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1. 发明专利

JP2003081933A Method for producing sulfonated substance and method for producing surfactant 审中-公开
标题翻译：生产硫化物质的方法和生产表面活性剂的方法
公开(公告)号：JP2003081933A
公开(公告)日：2003-03-19
申请号：JP2001269565
申请日：2001-09-05
申请人： Lion Corp , ライオン株式会社
发明人： NISHIO HIROSHI , ISHIKAWA TSUTOMU , MIYAWAKI YOZO , TERAO TOSHIMI
IPC分类号： C07C303/06 , C07C305/10 , C07C309/30
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a sulfonated substance, with which the multi-product production of a sulfonated substance having an excellent color tone can simultaneously be carried out at a low cost, and to provide a method for producing a surfactant, using the sulfonated substance.
SOLUTION: In this method for producing the sulfonated substance, when gas containing SO
3 gas is branched from an SO
3 gas generation system through a branching route and introduced into a sulfonation reactor, the pressure difference (pressure before the branching-pressure under which the gas is introduced into the sulfonation reactor) of the gas containing SO
3 gas between pressure before the branching and pressure under which the gas is introduced into the sulfonation reactor is 0.005-0.04 MPa.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供一种生产磺化物质的方法，可以以低成本同时进行具有优异色调的多种产物的多产物生产，并提供一种制备表面活性剂的方法，使用磺化物质。解决方案：在制备磺化物质的方法中，当SO 3气体从SO 3气体发生系统通过分支路线分支并引入磺化反应器时，压力差（气体分支压力之前的压力引入到磺化反应器中）在分支压力之前的含有SO 3气体的气体和引入到磺化反应器中的压力之间的压力为0.005-0.04MPa。

2. 发明专利

JPS59139327A Sulfonation apparatus 失效
标题翻译：硫化装置
公开(公告)号：JPS59139327A
公开(公告)日：1984-08-10
申请号：JP1436183
申请日：1983-01-31
申请人： Lion Corp
发明人： TERAO TOSHIMI , KONDOU FUSAO , KIYAMA KENTAROU
IPC分类号： C07B45/02 , C07B31/00 , C07C67/00 , C07C301/00 , C07C303/00 , C07C303/06
摘要： PURPOSE: To carry out sulfonation reaction by placing a heating surface to evaporate the unreacted oil from the sulfonation product flowing on the surface in the form of a thin film, and a condensation surface to condense the evaporated unreacted oil, interposing the vapor of the sulfonation agent having reduced pressure between said surfaces.
CONSTITUTION: A heating medium is passed through the jackets 3, 4 of the outer tube 1, and cooling water is passed through the inner tube 2. The vapor of sulfonation agent (sulfuric anhydride) is transferred through the vapor path 21 under reduced pressure, and the reaction liquid containing unreacted oil and sent from other sulfonation apparatus is supplied through the feed pipe 15 and the slit nozzle 16 and flowed down along the heating surfaces 11, 12 in the form of thin film. The evaporated unreacted oil vapor is made to contact with the condensing surface 19, and the condensed oil is flowed down along the condensing surface. The oil is sulfonated with the vapor of the sulfonation agent, and taken out of the outlet part 17 together with the formerly sulfonated product flowing down along the heating surfaces 11, 12. The evaporated vapor of the reaction liquid is condensed in the mist collecting part 20.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过放置加热表面来蒸发来自在表面上以薄膜形式流动的磺化产物的未反应的油和冷凝表面的磺化反应，以冷凝蒸发的未反应的油，将磺化的蒸气所述表面之间的压力降低。构成：将加热介质通过外管1的夹套3,4，使冷却水通过内管2.通过减压蒸气路径21将磺化剂蒸气（硫酸酐）从其他磺化装置送出的含有未反应油的反应液通过供给管15和狭缝喷嘴16供给，并沿着加热面11,12以薄膜形式向下流动。使蒸发的未反应的油蒸气与冷凝表面19接触，并且冷凝的油沿冷凝表面向下流动。油与磺化剂的蒸气一起磺化，并与出口部分17一起从与加热面11,12向下流动的先前磺化产物一起取出。反应液体的蒸发蒸气在雾收集部分 20。

