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1. 发明专利

JP2014214096A 新規な有機金属錯体およびアミン化合物の製造方法有权
标题翻译：生产新型有机复合物和胺化合物的方法
公开(公告)号：JP2014214096A
公开(公告)日：2014-11-17
申请号：JP2013090782
申请日：2013-04-23
申请人：関東化学株式会社 , Kanto Chem Co Inc
发明人： WATANABE MASATO , TAKEMOTO TOSHIHIDE , TANAKA KOICHI , MURATA KUNIHIKO
IPC分类号： C07F15/00 , B01J31/22 , C07C209/28 , C07C211/27 , C07C211/29 , C07C211/35 , C07C211/40 , C07C211/42 , C07C213/02 , C07C215/08 , C07C217/60 , C07C227/08 , C07C227/32 , C07C229/14 , C07C253/30 , C07C255/58 , C07D213/38 , C07D213/42 , C07D217/14 , C07D277/28
CPC分类号： C07F17/02 , B01J31/1815 , B01J31/183 , B01J31/22 , B01J31/2295 , B01J2231/64 , B01J2531/822 , B01J2531/827 , C07B43/04 , C07B2200/07 , C07C209/28 , C07C211/27 , C07C211/29 , C07C211/35 , C07C211/40 , C07C211/42 , C07C213/02 , C07C213/08 , C07C215/08 , C07C217/60 , C07C227/08 , C07C227/32 , C07C229/14 , C07C253/30 , C07C255/58 , C07C2601/14 , C07C2602/08 , C07C2602/10 , C07D209/48 , C07D213/38 , C07D213/42 , C07D217/14 , C07D277/28 , C07F15/0033 , C07C229/08
摘要：【課題】一般性が高く、高活性で、官能基選択性に優れた触媒として利用可能な、新規有機金属化合物の提供。【解決手段】下記一般式(1)で表される、還元的アミノ化反応を触媒する、新規有機金属化合物。【選択図】なし
摘要翻译：要解决的问题：提供可用作具有高通用性，高活性和优异的官能团选择性的催化剂的新型有机金属化合物。本发明涉及由特定通式（1）表示的新型有机金属化合物，催化还原胺化反应。

2. 发明专利

JP2010235604A Novel organometallic complex and process for preparing amine compound 有权
标题翻译：新型有机复合物和制备胺化合物的方法
公开(公告)号：JP2010235604A
公开(公告)日：2010-10-21
申请号：JP2010054359
申请日：2010-03-11
申请人： Kanto Chem Co Inc , 関東化学株式会社
发明人： WATANABE MASATO , HORI JUNICHI , MURATA KUNIHIKO , MIKI TAKASHI
IPC分类号： C07D213/81 , B01J31/22 , C07B61/00 , C07C209/28 , C07C211/27 , C07C211/29 , C07C211/35 , C07C255/58 , C07D215/30 , C07D217/26 , C07D241/24 , C07F15/00
CPC分类号： B01J31/2295 , C07C209/78 , C07F15/004 , C07F15/0053 , C07F15/008
摘要： PROBLEM TO BE SOLVED: To provide a novel organometallic compound usable as a catalyst having high generality and high activity, and excellent selectivity of a functional group. SOLUTION: The novel organometallic compound expressed by formula (1) catalyzes reductive amination. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供可用作具有高通用性和高活性的催化剂的新型有机金属化合物，以及官能团的优异的选择性。解决方案：由式（1）表示的新型有机金属化合物催化还原胺化。版权所有（C）2011，JPO＆INPIT

