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1. 发明专利

JP2005097158A Method for producing fluorine-containing organic compound 审中-公开
标题翻译：生产含氟的有机化合物的方法
公开(公告)号：JP2005097158A
公开(公告)日：2005-04-14
申请号：JP2003331917
申请日：2003-09-24
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： SHIMIZU TAMAKI , FUJIMA TOSHIHIKO , MORISAWA YOSHITOMI
IPC分类号： C07C51/43 , C07C27/02 , C07C51/09 , C07C61/15
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a fluorine-containing organic compound, by which the highly pure fluorine-containing organic compound having a geminal difluoro structure can efficiently be produced without needing a complicated separation operation.
SOLUTION: This method for producing the fluorine-containing organic compound represented by general formula (3) is characterized by converting the ester sites of a mixture of a compound represented by general formula (1) (R
1 is a 1 to 20C alkyl group, an alkyl group substituted with one or more aryl groups, an alkyl group substituted with one or more monovalent heterocyclic groups, a 3 to 8C cycloalkyl group, an aryl group, an aryl group substituted with one or more substituents, or a 1 to 20C fluoroalkyl group) and a compound represented by general formula (2) into the carboxy groups to obtain the mixture of the compound of formula (3) and the compound of formula (4), and then crystallizing the mixture.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题：提供一种含氟有机化合物的制造方法，通过该方法可以有效地制备具有偕二氟结构的高纯度的含氟有机化合物，而不需要复杂的分离操作。解决方案：该通式（3）所示的含氟有机化合物的制造方法的特征在于将通式（1）表示的化合物的混合物的酯部位（R 1 SP 1） SP>为1〜20C的烷基，被1个以上的芳基取代的烷基，被1个以上的1价杂环基取代的烷基，3〜8个环烷基，芳基，被1个或更多取代基或1〜20C氟代烷基）和通式（2）表示的化合物转化成羧基，得到式（3）的化合物和式（4）的化合物的混合物，然后结晶混合物。版权所有（C）2005，JPO＆NCIPI

2. 发明专利

JP2008044876A Method for producing monooxyalkylenediol 审中-公开
标题翻译：生产单羟基乙烯醇的方法
公开(公告)号：JP2008044876A
公开(公告)日：2008-02-28
申请号：JP2006221115
申请日：2006-08-14
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： SHIMIZU TAMAKI , SEKI TAKASHI
IPC分类号： C07C41/16 , C07B61/00 , C07C43/178
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a monooxyalkylenediol, especially 4-oxa-1,7-heptanediol. SOLUTION: The method for producing a compound represented by formula: HO(CH 2 ) y O(CH 2 ) z OH [(y) and (z) are each independently an integer of 2 to 6] comprises reacting a compound represented by formula: HO(CH 2 ) y OH with a compound of represented by formula: X(CH 2 ) z OH (X is Cl or Br) in the presence of an alkali metal hydroxide. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供一氧化亚烷基二醇，特别是4-氧杂-1,7-庚二醇的制备方法。＆lt; P＆gt;解决方案：由下式表示的化合物的方法：HO（CH 2 SBB）O（CH 2 SB 2）SB Z [OH] [（y）和（z）各自独立地为2〜6的整数]包括使式HO：CH（CH 2 SBR）在碱金属氢氧化物的存在下，使用式（X）表示的化合物：（S）SB（OH）版权所有（C）2008，JPO＆INPIT

3. 发明专利

JP2005306902A Silicone solution for coating and method for coating silicone compound 审中-公开
标题翻译：用于涂料的硅氧烷溶液和用于涂覆硅氧烷化合物的方法
公开(公告)号：JP2005306902A
公开(公告)日：2005-11-04
申请号：JP2004121830
申请日：2004-04-16
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： SHIMIZU TAMAKI , OKAMOTO SHUICHI , MORISHIMA NAOTERU , TSUZAKI MASAAKI
IPC分类号： A61M5/32 , B05D7/24 , C09D183/04 , C10M105/76 , C10M107/50 , C10M131/04 , C10M131/10 , C10M169/04 , C10N30/06 , C10N40/00 , C10N50/02
摘要： PROBLEM TO BE SOLVED: To provide a silicone solution for coating exhibiting excellent slipperiness without affecting the environment and to provide a method for coating the silicone compound with which a film of the silicone compound is formed on the surface of an article.
SOLUTION: The film is formed by coating the surface of the article such as a needle tubular part of an injection needle with a silicone solution for coating containing a silicone compound and a fluorine-containing solvent composed of a hydrofluorocarbon or a hydrofluoroether, evaporating and removing the fluorine-containing solvent and thereby forming the film of the silicone compound on the surface of the article. 1,1,1,2,2,3,3,4,4-Nonafluorohexane, 1,1,2,2-tetrafluoroethyl-2,2,2-trifluoroethyl ether, etc., are used as the fluorine-containing solvent.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：为了提供在不影响环境的情况下显示出优异的滑爽性的涂层用硅氧烷溶液，并且提供在物品表面上形成硅氧烷化合物的膜的硅氧烷化合物的涂布方法。解决方案：通过用包含硅氧烷化合物的涂料的硅溶液和由氢氟烃或氢氟醚组成的含氟溶剂涂布诸如注射针的针筒部分的物品的表面，蒸发除去含氟溶剂，从而在制品的表面上形成硅氧烷化合物的膜。 1,1,1,2,2,3,3,4,4-十氟己烷，1,1,2,2-四氟乙基-2,2,2-三氟乙基醚等用作含氟溶剂。版权所有（C）2006，JPO＆NCIPI

