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1. 发明专利

JP2003140287A SILVER HALIDE EMULSION AND SILVER HALIDE PHOTOGRAPHIC SENSITIVE MATERIAL 审中-公开
公开(公告)号：JP2003140287A
公开(公告)日：2003-05-14
申请号：JP2002188536
申请日：2002-06-27
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMADA KOZABURO , MAEDA HIDEKI , ASANUMA NAOKI
IPC分类号： G03C1/28 , G03C1/08 , G03C1/34 , G03C1/42
摘要： PROBLEM TO BE SOLVED: To provide a silver halide photographic sensitive material in which the photographic sensitivity of the photographic emulsion is increased while a fog accompanying the high sensitivity is suppressed, and increase in the fog is suppressed even when the material is stored under severe conditions such as high temperature, high humidity and an environment exposed to harmful gas produced during combustion such as exhaust gas from an automobile or the like. SOLUTION: The silver halide emulsion containing a compound in which an oxidized part with one electron by oxidation with one electron is successively subjected to processes of forming bonds and further emits one or more electrons, is characterized in that the silver halide photographic sensitive material contains the above emulsion.

2. 发明专利

JP2003114488A SILVER HALIDE EMULSION AND SILVER HALIDE PHOTOGRAPHIC SENSITIVE MATERIAL 审中-公开
公开(公告)号：JP2003114488A
公开(公告)日：2003-04-18
申请号：JP2002192374
申请日：2002-07-01
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMADA KOZABURO , MAEDA HIDEKI , ASANUMA NAOKI
IPC分类号： G03C1/08
摘要： PROBLEM TO BE SOLVED: To provide a silver halide photographic sensitive material which suppresses a fogging due to enhanced sensitivity while enhancing photographic sensitivity and is less liable to increase the fogging even when stored at a high temperature and a high humidity and under such severe conditions that it is exposed to harmful gas produced in combustion, such as automobile exhaust gas. SOLUTION: A silver halide emulsion containing one or more of the compounds of formulae (1)-(3) is provided. In the formula (1), Z1 is an atomic group capable of forming a 6-membered ring together with N and two C atoms of the benzene ring; R1 , R2 and RN1 are each H or a substituent; X1 is a substituent; m1 is an integer of 0-3; and L1 is a releasable group. In the formula (2), ED11 is an electron donative group; R11 , R12 , RN11 , R13 and R14 are each H or a substituent; X11 is a substituent; m11 is an integer of 0-3; L11 is a releasable group; and RN11 , R13 , R14 , X11 and ED11 may bond to each other to form a cyclic structure. In the formula (3), R22 , R23 , R21 , RN21 , Ra and Rb are each H or a substituent and L21 is a releasable group, but when RN21 is a group other then aryl, Ra and Rb bond to each other to form an aromatic ring.

3. 发明专利

JP2002003465A METHOD FOR PRODUCING SULFONIC ACID HALIDE COMPOUND 失效
公开(公告)号：JP2002003465A
公开(公告)日：2002-01-09
申请号：JP2000188371
申请日：2000-06-22
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMAKAWA KAZUYOSHI , ASANUMA NAOKI , MOTOKI MASUSHI
IPC分类号： C07C303/02 , C07C309/88
摘要： PROBLEM TO BE SOLVED: To provide a new method for producing a sulfonic acid halide compound containing a hydroxyl group in the molecule by a short process in a high yield. SOLUTION: This method for producing a sulfonic acid halide compound containing a hydroxyl group in the molecule comprises reacting an alkali metal salt of a sulfonic acid compound containing a hydroxyl group in the molecule with an ammonium salt and then reacting the reaction product with a halogenating agent.

4. 发明专利

JP2001264912A SILVER HALIDE PHOTOGRAPHIC EMULSION, METHOD FOR PREPARING THE SAME AND SILVER HALIDE PHOTOGRAPHIC SENSITIVE MATERIAL USING THE SAME 失效
公开(公告)号：JP2001264912A
公开(公告)日：2001-09-28
申请号：JP2000078281
申请日：2000-03-21
申请人： FUJI PHOTO FILM CO LTD
发明人： ASANUMA NAOKI
IPC分类号： G03C1/035 , G03C1/015 , G03C1/047
摘要： PROBLEM TO BE SOLVED: To provide a thin flat platy grain emulsion further excellent in sensitivity to color sensitization, a method for preparing the emulsion and a silver halide photographic sensitive material using the emulsion. SOLUTION: The silver halide photographic emulsion has =50% of the total projected area is occupied by flat platy grains which satisfy the following requirements (i)-(vi); (i) silver iodobromide or silver iodochlorobromide grains having (111) faces as the principal surfaces, (ii) >=1.0 μm equivalent circular diameter and =10 dislocation lines ranging from the interface between the shell and the core to the edge of the grain, (iv) when each of the flat platy grains is seen from a direction perpendicular to the principal surfaces, the shell forming region is a circular region corresponding to >=10% of the length from a side of the grain to the center, (v) when the average silver iodide content of the grains is represented by I mol% (0.3 =0.5 μm equivalent spherical diameter.