3. 发明专利

JP2008088090A Manufacturing method of optically active quinuclidinols having substituent group at 2-position 有权
标题翻译：具有二位置取代基的光学活性喹啉醇的制备方法
公开(公告)号：JP2008088090A
公开(公告)日：2008-04-17
申请号：JP2006269642
申请日：2006-09-29
申请人： Kanto Chem Co Inc , 関東化学株式会社
发明人： KATAYAMA TAKEAKI , MURATA KUNIHIKO
IPC分类号： C07D453/02 , B01J31/22 , C07B53/00 , C07B61/00
CPC分类号： C07D453/02
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method of optically active 3-quinuclidinols having a substituent group at the 2-position, particularly optically active cis-3-quinuclidinols having a substituent group at the 2-position useful as an optically active and physiologically active compound utilized for pharmaceuticals, agrochemicals and the like or as a synthetic intermediate of liquid crystal materials and the like.
SOLUTION: The manufacturing method of the optically active 3-quinuclidinols having a substituent group at the 2-position comprises causing 3-quinuclidinones having a substituent group at the 2-position to react with a hydrogen-donating compound in the presence of a predetermined metal complex.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供在2位具有取代基的光学活性3-奎宁环醇的制造方法，特别是在2-位具有取代基的光学活性顺式-3-奎宁环醇，其可用作光学用于药物，农业化学品等的活性和生理活性化合物或作为液晶材料的合成中间体等。解决方案：在2位具有取代基的光学活性3-奎宁环醇的制备方法包括在2-位上具有取代基的3-奎宁环醌与供氢化合物在存在下反应预定的金属络合物。版权所有（C）2008，JPO＆INPIT

4. 发明专利

JP2008088089A Manufacturing method of optically active quinuclidinols having substituent group at 2-position 有权
标题翻译：具有二位置取代基的光学活性喹啉醇的制备方法
公开(公告)号：JP2008088089A
公开(公告)日：2008-04-17
申请号：JP2006269610
申请日：2006-09-29
申请人： Kanto Chem Co Inc , 関東化学株式会社
发明人： KATAYAMA TAKEAKI , MURATA KUNIHIKO
IPC分类号： C07D453/02 , B01J31/22 , C07B61/00
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide an efficient manufacturing method of optically active quinuclidinols having a substituent group at the 2-position which have been heretofore prepared only by an optical resolution method. SOLUTION: The manufacturing method of the optically active 3-quinuclidinols having a substituent group at the 2-position comprises causing 3-quinuclidinones having a substituent group at the 2-position to react with hydrogen in the presence of a predetermined ruthenium complex and a base. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：为了提供迄今为止仅通过光学拆分方法制备的在2-位具有取代基的光学活性奎宁环醇的有效制备方法。解决方案：在2位具有取代基的光学活性3-奎宁环醇的制备方法包括在预定的钌络合物的存在下，使2-位具有取代基的3-奎宁环酮与氢反应和一个基地。版权所有（C）2008，JPO＆INPIT

5. 发明专利

JP2012006888A Method for producing aliphatic optically-active fluoroalcohol 有权
标题翻译：生产水性光活性氟代醇的方法
公开(公告)号：JP2012006888A
公开(公告)日：2012-01-12
申请号：JP2010146219
申请日：2010-06-28
申请人： Kanto Chem Co Inc , 関東化学株式会社
发明人： KATAYAMA TAKEAKI , TAKEMOTO TOSHIHIDE , MURATA KUNIHIKO
IPC分类号： C07C29/143 , C07B53/00 , C07B61/00 , C07C29/80 , C07C31/38
CPC分类号： C07C29/143 , C07B2200/07 , C07C31/38
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently synthesizing a lower aliphatic optically-active fluoroalcohol that has difficulty in separation from a solvent, without using a special reaction vessel.SOLUTION: In this method for producing an aliphatic optically-active alcohol having a fluorine atom at α position, the optically-active alcohol is produced by reacting an aliphatic ketone having a fluorine atom at α position in water using a formate, under the presence of an asymmetric catalyst represented by general formula (1) and an acid.
摘要翻译：要解决的问题：提供一种高效合成难以与溶剂分离的低级脂族光学活性氟代醇的方法，而不使用特殊的反应容器。解决方案：在这种制备在α位具有氟原子的脂肪族光学活性醇的方法中，光学活性醇是通过在甲酸中的α位置上具有氟原子的脂肪族酮在甲酸中反应制备的，存在由通式（1）表示的不对称催化剂和酸。版权所有（C）2012，JPO＆INPIT