4. 发明专利

JP2011021082A Water-repellent and oil-repellent agent composition and manufacturing method for the same 审中-公开
标题翻译：水及其制剂的组合物及其制造方法
公开(公告)号：JP2011021082A
公开(公告)日：2011-02-03
申请号：JP2009165821
申请日：2009-07-14
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： KANEKO KYOICHI , SUGIYAMA KAZUNORI , SHIMIZU TAMAKI , FUKUDA REIKA
IPC分类号： C09K3/18
摘要： PROBLEM TO BE SOLVED: To provide a water-repellent and oil-repellent agent composition that imparts water-repellent and oil-repellent properties on the surface of an article without deteriorating the touch of the article and a manufacturing method for the same.
SOLUTION: The water-repellent and oil-repellent agent composition comprises a fluorine-containing copolymer comprising 1-35 mass% of a polymerized unit of a perfluoroalkyl group-bearing (meth)acrylate or the like, 0-70 mass% of a polymerized unit of behenyl (meth)acrylate, 10-70 mass% of a polymerized unit of stearyl (meth)acrylate, 3-45 mass% of a polymerized unit (d) of vinyl chloride and 0-15 mass% of a polymerized unit (e) of a monomer bearing a crosslinkable functional group.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：为了提供在物品的表面上赋予防水和防油性能的拒水拒油剂组合物，而不会降低物品的触感和其制造方法。防水防油剂组合物包含含有全氟烷基（甲基）丙烯酸酯等的聚合单元的1-35质量％的含氟共聚物，0-70质量％的（甲基）丙烯酸山萮酯的聚合单元，（甲基）丙烯酸硬脂酯的聚合单元的10-70质量％，氯乙烯的聚合单元（d），质量分数为3-45质量％具有可交联官能团的单体的聚合单元（e）。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2006265182A New fluorine-containing compound and fluorine-containing polymer 有权
标题翻译：新的含氟化合物和含氟聚合物
公开(公告)号：JP2006265182A
公开(公告)日：2006-10-05
申请号：JP2005086604
申请日：2005-03-24
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： KAMIYA HIROKI , FUNAKI CHU , SHIMIZU TAMAKI , TAKAGI YOICHI , SUGIMOTO SUSUMU , MUROTANI EISUKE
IPC分类号： C07C43/17 , C07C41/28 , C08F16/24
摘要： PROBLEM TO BE SOLVED: To provide a new fluorine-containing compound [CF
2 =C(OCF
2 CF
3 )
2 ], and to provide a fluorine-containing polymer obtained by polymerizing the fluorine-containing compound.
SOLUTION: CF
2 =C(OCF
2 CF
3 )
2 is provided. The method for producing CF
2 =C(OCF
2 CF
3 )
2 comprises thermally decomposing reaction of CF
3 C(OCF
2 CF
3 )
2 (COF). The fluorine-containing polymer is obtained by polymerizing CF
2 =C(OCF
2 CF
3 )
2 and comprises polymer unit based on CF
2 =C(OCF
2 CF
3 )
2 , such as CF
2 =CF
2 /CF
2 =C(OCF
2 CF
3 )
2 copolymer.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：为了提供新的含氟化合物[CF 2 SB 2 = C（OCF 2 SB SB 3）SB > 2 ]，并提供通过使含氟化合物聚合而获得的含氟聚合物。
解决方案：提供了CF 2 = C（OCF 2 CF 3 ） 2 。制备CF 2 SBB = C（OCF 2 SBB）的方法包括CF 3的热分解反应， SB> 3 C（OCF 2 CF 3 ） 2 （COF）。含氟聚合物通过聚合CF 2 SBB = C（OCF SB SB 2）/ SB SB 3）SB获得，并且包含基于CF = C（OCF 2 CF 3 ）的聚合物单元，例如CF 2 = CF 2 / CF 2 = C（OCF 2 CF 3 ） 2 共聚物。版权所有（C）2007，JPO＆INPIT

