a dialkyl cyclohexanedicarboxylate and producing cyclohexanedimethanol. In this case, the composition of the copper-zinc-silica molded catalyst is 10-800 pts.wt. of zinc oxide based on 100 pts.wt. of copper oxide and 1-300 pts.wt. of silica based on 100 pts.wt. of the copper oxide. The surface area of the copper-zinc-silica molded catalyst is 20-100 m2/g.

9. 发明专利

JPH08325196A PRODUCTION OF ALICYCLIC POLYCARBOXYLIC ACID AND ITS ACID ANHYDRIDE 失效
公开(公告)号：JPH08325196A
公开(公告)日：1996-12-10
申请号：JP15847195
申请日：1995-05-31
申请人： NEW JAPAN CHEM CO LTD
发明人： ITO MUNEAKI , YOSHIDA YASUHISA , ITO HIROSHI
IPC分类号： B01J23/44 , B01J23/46 , C07C27/02 , C07C51/09 , C07C51/56 , C07C61/09 , C07C61/12 , C07C62/12 , C07C62/24
摘要： PURPOSE: To industrially and advantageously obtain a carboxylic acid useful as a raw material, etc., of a solvent-soluble type polyimide in high purity and yield at a short time by carrying out hydrolysis of an alicyclic polycarboxylic ester in a specific solvent. CONSTITUTION: (A) compound of the formula, R OOC-A-COOR A is a group of formula I (X is a single bond, CO, O, etc.; R and R are each H or an alkyl) or a group of formula II [R to R are each H, CH3 or a group of COOR (R is R )]; R and R are each R ; on or more groups among R to R and one or more groups among R , R and R are each an alkyl} is hydrolyzed in (B) a water-soluble, aprotic and polar solvent [e.g. sulforane or dimethyl sulfoxide], having 120-350 deg.C boiling point, which is a good solvent for the component A and a poor solvent of an alicyclic polycarbonic ester which is a hydrolyzate of the component A to provide the objective compound of the formula, HOOC-B-COOH [B is a group of formula III or a group of formula IV (R to R are each H, CH3 or carboxyl].

10. 发明专利

JP2008143832A Method for producing alicyclic amine or saturated heterocyclic amine 审中-公开
标题翻译：生产水解胺或饱和杂环胺的方法
公开(公告)号：JP2008143832A
公开(公告)日：2008-06-26
申请号：JP2006332628
申请日：2006-12-08
申请人： New Japan Chem Co Ltd , 新日本理化株式会社
发明人： SOGABE KENSAKU , YOSHIDA YASUHISA , KOSHIYAMA TOMOKI
IPC分类号： C07C209/48 , C07B61/00 , C07C211/17 , C07C211/18 , C07C211/19 , C07C213/02 , C07C215/42 , C07D211/26 , C07D241/04 , C07D307/14
摘要： PROBLEM TO BE SOLVED: To provide a useful method for easily producing an alicyclic amine or a saturated heterocyclic amine in high yield. SOLUTION: The alicyclic amine or the saturated heterocyclic amine usable as a raw material or the like for a medicine can be produced in a high yield and industrially advantageously by carrying out the hydrogenation reaction of an aromatic nitrile or an unsaturated heterocyclic nitrile in the presence of a noble metal-based catalyst containing palladium and rhodium and/or ruthenium, and an amino alcohol. COPYRIGHT: (C)2008,JPO&INPIT

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