3. 发明专利

JPS63189407A PRODUCTION OF WATER-SOLUBLE POLYSTYRENESULFONIC ACID 失效
公开(公告)号：JPS63189407A
公开(公告)日：1988-08-05
申请号：JP1996387
申请日：1987-01-30
申请人： LION CORP
发明人： TERAO TOSHIMI , MIKUCHI FUMIHIRO , NAGANO KATSUMASA , IDE MASAYUKI
IPC分类号： C08F12/12 , C08F12/00
摘要： PURPOSE:To obtain the titled compound having high purity and low organic solvent content and to reutilize the solvent, by sulfonating a polystyrene in a halogenated hydrocarbon solvent and separating produced polystyrenesulfonic acid from the reaction mixture using a specific method. CONSTITUTION:A polystyrene having an average molecular weight of 200-50,000 is sulfonated in a halogenated hydrocarbon solvent (preferably methylene dichloride, etc.). The obtained sulfonation reaction product is stirred to disperse the polystyrenesulfonic acid to particles having an average diameter of 5-500mu and the particles are subjected to centrifugal separation under a condition to satisfy 1

4. 发明专利

JPS62249104A METHOD FOR TAKING OUT RAY OF SPECIFIC WAVELENGTH COMPONENT 失效
公开(公告)号：JPS62249104A
公开(公告)日：1987-10-30
申请号：JP9280886
申请日：1986-04-22
申请人： LION CORP
发明人： NAKAYA HIROSHI , TERAO TOSHIMI , MIKUCHI FUMIHIRO , MURAKOSHI TOMOAKI
IPC分类号： G01J3/12 , G02B5/22
摘要： PURPOSE:To efficiently utilize light by allowing the incidence of a beam into liquid in which specific pulverized semiconductor powder is dispersed, causing the oxidation-reduction of the liquid, etc., by a 1st light component, heating the liquid by a 3rd light component, taking out a 2nd light component to the outside and using the same. CONSTITUTION:The pulverized semiconductor powder (e.g.: CdS) having 30Angstrom -100mu grain size and 0.3-6.2eV energy band gap is dispersed at 10-100,000ppm concn. in the liquid. The semiconductor is excited by the 1st light having approximately =1,000nm is absorbed and is converted to heat energy. The 2nd light between 450-1,000nm is transmitted through a liquid vessel and is irradiated on living bodies, etc. so that said light is utilized as the energy source useful for the same. The entire wavelength region of the incident light is thereby effectively utilized.

5. 发明专利

JPH0582401B2 失效
公开(公告)号：JPH0582401B2
公开(公告)日：1993-11-18
申请号：JP9103885
申请日：1985-04-30
申请人： LION CORP
发明人： TERAO TOSHIMI , MIKUCHI FUMIHIRO , KITANO KYOZO , BANDAI HIROSHI
IPC分类号： C08F8/36

6. 发明专利

JPH0443904B2 失效
公开(公告)号：JPH0443904B2
公开(公告)日：1992-07-20
申请号：JP25652784
申请日：1984-12-06
申请人： LION CORP
发明人： MIKUCHI FUMIHIRO , TERAO TOSHIMI , KITANO KYOZO
IPC分类号： C07C309/20 , C07B63/00 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C303/42

7. 发明专利

JPS6033382B2 失效
公开(公告)号：JPS6033382B2
公开(公告)日：1985-08-02
申请号：JP8625279
申请日：1979-07-06
申请人： LION CORP
发明人： KONDO FUSAO , TERAO TOSHIMI , NAGANO KATSUMASA , KITANO KYOZO
IPC分类号： C07C309/30 , C07C67/00 , C07C301/00 , C07C303/06 , C07C309/31 , C07C309/37

