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1. 发明专利

JPH0416196A PRODUCTION OF ALKYLGLYCOSIDE MONOESTER OF FATTY ACID 失效
公开(公告)号：JPH0416196A
公开(公告)日：1992-01-21
申请号：JP11632890
申请日：1990-05-02
申请人： LION CORP
发明人： MIYAKE HIROSHI , MORI TAKAO , TODA HARUHIKO , KITANO KYOZO
IPC分类号： C12P19/44 , C07H15/04
摘要： PURPOSE:To enable efficient obtaining of the subject monoester by reacting alkylglycosides of sugars selected from disaccharides, etc., and specific fatty acids with a neutral thermoduric immobilized hydrolase in an organic solvent. CONSTITUTION:(A) Alkylglycosides of sugars having 1-6C alkyl groups as an aglycone on hemiacetal (anomeric) hydroxyl groups of the sugars are obtained by selection from 5-7C monosacharides, such as ribose as disaccharides composed of hexoses. (B) Fatty acids such as caproic acid (methyl caproate) are then obtained by selection from 6-22C (un)saturated fatty acids and esters of the aforementioned fatty acids with 1-3C lower alcohols. (C) A neutral thermoduric immobilized hydrolase is subsequently obtained by immobilizing a porcine pancreatic lipase, etc., on active carbon, etc. To 1mol ingredient (B), is added 0.05-50mol ingredient (A). The ingredient (C) is then added so as to afford 0.1-10000 pts.wt. amount of the ingredient (C), based on 100 pts.wt. ingredient (B). Reaction is subsequently carried out in a solvent, such as tertiary butanol without containing water, at 50-120 deg.C for about 24hr, to produce the objective alkylglycoside of the fatty acids.

2. 发明专利

JPH03151885A PREPARATION OF POLYOL MONOFATTY ACID ESTER 失效
公开(公告)号：JPH03151885A
公开(公告)日：1991-06-28
申请号：JP29171989
申请日：1989-11-09
申请人： LION CORP
发明人： MORI NOBUHIRO , SASAMOTO HISASHI , AKAMATSU TAKU , IWASAKI RYOZO , KITANO KYOZO
IPC分类号： C12P7/64
摘要： PURPOSE:To improve the yield and content of the subject ester by treating a mixture of a glycerol fat and a specific polyol with a heat-resistant immobilized lipase in the presence of a secondary alcohol and/or a tertiary alcohol. CONSTITUTION:A heat-resistant immobilized lipase prepared by immobilizing the heat-resistant lipase having a protein content of 0.1-500mg per g of an immobilizing carrier and the remained activity of >=40% is packed in a column and the inlet and outlet of the column are filled with glass wool 3. A substrate solution 6 containing a secondary alcohol and/or a tertiary alcohol and a mixture comprising 1 mole of a glyceride oil containing 6-22C (un)saturated fatty acids as a constituting component and 0.2-20 moles of a polyol selected from (poly)glycerol and propylene glycol is fed into the column 1 through a pump 7 to subject to an ester exchange reaction.

3. 发明专利

JPH0212465B2 失效
公开(公告)号：JPH0212465B2
公开(公告)日：1990-03-20
申请号：JP23480282
申请日：1982-12-27
申请人： LION CORP
发明人： SEKIGUCHI SHIZUO , NAGANO KATSUMASA , KITANO KYOZO
IPC分类号： C07C309/17 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C309/20 , C07C309/22 , C07C309/62

4. 发明专利

JPH0210145B2 失效
公开(公告)号：JPH0210145B2
公开(公告)日：1990-03-06
申请号：JP13438482
申请日：1982-07-31
申请人： LION CORP
发明人： SEKIGUCHI SHIZUO , NAGANO KATSUMASA , KYAMA KENTARO , KITANO KYOZO
IPC分类号： C11D1/12 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/44 , C07C305/20 , C07C309/17

5. 发明专利

JPS62283948A PRODUCTION OF UNSATURATED FATTY ACID OR ESTERIFIED SUBSTANCE THEREOF 失效
公开(公告)号：JPS62283948A
公开(公告)日：1987-12-09
申请号：JP12521986
申请日：1986-05-30
申请人： LION CORP
发明人： OGOSHI TOSHIAKI , ANDO HIDEO , KITANO KYOZO
IPC分类号： C07C57/03 , C07C51/00 , C07C51/377 , C07C67/00 , C07C67/28 , C07C67/297 , C07C69/533
摘要： PURPOSE:To readily obtain an unsaturated fatty acid, by simply heating a sulfofatty acid or a salt and/or esterified substance thereof in a specific ethereal solvent, e.g. anisole, etc., to extremely selectively eliminate sulfone group without decarboxylation. CONSTITUTION:A sulfofatty acid having an 8-24C fatty acid, salt and/or esterified substance thereof, e.g. alpha-sulfolauric acid, etc., is heated in an ether, having 120-300 deg.C boiling point, and expressed by the formula (R1 and R2 are 1-15C alkyl, alkenyl, aryl or alkylaryl; A is 1-3C alkylene; n is 0-6), e.g. tetraethylene glycol dimethyl ether, etc., to eliminate the sulfonic acid or sulfonate group and afford the aimed unsaturated fatty acid or esterified substance thereof. EFFECT:The aimed unsaturated fatty acid can be produced in a large amount in high yield by a simple means.

