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1. 发明专利

JP2007146191A Process for producing unsaturated group-containing polyether and hydrolyzable group-containing silicon group-containing polyether using the unsaturated group-containing polyether as raw material 审中-公开
标题翻译：使用不饱和基团的聚合物作为原料生产含不饱和基团的聚合物和含可氢化基团的含硅基团聚合物的方法
公开(公告)号：JP2007146191A
公开(公告)日：2007-06-14
申请号：JP2007070569
申请日：2007-03-19
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： WATABE TAKASHI , HATANO HIROSHI , CHIBA KAZUNORI , DOI TAKAO , UENO TORU , SAKAI ETSUKO , SAIKI SHINYA , YAMADA MINORU , YAMAMOTO HIROTSUGU , HIGUCHI TOSHIHIKO
IPC分类号： C08G65/30
摘要： PROBLEM TO BE SOLVED: To provide a process for purifying a polyether, remaining no salt.
SOLUTION: The process for purifying a polyether is provided, which process comprises adding to a polyether (A) containing a first salt, water (B) and a compound (C) which is capable of reacting with an ion constituting the first salt to form a second salt which is essentially insoluble in the polyether (A), then removing water, followed by removing the second salt from the polyether (A). A surfactant (D) is preferably added together with the water (B) and the compound (C).
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种纯化聚醚的方法，不保留盐。解决方案：提供聚醚的提纯方法，该方法包括加入含有第一盐的聚醚（A），水（B）和化合物（C），其能够与构成第一盐的离子反应盐形成基本上不溶于聚醚（A）的第二盐，然后除去水，然后从聚醚（A）中除去第二种盐。表面活性剂（D）优选与水（B）和化合物（C）一起加入。版权所有（C）2007，JPO＆INPIT

2. 发明专利

JP2003073417A Recovery device and recovery method for fluorine- containing polymer 有权
标题翻译：含氟聚合物的恢复装置和恢复方法
公开(公告)号：JP2003073417A
公开(公告)日：2003-03-12
申请号：JP2001263596
申请日：2001-08-31
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： CHIBA KAZUNORI , MUROFUSHI HIDENOBU , HATANO HIROSHI
IPC分类号： B01D1/00 , C08F6/06
摘要： PROBLEM TO BE SOLVED: To provide a recovery device for obtaining a bulky fluorine-containing polymer by performing the operations to achieve a desired amount of a residual volatile component under a thermal stable evaporating condition in batch-wise way or continuously and draining directly or with other methods from a container after evaporating the component to a receiver, and to provide a recovery method.
SOLUTION: In the method for recovering the polymer from a fluorine- containing polymer solution, the component is heated at a temperature equal to or higher than a lowest temperature which the solution is subjected to a phase separation, equal to or higher than a boiling point and equal to or lower than a decomposition point of the component to remove by evaporating and the resulting bulky polymer is melted and drained to the receiver.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供一种用于通过在热稳定蒸发条件下以分批的方式进行操作以获得所需量的残留挥发性成分的操作或连续排出或直接排出或与将组分蒸发到接收器之后的容器中的其它方法，以及提供回收方法。解决方案：在从含氟聚合物溶液中回收聚合物的方法中，将组分在等于或高于溶液进行相分离的等于或高于沸点的最低温度的温度下加热并且等于或低于通过蒸发除去的组分的分解点，并将所得的大体积聚合物熔化并排出到接收器中。

3. 发明专利

JPH03146510A FLUORINE-CONTAINING COPOLYMER AND ITS PRODUCTION 失效
公开(公告)号：JPH03146510A
公开(公告)日：1991-06-21
申请号：JP28500989
申请日：1989-11-02
申请人： ASAHI GLASS CO LTD
发明人： KODAMA SHUNICHI , KANBA MOTOI , KIMURA ISAO , CHIBA KAZUNORI
IPC分类号： C08F14/18 , C08F14/24 , C08F16/14 , C08F16/16 , C08F214/18 , C08F214/24 , C08F214/26 , C08F216/14 , C08F216/16 , C08G18/62 , C09D127/12
摘要： PURPOSE:To obtain the subject copolymer, excellent in surface hardness and gloss and capable of providing films having visibility by polymerizing a fluorine- based monomer mixture in the presence of a polymerization initiator while supplying the aforementioned mixture to a monomer polymerization system with advance of the polymerization. CONSTITUTION:A mixture of (A) a monomer expressed by formula I (X is Cl, F, 1-3C perfluoroalkyl or perfluoroalkoxy) with (B) a monomer expressed by formula II [R is H or methyl; R is 1-12C (fluorine-substituted) alkyl; (l) is 0 or 1] and (C) a monomer expressed by formula III [R is H or methyl; R is (fluorine-substituted) alkyl having OH group] is polymerized in the presence of a polymerization initiator while supplying the monomers to a monomer polymerization system with advance of the polymerization to afford the objective copolymer capable of providing films excellent in solvent, fouling resistance, etc.