5. 发明专利

JP2000327940A AZOMETHINE COMPOUND AND OILY MAGENTA INK 失效
公开(公告)号：JP2000327940A
公开(公告)日：2000-11-28
申请号：JP2000024454
申请日：2000-02-01
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMAKAWA KAZUYOSHI , MOTOKI MASUSHI , ASANUMA NAOKI , SUZUKI AKIRA , SATO TADAHISA , MIKOSHIBA TAKASHI
IPC分类号： B41J2/01 , B41M5/00 , C09B55/00 , C09D11/00 , C09D11/328 , C09D11/36
摘要： PROBLEM TO BE SOLVED: To obtain a new compound of an oily dye, excellent in color reproductivity, preservability and solubility and useful for preparation of a magenta ink for an ink jet printing method. SOLUTION: This azomethine compound is represented by formula I [R1 is a 1-16C alkyl; R2 is a halogen, a 1-20C alkyl or the like; R3 is a 1-30C alkylene or the like; R4 is a 1-16C alkyl; L1 is a 1-30C alkylene or the like; L2 is CO-NH group or the like; X is cyano or the like; Y is H, a halogen or the like; m is 1-4; n is 1-18; p is 0-4; the number of the carbon atoms of R1, L1, L2, R3 and R4 totals 20-50] e.g. a compound of formula II. The compound of the formula I is obtained by reacting an azole-based compound of formula III, e.g. 2-[4- 3-(tetradecyloxycarbonyl)propanoylamino}phenyl]-6-tert-butyl-7- chloropyrazolo[1,5-b][1,2,4]triazol, with a p-phenylenediamine-based compound of formula IV under an oxidative condition.

6. 发明专利

JPH10339931A HEAT DEVELOPABLE PHOTOGRAPHIC MATERIAL 失效
公开(公告)号：JPH10339931A
公开(公告)日：1998-12-22
申请号：JP16499097
申请日：1997-06-06
申请人： FUJI PHOTO FILM CO LTD
发明人： ASANUMA NAOKI , ISHIZAKA TATSUYA
IPC分类号： G03C1/498 , B41M5/337
摘要： PROBLEM TO BE SOLVED: To obtain the heat-developable photographic material small in deterioration of image density due to storage left in an unexposed state and superior in image storage stability even under conditions of being exposed to light and heat by incorporating a reducible silver salt, a reducing agent, a binder, a specified compound, and a specified organic acid compound. SOLUTION: This heat developable photographic mateal contains the reducible silver salt, the reducing agent, the binder, and at least one kind of compound represented by formula I and the organic acid compound represented buy formula II. In formula I, R is a univalent substituting; and (m) is 1, 2, 3, or 4, and when (m) is >=2, plural G may be same or different, and when plural G are adjacent, they may combine with each other to form an aliphatic or aromatic or hetero ring. In formula II, A is a mono- or poly-cyclic aromatic ring; Y is a -COOH or -SO2 H or -SO3 H group; and (n) is 1 or 2, thus permitting the obtained heat developable photographic material to be high in image density and freed of deterioration image density by raw stock storage and superior in image storage stability.

7. 发明专利

JPH09258367A NOVEL POLYHALOMETHANE COMPOUND AND PHOTOSENSITIVE MATERIAL 失效
公开(公告)号：JPH09258367A
公开(公告)日：1997-10-03
申请号：JP7058196
申请日：1996-03-26
申请人： FUJI PHOTO FILM CO LTD
发明人： ASANUMA NAOKI , OKADA HISASHI , TOTANI ICHIZO
IPC分类号： G03C1/498
摘要： PROBLEM TO BE SOLVED: To enhance the storage stability of the photosensitive material and that of an image without deteriorating sensitivity and color ones by incorporating a specified polyhalomethane compound. SOLUTION: This photosensitive material contains the polyhalo-methane compound represented by the formula in which Q is an aryl group: each of Z1 and Z2 is a halogen atom; Y is -C(=O)-, -SO-, or -SO2 -; (k) is 0 or 1; W is an electron withdrawing group; (m) is an integer of 2-7; and A is an H atom or an electron withdrawing group. This compound can be added either to a photosensitive layer or a nonphotosensitive layer, but preferably, to photosensitive layer. It is added in an amount of 1×10 -1mol/mol of silver halide, preferably, 1×10 -3×10 mol/mol of silver halide, but it varies as the case may be, and it is preferred to add it by dissolving it in an organic solvent in all the case.