6. 发明专利

JP2011021081A Water- and oil-repellent agent composition and method for producing the same 审中-公开
标题翻译：水和油性物质组合物及其生产方法
公开(公告)号：JP2011021081A
公开(公告)日：2011-02-03
申请号：JP2009165820
申请日：2009-07-14
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： INOUE HIROAKI , SUGIYAMA KAZUNORI , SHIMIZU TAMAKI
IPC分类号： C09K3/18 , C08F220/12 , C08F220/24 , C09D127/06 , C09D127/12 , C09D133/04 , C09D135/02 , D06M15/248 , D06M15/256 , D06M15/263
摘要： PROBLEM TO BE SOLVED: To provide a water- and oil-repellent agent composition imparting water- and oil-repellency to a surface of an article without degrading the texture of the article, and to provide a method for producing the composition. SOLUTION: The water- and oil-repellent agent composition comprises a fluorine-containing copolymer containing: 1 to 35 mass% of a polymer unit derived from (meth)acrylate or the like having a perfluoroalkyl group, 10 to 70 mass% of a polymer unit derived from behenyl (meth)acrylate, 0.1 to 30 mass% of a polymer unit derived from a maleic acid alkyl ester, 3 to 40 mass% of a polymer unit (d) derived from vinyl chloride, and 0 to 15 mass% of a polymer unit (e) derived from a monomer having a crosslinkable functional group. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种赋予物品表面赋予拒水拒油性的拒水拒油剂组合物，而不会降低制品的质感，并提供制备该组合物的方法。防水防油剂组合物包含含有1〜35质量％的来自（甲基）丙烯酸酯等的具有全氟烷基的聚合物单元的含氟共聚物，10〜70质量％的衍生自（甲基）丙烯酸山嵛酯的聚合物单元，0.1〜30质量％的来源于马来酸烷基酯的聚合物单元，3〜40质量％的来自氯乙烯的聚合物单元（d）和0〜15 衍生自具有交联性官能团的单体的聚合物单元（e）的质量％。版权所有（C）2011，JPO＆INPIT

7. 发明专利

JP2010132844A Urethane/urea compound, production method thereof, and water repellent composition 有权
标题翻译： URETHANE / UREA化合物，其生产方法和水组合物
公开(公告)号：JP2010132844A
公开(公告)日：2010-06-17
申请号：JP2008312737
申请日：2008-12-08
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： SHIMIZU TAMAKI , OTOSAWA NOBUYUKI , SHIMADA MINAKO , SHIMADA TOYOMICHI
IPC分类号： C08G18/62 , C08F220/22 , C09D175/04 , C09K3/18
摘要： PROBLEM TO BE SOLVED: To provide a compound which can impart sufficient water repellency to a surface of an article and has a low environmental load, and also to provide a method of production thereof and a water repellent composition. SOLUTION: The compound is obtained by reacting a hydroxy- or amino-containing oligomer (A), obtained by polymerizing a monomer mixture containing the following monomer (a), with a compound (B) having two or more isocyanate groups in the presence of the following compound (x), and the water repellent composition contains the compound. The compound (x) is a hydroxyl- or amino-containing thiol compound. The monomer (a) is a (meth)acrylate having a 20-30C alkyl group but a polyfluoroalkyl group. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供能够赋予制品表面足够的防水性并且具有低环境负荷的化合物，并提供其制备方法和防水组合物。解决方案：通过使含有下列单体（a）的单体混合物聚合得到的含羟基或氨基的低聚物（A）与具有两个或多个异氰酸酯基团的化合物（B）反应，得到化合物以下化合物（x）的存在和防水组合物含有该化合物。化合物（x）是含羟基或氨基的硫醇化合物。单体（a）是具有20-30C烷基但多氟烷基的（甲基）丙烯酸酯。版权所有（C）2010，JPO＆INPIT