6. 发明专利

JPS6232743B2 失效
公开(公告)号：JPS6232743B2
公开(公告)日：1987-07-16
申请号：JP9073080
申请日：1980-07-04
申请人： LION CORP
发明人： ANDO HIDEO , HAYASHI AKIRA , KITANO KYOZO
IPC分类号： C11D1/29 , B01F17/02 , B01F17/04 , C07C67/00 , C07C301/00 , C07C303/42 , C07C305/06 , C07C305/10

7. 发明专利

JPS6133019B2 失效
公开(公告)号：JPS6133019B2
公开(公告)日：1986-07-31
申请号：JP15424578
申请日：1978-12-15
申请人： LION CORP
发明人： SEKIGUCHI SHIZUO , TANO TETSUO , KITANO KYOZO , OOGOSHI TOSHIAKI
IPC分类号： C11D1/14 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C309/20

8. 发明专利

JPS61100556A Preparation of saturated/unsaturated-mixed-fatty acid ester sulfonate 失效
标题翻译：饱和/不饱和混合脂肪酸酯磺酸盐的制备
公开(公告)号：JPS61100556A
公开(公告)日：1986-05-19
申请号：JP22148084
申请日：1984-10-20
申请人： Lion Corp
发明人： KITANO KYOZO , SEKIGUCHI SHIZUO
IPC分类号： C07C309/62 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C309/17 , C07C309/20 , C11D1/28 , C11D11/04
CPC分类号： C07C309/00 , C11D1/28
摘要： PURPOSE: To obtain a compound useful as an active ingredient of an excellent detergent in high yield, by reacting a saturated/unsaturated fatty acid ester which absorbed a specific amount of SO
3 as a sulfonating agent, followed by neutralization.
CONSTITUTION: A saturated/unsaturated fatty acid ester is reacted with a saturated fatty acid, as a sulfonating agent, which absorbed SO
3 in an equimolar amount, preferably in a molar amount of 1.5W3.0 times that of said ester kept at ≥ the solidifying temperature and ≤150°C for 1W120min to obtain both a sulfonated product of saturated fatty acid and a sulfonated product of unsaturated fatty acid together. Then thus obtained sulfonated product is neutralized with an aqueous solution such as NaOH to obtain the aimed light-colored substance.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过使吸收了特定量的SO 3的饱和/不饱和脂肪酸酯作为磺化剂进行中和，得到高收率的作为优异洗涤剂的活性成分的化合物。构成：饱和/不饱和脂肪酸酯与作为磺化剂的饱和/不饱和脂肪酸反应，其以等摩尔量吸收SO 3，优选摩尔量为保持在≥=固化的所述酯的摩尔量的1.5-3.0倍温度和<= 150℃反应1-120分钟，得到饱和脂肪酸的磺化产物和不饱和脂肪酸的磺化产物。然后由此得到的磺化产物用NaOH水溶液中和，得到目标淡色物质。

9. 发明专利

JPH0377181B2 失效
公开(公告)号：JPH0377181B2
公开(公告)日：1991-12-09
申请号：JP24968983
申请日：1983-12-27
申请人： LION CORP
发明人： NAGANO KATSUMASA , SEKIGUCHI SHIZUO , KITANO KYOZO
IPC分类号： C07B63/04 , C07B31/00 , C07B63/00 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C303/42 , C07C309/17 , C07C309/22

10. 发明专利

JPH0376593A PRODUCTION OF SACCHARIDE MONO-FATTY ACID ESTER 失效
公开(公告)号：JPH0376593A
公开(公告)日：1991-04-02
申请号：JP21049589
申请日：1989-08-15
申请人： LION CORP
发明人： MIYAKE HIROSHI , KANDA MIDORI , TODA HARUHIKO , KITANO KYOZO
IPC分类号： C12P19/00 , C12P19/02 , C12P19/04 , C12P19/12
摘要： PURPOSE:To synthesize a saccharide mono-fatty acid ester in a short time in high synthetic attainment ratio by blending a specific fatty acid with a spe cific saccharide such as monosaccharide and carrying out enzymatic reaction using thermostable immobilized lipase in the presence of an organic solvent. CONSTITUTION:6-22C saturated fatty acid such as caproic acid, an unsaturated fatty acid or an ester such as methyl caproate of the fatty acid and 1-3C lower alcohol such as methanol is blended with a saccharide selected from 5-7C monosaccharide such as arabinose not containing a substituent group, disaccharide comprising a hexose such as aldose and 4-6C sugaralcohol such as erythritol and enzymatic reaction is carried out using thermostable lipase derived from immobilized Candida antarctica in the presence of an organic solvent such as benzene. Then, after the reaction is over, a saccharide mono- ratty acid ester is separated and collected from the reaction product by a conven tional procedure. Consequently, the saccharide mono-fatty acid ester is separated and collected from the reaction product can be synthesized in high synthetic attainment ratio, in high content, industrially and advantageously.

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