6. 发明专利

JP2010285443A Method for producing optically active alcohol 有权
标题翻译：用于生产光学活性醇的方法
公开(公告)号：JP2010285443A
公开(公告)日：2010-12-24
申请号：JP2010167292
申请日：2010-07-26
申请人： Kanto Chem Co Inc , Nagoya Industrial Science Research Inst , 財団法人名古屋産業科学研究所 , 関東化学株式会社
发明人： NOYORI RYOJI , OKUMA TAKESHI , TSUTSUMI KUNIHIKO , UCHIUMI NORIYUKI , MURATA KUNIHIKO
IPC分类号： C07C29/145 , B01J31/22 , C07B53/00 , C07B61/00 , C07C33/30 , C07C33/46 , C07C35/32 , C07D311/22 , C07D495/04
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method of production by which an optically active alcohol can highly stereoselectively be obtained in good yield from a ketone compound that has heretofore been difficult to hydrogenate. SOLUTION: A ruthenium complex RuCl[(S,S)-TsDPEN](p-cymene) represented by formula and the ketone compound are introduced into a polar solvent, and mixed under pressurized hydrogen to thereby hydrogenate the ketone compound, to produce an optically active alcohol. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种通过以往难以氢化的酮化合物以良好的收率高度立体选择地获得光学活性醇的制造方法。解决方案：将由式表示的钌络合物RuCl [（S，S）-TsDPEN]（对甲基异丙基苯）和酮化合物引入极性溶剂中，并在加压氢气下混合，从而将酮化合物氢化成产生光学活性的醇。版权所有（C）2011，JPO＆INPIT

7. 发明专利

JP2005263662A Method for producing optically active alcohol having nitrogen-containing heterocyclic ring 有权
标题翻译：生产具有含氮杂环化合物的光学活性醇的方法
公开(公告)号：JP2005263662A
公开(公告)日：2005-09-29
申请号：JP2004076676
申请日：2004-03-17
申请人： Kanto Chem Co Inc , 関東化学株式会社
发明人： KATAYAMA TAKEAKI , MURATA KUNIHIKO
IPC分类号： C07D211/14 , C07D401/04
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently producing an optically active alcohol having a nitrogen-containing heterocyclic ring, by conducting reduction of a nitrogen-containing heteroaromatic ring and a carbonyl group in a ketone compound having a nitrogen-containing heteroaromatic salt with a single catalyst in one pot. SOLUTION: This method for producing the optically active alcohol having the nitrogen-containing heterocyclic ring expressed by general formula (C) and/or general formula (D) comprises reacting a ketone compound having the nitrogen-containing heteroaromatic salt expressed by general formula (A) with an asymmetric metal complex obtained by acting an optically active nitrogen-containing compound expressed by general formula (B) on a compound of a metal belonging to the group VIII of the periodic table, together with a hydrogen donor. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：解决的问题：提供一种有效制备含氮杂环的光学活性醇的方法，通过在具有含氮杂环的酮化合物中还原含氮杂芳环和羰基一个单一催化剂的杂芳香盐。解决方案：用于制备具有由通式（C）和/或通式（D）表示的含氮杂环的光学活性醇的方法包括使具有由一般表示的含氮杂芳族盐的酮化合物式（A）与通过式（B）表示的光学活性含氮化合物与属于元素周期表第Ⅷ族的金属化合物一起获得的不对称金属络合物与氢供体一起使用。版权所有（C）2005，JPO＆NCIPI

8. 发明专利

JP2004269481A Method for production of optically active compound 有权
公开(公告)号：JP2004269481A
公开(公告)日：2004-09-30
申请号：JP2003071368
申请日：2003-03-17
申请人： Kanto Chem Co Inc , 関東化学株式会社
发明人： WATANABE MASATO , MURATA KUNIHIKO , IKARIYA TAKAO
IPC分类号： B01J31/22 , C07B53/00 , C07B61/00 , C07C67/347 , C07C69/716
CPC分类号： C07C67/347 , B01J31/1805 , B01J2231/348 , B01J2531/821 , B01J2540/34 , C07B2200/07 , C07C2601/08 , C07C2601/14 , C07C2601/18 , C07C69/716
摘要： PROBLEM TO BE SOLVED: To provide an optically active compound having high optical purity obtained by a reaction using an asymmetrical metal complex as a catalyst. SOLUTION: The optically active compound having high optical purity can be obtained in a high yield by an asymmetric reaction using, as a catalyst, a transition metal complex having a nitrogen-containing optically active compound as an asymmetric ligand. COPYRIGHT: (C)2004,JPO&NCIPI