8. 发明专利

JPS62250946A LIGHT ENERGY UTILIZING APPARATUS 失效
公开(公告)号：JPS62250946A
公开(公告)日：1987-10-31
申请号：JP9280986
申请日：1986-04-22
申请人： LION CORP
发明人： NAKAYA HIROSHI , MIKUCHI FUMIHIRO , TERAO TOSHIMI , MURAKOSHI TOMOAKI
IPC分类号： B01J19/12
摘要： PURPOSE:To enable the synthetic utilization of solar energy, by providing a first transparent plate made of material pervious to ultraviolet rays, visible light and infrared rays and a second flat plate made of a visible light pervious material opposed to said first plate so as to leave an interval therefrom. CONSTITUTION:Ultraviolet rays having a short wavelength and a high energy level and visible light near to said ultraviolet rays in solar rays 16 incident through a first flat plate 2 excite a semiconductive fine powder and activate the liquid in a container. When the liquid is water, water is decomposed, and hydrogen and oxygen generated are taken out to the outside from an energy take-out apparatus 14. Infrared rays having a long wavelength in sunrays are absorbed by a solvent to be converted to heat energy which is, in turn, taken out from the take-out apparatus 14. The remaining visible light transmits through a powdery semiconductive dispersion 6 and a second flat plate 4 to be taken out of the apparatus and irradiates upon organisms to be utilized as an energy source.

9. 发明专利

JPS62174205A SULFONATION OF POLYSTYRENE 失效
公开(公告)号：JPS62174205A
公开(公告)日：1987-07-31
申请号：JP2526986
申请日：1986-02-07
申请人： LION CORP
发明人： KITANO KYOZO , MIKUCHI FUMIHIRO , TERAO TOSHIMI
IPC分类号： C08F8/36
摘要： PURPOSE:To obtain a high-purity, water-soluble sulfonated polystyrene in high yields, by reacting polystyrene with a sulfonating agent under a specified shear strength in a halohydrocarbon solvent. CONSTITUTION:Polystyrene of an average MW of 200-50000 is sulfonated with a sulfonating agent in a halohydrocarbon solvent under the conditions in which an agitator which can meet the relationships: 0.1 ), and Q/V is the number of times of recirculation (I/min)] is used and the shearing force (N/cm falls within a range of 0.08-1.5. As the halohydrocarbon solvents used, 1-2 C aliphatic halohydrocarbons are desirable, and those inert to the sulfonating agent, such as methylene dichloride, carbon tatrachloride and chloroform, can be mentioned as examples.

10. 发明专利

JPS61134366A Oil separation from surface active agent 失效
标题翻译：表面活性剂的油分离
公开(公告)号：JPS61134366A
公开(公告)日：1986-06-21
申请号：JP25652784
申请日：1984-12-06
申请人： Lion Corp
发明人： MIKUCHI FUMIHIRO , TERAO TOSHIMI , KITANO KYOZO
IPC分类号： C07C309/20 , C07B63/00 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C303/42
摘要： PURPOSE: An alkane or alkene is added to separate unreacting olefin from the reaction mixture resulting from sulfonation of an olefin, neutralization and hydrolysis whereby the titled compound which is used as an active ingredient in detergents is obtained in high efficiency at low temperature.
CONSTITUTION: An olefin of 10W30C is sulfonated, neutralized and hydrolyzed and unreacting olefin is separated from the reaction mixture where an alkane or alkene of 8W27C less than that of the sulfonated olefin is added in an amount of 5W200pts.wt., per 100pts.wt. of the olefinsulfonate salt to effect separation into the aqueous phase containing the sulfonate salt and the oil phase containing the unreacting olefin. Since this process permits low conversion of sulfonation, it can be applied to the sulfonation of an inner olefin of low reactivity advantageously.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：加入烷烃或烯烃以从烯烃磺化得到的反应混合物中分离未反应的烯烃，中和和水解，从而在低温下以高效率获得用作洗涤剂中活性成分的标题化合物。构成：将10-30℃的烯烃磺化，中和并水解，从反应混合物中分离未反应的烯烃，其中加入少于磺化烯烃的烷烃或烯烃的量为5-200pts.wt 每100pts.wt。的烯烃磺酸盐进行分解成含有磺酸盐的水相和含有未反应烯烃的油相。由于该方法允许磺化的低转化率，所以可以有利地将其应用于低反应性的内烯烃的磺化。

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