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1. 发明专利

JPS59116272A Imidazole derivative and agricultural and hotricultural fungicide 失效
标题翻译：咪唑衍生物和农业和农村化学品
公开(公告)号：JPS59116272A
公开(公告)日：1984-07-05
申请号：JP22489682
申请日：1982-12-23
申请人： Hokko Chem Ind Co Ltd
发明人： OOYAMA HIROSHI , MORITA TAKESHI , OONO TOSHIJI , WADA TAKUO
IPC分类号： C07D233/61 , A01N43/50
摘要： NEW MATERIAL:The imidazole derivative of formula I (R
1 is lower alkyl; R
2 is R
1 or lower alkenyl) or its salt.
EXAMPLE: 1-[N-(2-Chloro-4-fluorophenyl)-2-ethoxypropaneimidoyl]-imidazole.
USE: An agricultural or horticultural fungicide or seed disinfectant. It has broad fungicidal activity, and exhibits excellent controlling effect against various plant blights, especially rust and powdery mildew of wheat, helminthosporium leaf spot of rice, bean, etc., blast of rice, mildew of cucumber, water melon, etc. at a low rate of application. It is harmless to useful crops, and free from toxicity to man, animal and fish, and can be used safely.
PROCESS: The compound of formula I can be prepared by reacting the compound of formula II (X is halogen) with imidazole of formula III preferably in an or ganic solvent, if necessary in the presence of an acid acceptor such as triethylamine, under ice cooling at 0W100°C for ≤1hr.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：式Ⅰ咪唑衍生物（R1为低级烷基; R2为R1或低级链烯基）或其盐。实施例：1- [N-（2-氯-4-氟苯基）-2- ethoxypropaneimidoyl] - 咪唑。用途：农业或园艺杀菌剂或种子消毒剂。具有广泛的杀菌活性，对各种植物枯萎病，特别是小麦锈病和白粉病，水稻，豆类等等的杀虫剂，水稻，黄瓜，西瓜等霉菌的防治效果优异。使用率低。有用的作物无害，对人，动物和鱼类无毒，可安全使用。方法：式I化合物可以通过使式II化合物（X为卤素）与式III咪唑在惰性溶剂中反应，如果需要，在酸受体如三乙胺存在下，在冰冷却下在0-100℃下<= 1小时。

2. 发明专利

JPS59122473A Imidazole derivative and agricultural and horticultural fungicide 失效
标题翻译：咪唑衍生物和农业和农业化学品
公开(公告)号：JPS59122473A
公开(公告)日：1984-07-14
申请号：JP23056782
申请日：1982-12-29
申请人： Hokko Chem Ind Co Ltd
发明人： OOYAMA HIROSHI , MORITA TAKESHI , OONO TOSHIJI , WADA TAKUO
IPC分类号： C07D233/61 , A01N43/50
摘要： NEW MATERIAL:The compound of formula I (A is lower alkylene; R is lower alkynyl, cycloalkyl, cycloalkylalkyl, lower saturated alkyl or lower unsaturated alkyl which is interrupted by O or S, cyanoalkyl or arylalkyl) and its salt.
EXAMPLE: 1-[N-(2-chloro-4-fluorophenyl)-2-propargyloxyethanimidoyl]imidazole.
USE: An agricultural and horticultural fungicide having little phtotoxicity to useful crops and harmless to man and animal.
PROCESS: The compound of formula I can be prepared by reacting the compound of formula II (X is halogen) with imidazole and an amophoteric substance (e.g. alkali metal salt, inorganic acid salt, organic acid salt, metal complex salt, etc.) in an organic solvent at 0W85°C, optionally in the presence of an acid acceptor.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：式I化合物（A为低级亚烷基; R为低级炔基，环烷基，环烷基烷基，低级饱和烷基或被O或S间隔的低级不饱和烷基，氰基烷基或芳基烷基）及其盐。实施例：1- [N-（2-氯-4-氟苯基）-2-丙酰氧基乙亚氨基]咪唑。用途：农用和园艺杀菌剂对有用作物几乎没有毒性，对人类和动物无害。方法：式I化合物可以通过使式II化合物（X为卤素）与咪唑和amophoteric物质（例如碱金属盐，无机酸盐，有机酸盐，金属络盐等）反应来制备 0-85℃的有机溶剂，任选在酸受体存在下进行。