9. 发明专利

JP2011051929A Method for producing optically active alcohol having aromatic heterocycle 有权
标题翻译：生产具有芳香杂环的光学活性醇的方法
公开(公告)号：JP2011051929A
公开(公告)日：2011-03-17
申请号：JP2009201953
申请日：2009-09-01
申请人： Kanto Chem Co Inc , 関東化学株式会社
发明人： SHIBATA KAZUFUMI , TSUTSUMI KUNIHIKO , KATAYAMA TAKEAKI , MURATA KUNIHIKO , YOSHIDA MASAHIKO
IPC分类号： C07D213/30 , C07B61/00
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently synthesizing an optically active alcohol with high optical purity which has an aromatic hydrocarbon group and a heterocycle in producing an optically active alcohol expected as an intermediate for synthesizing a drug and various intermediates of agricultural chemicals and the like. SOLUTION: The method for producing the optically active alcohol comprises reacting a carbonyl compound having an aromatic hydrocarbon group and a heterocycle with a hydrogen source in the presence of a catalyst including a ruthenium complex having an optically active diphosphine compound having asymmetry on carbon and a certain specific diamine compound as ligands to efficiently synthesize the optically active alcohol having high optical purity. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种有效合成具有高光学纯度的光学活性醇的方法，其具有芳族烃基和杂环，以制备预期作为合成药物的中间体的光学活性醇和各种中间体农药等。解决方案：制备光学活性醇的方法包括在催化剂存在下使具有芳族烃基和杂环的羰基化合物与氢源反应，所述催化剂包括具有对碳不对称的光学活性二膦化合物的钌络合物和一些特定的二胺化合物作为有效合成具有高光学纯度的光学活性醇的配体。版权所有（C）2011，JPO＆INPIT

10. 发明专利

JP2007283302A Catalyst composition 有权
标题翻译：催化剂组合物
公开(公告)号：JP2007283302A
公开(公告)日：2007-11-01
申请号：JP2007165566
申请日：2007-06-22
申请人： Japan Science & Technology Agency , Jfe Steel Kk , Jfeスチール株式会社 , Kanto Chem Co Inc , Nippon Soda Co Ltd , Takasago Internatl Corp , Takeda Chem Ind Ltd , 日本曹達株式会社 , 武田薬品工業株式会社 , 独立行政法人科学技術振興機構 , 関東化学株式会社 , 高砂香料工業株式会社
发明人： IKARIYA TAKAO , IKEHIRA HIDEYUKI , MURATA KUNIHIKO , KIYOFUJI NOBUO , OOOKA HIROHITO , HASHIGUCHI SHOHEI , OKUMA TAKESHI , NOYORI RYOJI
IPC分类号： B01J31/22
摘要： PROBLEM TO BE SOLVED: To provide a catalyst composition for obtaining an optically-active alcohol compound in a high yield and a high selectivity.
SOLUTION: The catalyst composition is composed of a ruthenium complex represented by general formula (1) (wherein, X and Y each represent a hydrogen atom, halogen atom, carboxyl group, or other anion group, R
1 , R
2 , and R
3 each represent a hydrocarbon group which may have a substituent, both the R
1 and the R
2 may form a carbon chain ring which may have a substituent, n is an integer of 1 to 4, R
6 , R
7 , and R
8 each represent a hydrocarbon group which may have a hydrogen atom or a substituent, m is an integer of 1 to 4, and both of PR
1 R
2 R
3 and NR
6 R
7 R
8 are an optically-active group).
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供以高产率和高选择性获得光学活性醇化合物的催化剂组合物。解决方案：催化剂组合物由通式（1）表示的钌络合物（其中X和Y各自表示氢原子，卤素原子，羧基或其它阴离子基团，R 1， / SP>，R 2 和R 3 各自表示可以具有取代基的烃基，R 1 SP> 2可以形成可以具有取代基的碳链环，n为1〜4的整数，R SP 6，R SP 7，和R 各自表示可以具有氢原子或取代基的烃基，m为1〜4的整数，PR 1 2 < / SP> R 3 和NR 6 R 7 R 8 是光学活性基团）。版权所有（C）2008，JPO＆INPIT

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