8. 发明专利

JP2007332068A New fluoroadamantane derivative and method for producing the same 审中-公开
标题翻译：新的氟代丹参酮衍生物及其生产方法
公开(公告)号：JP2007332068A
公开(公告)日：2007-12-27
申请号：JP2006164865
申请日：2006-06-14
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： OU JIYOSHIYOU , MURATA KOICHI , SEKI TAKASHI , SHIMIZU TAMAKI , YAMASHITA HIROMASA
IPC分类号： C07C31/27 , C07B61/00 , C07C29/38 , C07C62/06 , C07C67/03 , C07C69/757
摘要： PROBLEM TO BE SOLVED: To obtain a new fluoroadamantane derivative and to provide a method for producing the same.
SOLUTION: The method for producing a compound represented by formula (5) comprises reacting a compound represented by formula (6) with a compound represented by formula (R
FA C(O))
2 O and then with a compound represented by formula (R
FB CH
2 OH). The method for producing a compound represented by formula (1) comprises reacting a compound represented by formula (31) with a protonic nucleophilic species to give a compound represented by formula (2) and then reacting the compound represented by formula (2) with a basic compound represented by formula R-CHO in the presence of a basic compound.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：获得新的氟金刚烷衍生物并提供其制备方法。解决方案：由式（5）表示的化合物的制备方法包括使由式（6）表示的化合物与式（R“SP”C（O））表示的化合物 2 O，然后与由式（R 2 SP 2 CH 2 CH 2）表示的化合物反应。制备由式（1）表示的化合物的方法包括使式（31）表示的化合物与质子亲核物质反应，得到由式（2）表示的化合物，然后使由式（2）表示的化合物与在碱性化合物存在下由式R-CHO表示的碱性化合物。版权所有（C）2008，JPO＆INPIT

9. 发明专利

JP2004115463A Production method for 1-chloro-1-fluoroethylene 审中-公开
公开(公告)号：JP2004115463A
公开(公告)日：2004-04-15
申请号：JP2002282964
申请日：2002-09-27
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： OSAKA KOJI , OKURA KAZUHIRO , SHIMIZU TAMAKI , WADA AKIHIRO , FUJIMA TOSHIHIKO
IPC分类号： C07C17/25 , C07B61/00 , C07C21/18
摘要： PROBLEM TO BE SOLVED: To produce 1-chloro-1-fluoroethylene (R1131a) by the liquid phase dehydrochlorination reaction of 1, 1-dichloro-1-fluoroethane (R141b) with a basic compound (an alkali) in high selectivity and yield.
SOLUTION: This method for producing the 1-chloro-1-fluoroethylene comprises subjecting the R141b to liquid phase dehydrochlorination reaction with the alkali while extracting the R1131a from the reaction system so as to keep the concentration of the R1131a in the reaction system at 5 mass% or lower.
COPYRIGHT: (C)2004,JPO

10. 发明专利

JPH06329566A DIFLUOROSTILBENE DERIVATIVE COMPOUND AND LIQUID CRYSTAL COMPOSITION CONTAINING THE SAME 失效
公开(公告)号：JPH06329566A
公开(公告)日：1994-11-29
申请号：JP14282193
申请日：1993-05-21
申请人： ASAHI GLASS CO LTD , SEIMI CHEM KK
发明人： IRISAWA JUN , YOKOKOJI OSAMU , SHIMIZU TAMAKI , ISHIDA YOSHIAKI , KO HIDEMASA , OIKE KEIKO , MACHIDA KATSUTOSHI
IPC分类号： C07C25/24 , C07C43/225 , C07C255/50 , C07C255/54 , C09K19/16
摘要： PURPOSE:To obtain a compound having low viscosity and high stability to light and useful as a liquid crystal material. CONSTITUTION:The compound of formula I [R and R are H, 1-10C alkyl, halogen or cyano; X, Y and Z are H, F, OCF3 or 1-10C alkyl], e.g. (Z)-1,2- difluoro-1-(4-fluorophenyl)-2-(4-n-pentylphenyl)ethylene. In the compound of formula I, an absorption edge at a long wavelength side of absorption band which appears in an ultraviolet absorbing area is positioned at a shorter wavelength area than the absorption edge of trans 1,2-difluoro-1,2-bis(4-methoxyphenyl) ethylene. The compound of formula I is obtained by subjecting a benzene derivative of formula II (W is Cl, Br or I) with to lithiation with n-butyllithium and reacting the resultant lithiated compound with a trifluoroethylene compound of formula III. The response speed is improved even in the case of adding a small amount of the compound of formula I and low voltage driving, high duty driving, action in wide temperature area, etc., are exhibited by using the compound of formula I as a liquid crystal composition.

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