3. 发明专利

JPS59116271A Imidazole derivative and agricultural and horticultural fungicide 失效
标题翻译：咪唑衍生物和农业和农业化学品
公开(公告)号：JPS59116271A
公开(公告)日：1984-07-05
申请号：JP22489582
申请日：1982-12-23
申请人： Hokko Chem Ind Co Ltd
发明人： OOYAMA HIROSHI , MORITA TAKESHI , OONO TOSHIJI , WADA TAKUO
IPC分类号： C07D233/61 , A01N43/50
摘要： NEW MATERIAL:The imidazole derivative of formula I (R is lower alkyl or lower alkenyl) or its salt.
EXAMPLE: 1-[N-(2-Chloro-4-fluorophenyl)-2-n-propyloxyethaneimidoyl]-imidazole.
USE: An agricultural or horticultural fungicide or seed disinfectant. It has broad fungicidal activity, and exhibits excellent controlling effect against various plant blights, especially rust and powdery mildew of wheat, helminthosporium leaf spot of rice, bean, etc., blast of rice, mildew of cucumber, water melon, etc. at a low rate of application. It is harmless to useful crops, and free from toxicity to man, animal and fish, and can be used safely.
PROCESS: The compound of formula I can be prepared by reacting the compound of formula II (X is halogen) with imidazole of formula III preferably in an organic solvent, if necessary in the presence of an acid acceptor such as triethylamine, under ice cooling at 0W100°C for ≤1hr.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：式I的咪唑衍生物（R是低级烷基或低级烯基）或其盐。实施例：1- [N-（2-氯-4-氟苯基）-2-正丙氧基亚氨基] - 咪唑。用途：农业或园艺杀菌剂或种子消毒剂。具有广泛的杀菌活性，对各种植物枯萎病，特别是小麦锈病和白粉病，水稻，豆类等的防治，防治黄瓜，黄瓜，水瓜等的防治效果显着。使用率低。有用的作物无害，对人，动物和鱼类无毒，可安全使用。方法：式I化合物可以通过使式II的化合物（X为卤素）与式III的咪唑优选在有机溶剂中反应，如果需要，在酸受体如三乙胺的存在下，在冰冷却下， 0-100℃，<= 1小时。

4. 发明专利

JPS59116273A Imidazole derivative and agricultural and horticultural fungicide 失效
标题翻译：咪唑衍生物和农业和农业化学品
公开(公告)号：JPS59116273A
公开(公告)日：1984-07-05
申请号：JP22489782
申请日：1982-12-23
申请人： Hokko Chem Ind Co Ltd
发明人： OOYAMA HIROSHI , MORITA TAKESHI , OONO TOSHIJI , WADA TAKUO
IPC分类号： C07D233/61 , A01N43/50
摘要： NEW MATERIAL:The compound of formula 1 (A is straight or branched chain lower alkylene; R is saturated or unsaturated lower alkyl which may be interrupted with O or S, cyanoalkyl, cycloalkyl, benzyl, halobenzyl, or phenyl; n is 0, 1 or 2) and its salt.
EXAMPLE: 1-[N-(2-Chloro-4-fluorophenyl)-2-n-propylthioethaneimidoyl]-imidazole.
USE: An agricultural and horticultural fungicide free from phytotoxicity and harmless to man and animal.
PROCESS: The compound of formula 1 can be prepared by reacting the compound of formula 2 with the compound of formula 3 preferably in an organic solvent such as benzene, chloroform, etc., if necessary in the presence of an acid acceptor, at 0W85°C.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：式1化合物（A为直链或支链低级亚烷基; R为可被O或S间隔的饱和或不饱和低级烷基，氰基烷基，环烷基，苄基，卤代苄基或苯基; n为0,1 或2）及其盐。实施例：1- [N-（2-氯-4-氟苯基）-2-正丙硫基亚氨代] - 咪唑。用途：无植物毒性的农业和园艺杀菌剂，对人类和动物无害。方法：式1的化合物可以通过使式2的化合物与式3的化合物在需要时在酸受体的存在下，在有机溶剂如苯，氯仿等中反应来制备， 85摄氏度

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