8. 发明专利

JP2004245929A Silver halide emulsion and silver halide photographic sensitive material 审中-公开
标题翻译：银红色乳液和银红色摄影敏感材料
公开(公告)号：JP2004245929A
公开(公告)日：2004-09-02
申请号：JP2003033446
申请日：2003-02-12
申请人： Fuji Photo Film Co Ltd , 富士写真フイルム株式会社
发明人： ICHIJIMA YASUSHI , YAMADA KOZABURO , ASANUMA NAOKI
IPC分类号： G03C1/28 , G03C1/08 , G03C1/34 , G03C1/42
摘要： PROBLEM TO BE SOLVED: To provide a silver halide emulsion and a silver halide photographic sensitive material which suppress fogging due to increased sensitivity while increasing the photographic sensitivity of the photographic emulsion and ensure little increase of fog even when stored at high temperature and high humidity or under severe conditions including exposure to noxious gas generated during combustion, such as automobile exhaust gas. SOLUTION: The silver halide emulsion contains a compound capable of taking part in reactions including a cyclization reaction represented by a chemical reaction formula (1) after oxidation of the compound, wherein X 1 represents a group forming a 5-membered heterocyclic group in combination with C=C; Y 1 represents a group forming a 5- or 6-membered aryl or heterocyclic group in combination with C=C; R 1 and R 2 each represent H or a substituent; M represents a radical, a radical cation or a cation; and R 1 and R 2 may link together to form a 5- or 7-membered ring in combination with C=C. COPYRIGHT: (C)2004,JPO&NCIPI
摘要翻译：要解决的问题：提供卤化银乳剂和卤化银照相感光材料，其在增加感光乳剂的感光度的同时抑制起雾，同时确保即使在高温下储存时几乎不增加雾度，高湿度或恶劣条件下，包括暴露在燃烧过程中产生的有害气体，如汽车废气。解决方案：卤化银乳剂含有能够参与反应的化合物，包括在化合物氧化后由化学反应式（1）表示的环化反应，其中X 1 表示基团与C = C组合形成5元杂环基; Y 1表示与C = C组合形成5或6元芳基或杂环基的基团; R 1 和R SB 2各自表示H或取代基; M表示自由基，自由基阳离子或阳离子; 和R 1 和R SB 2可以连接在一起形成与C = C组合的5-或7-元环。版权所有（C）2004，JPO＆NCIPI

9. 发明专利

JP2000103767A AROMATIC ACETYLENE COMPOUND 失效
公开(公告)号：JP2000103767A
公开(公告)日：2000-04-11
申请号：JP27571798
申请日：1998-09-29
申请人： FUJI PHOTO FILM CO LTD
发明人： SUZUKI AKIRA , ASANUMA NAOKI , YAMAKAWA KAZUYOSHI
IPC分类号： C07C211/54 , C07C215/76 , C07C217/86 , C07C225/22 , C07C229/60 , C07C255/59 , C09K19/10
摘要： PROBLEM TO BE SOLVED: To obtain an aromatic acetylene compound useful as a liquid crystal material, an electronic material, a gas-permeable membrane material or a raw material therefor. SOLUTION: A compound of formula I [R is H or a substituent; Z1, Z2 are each a halogen, an alkyl, an aryl, an alkoxy, carboxyl, an alkylamino, nitro, cyano, sulfo or an acylamino; (1) is 0 to 4; (m), (n) are each 0 to 5]. For example, a compound of formula II. The compound of formula I is obtained by halogenating a triphenylamine derivative of formula III, subjecting the obtained compound of formula IV (X is I or Br) and an acetylene derivative to a cross- coupling reaction in the presence of a palladium metal catalyst [for example, PdCl2(PPh3)2] and a copper metal catalyst (for example, cuprous iodide) and subsequently removing a protecting group from the obtained compound of formula V (G is the protecting group).

10. 发明专利

JP2000072747A 7-ALKOXY-1,1-DISUBSTITUTED-1H-BENZO(e)INDOLE COMPOUND 失效
公开(公告)号：JP2000072747A
公开(公告)日：2000-03-07
申请号：JP24630198
申请日：1998-08-31
申请人： FUJI PHOTO FILM CO LTD
发明人： ASANUMA NAOKI , YAMAKAWA KAZUYOSHI
IPC分类号： C07D401/04 , C07D209/60
摘要： PROBLEM TO BE SOLVED: To obtain a new compound useful as a dye, a sensitizing dye in a halogenated silver photosensitive material field or a raw material of a synthetic intermediate of a medicine or agricultural chemicals. SOLUTION: This compound is expressed by the formula (R1 is an alkyl; R2 and R2 are each an alkyl, an aryl or a heterocyclic ring; R4 is H, an alkyl, an aryl or a heterocyclic ring). The compound is obtained by an indole synthesis of E.Fischer wherein 2-hydrazinonaphthalenes and ketones are synthesized as intermediates, concretely 6-methoxy-2-naphthol and 3-methyl-2-butanone are mixed while being stirred with xylene under a nitrogen atmosphere and methane sulfonic acid, then hydrazine hydrate are dropped and reacted at about 140 deg.C for about 24 hrs.

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