4. 发明专利

JPH08231707A PURIFICATION OF POLYETHER 失效
公开(公告)号：JPH08231707A
公开(公告)日：1996-09-10
申请号：JP18033695
申请日：1995-07-17
申请人： ASAHI GLASS CO LTD
发明人： WATABE TAKASHI , HATANO HIROSHI , CHIBA KAZUNORI , DOI TAKAO , UENO TORU , SAKAI ETSUKO , SAIKI SHINYA , YAMADA MINORU , YAMAMOTO HIROTSUGU , HIGUCHI TOSHIHIKO
IPC分类号： C08G65/30 , C08G59/40 , C08G65/02 , C08G65/26 , C08G65/32 , C08G65/327 , C08G65/336
摘要： PURPOSE: To produce a purified polyether excellent in storage stability, etc., and free from remaining salt by adding a salt-containing polyether with water and a compound capable of forming another salt insoluble in the polyether, and removing water and the formed salt from the mixture. CONSTITUTION: A polyether containing (A) the first salt (preferably, a zinc salt or an alkali metal salt) is compounded with (B) water and (C) a compound (preferably, sodium dihydrogen pyrophosphate) which can form the second salt essentially insoluble in the component A by reacting with the ion constituting the first salt, water is removed, and subsequently the second salt is removed to obtain a purified polyether containing an extremely small amount of the remaining salt. Preferably, (D) a surfactant is further added to the mixture. The polyether of the component A is preferably a hydroxide-containing polyether obtained by reacting an initiator with a monoepoxide in the presence of a metal catalyst, or its modified compound.

5. 发明专利

JPH08118357A RECOVERY OF SOLID FLUOROPLASTIC FROM FLUOROPLASTIC SOLUTION 失效
公开(公告)号：JPH08118357A
公开(公告)日：1996-05-14
申请号：JP26060994
申请日：1994-10-25
申请人： ASAHI GLASS CO LTD
发明人： UENO TORU , YAMADA MINORU , CHIBA KAZUNORI
IPC分类号： C08J9/28 , B29B17/00 , B29K27/12
摘要： PURPOSE: To obtain solid fluoroplastic extremely reduced in residual solvent content within a short time in high yield by passing a soln. of solvent soluble fluoroplastic through a membrane forming device to remove a solvent within the device and discharging solid fluoroplastic in a dissolved state to recover the same. CONSTITUTION: Since the fluoroplastic soln. A thrown into a membrane evaporator 3 from a soln. throwing-in port 2' becomes a membrane state by stirring blades 7 and heated by the heating medium allowed to flow from a heating medium inlet 6, the fluoroplastic soln. A is guided to the lower part of the membrane evaporator 3 by the rotation of the stirring blades 7 while the solvent in the soln. A is evaporated. Dissolved fluoroplastic is discharged to the outside by a screw 8 to be cast on a cooling drum 9' to be pressed to the drum 9' by a pressure roll 10 and perfectly solidified while cooled to be peeled from a belt 11 by the bending of the belt 11 and plate-shaped or powdery solid fluoroplastic C is recovered by a solid resin recovery port.

6. 发明专利

JPH08109253A METHOD FOR PURIFYING POLYETHER 失效
公开(公告)号：JPH08109253A
公开(公告)日：1996-04-30
申请号：JP24421994
申请日：1994-10-07
申请人： ASAHI GLASS CO LTD
发明人： UENO TORU , YAMADA MINORU , SAKAI ETSUKO , HATANO HIROSHI , CHIBA KAZUNORI
IPC分类号： C08G65/30 , C08G65/02
摘要： PURPOSE: To remove a halide from a high mol.wt. polyether contg. a minor amt. of an alkali metal halide by adding a nonionic surfactant, a solvent, an anionic surfactant and an acid-contg. water to polyether. CONSTITUTION: A nonionic surfactant and a solvent are first added and mixed with a high mol.wt. polyether contg. a minor amt. of an alkali metal halide. An anionic surfactant and an acid-contg. water are added thereto, and the alkali metal halide is extracted into an aq. phase without vigorous stirring. Further, the aq. phase is removed to remove the alkali metal halide, thereby purifying the polyether. In general, stirring is known as a method for extracting an alkali metal halide into an aq. phase. The stirring, however, is unfavorable because when the stirring intensity is excessively high, the whole system becomes emulsified, making the separation difficult, while when the stirring intensity is excessively low, mixing of the org. phase with the aq. phase becomes unsatisfactory, rendering the extraction unsatisfactory.

7. 发明专利

JPH07119260B2 失效
公开(公告)号：JPH07119260B2
公开(公告)日：1995-12-20
申请号：JP28500989
申请日：1989-11-02
申请人： ASAHI GLASS CO LTD
发明人： KODAMA SHUNICHI , KANBA MOTOI , KIMURA ISAO , CHIBA KAZUNORI
IPC分类号： C08F14/18 , C08F14/24 , C08F16/14 , C08F16/16 , C08F214/18 , C08F214/24 , C08F214/26 , C08F216/14 , C08F216/16 , C08G18/62 , C09D127/12

8. 发明专利

JPH0286602A PRODUCTION OF FLUOROCOPOLYMER 失效
公开(公告)号：JPH0286602A
公开(公告)日：1990-03-27
申请号：JP23646688
申请日：1988-09-22
申请人： ASAHI GLASS CO LTD
发明人： CHIBA KAZUNORI , KANBA MOTOI , MIYAZAKI NOBUYUKI
IPC分类号： C08F14/18 , C08F2/00 , C08F2/04 , C08F2/06
摘要： PURPOSE:To prepare a fluorocopolymer economically with excellent process operation properties, by continuously copolymerizing a fluoroolefin with a polymerizable unsatd. monomer in a tubular reactor equipped with a static mixer. CONSTITUTION:In a process wherein a fluoroolefin is copolymerized with a polymerizable unsatd. monomer in a solvent in the presence of a radical initiator to produce a copolymer essentially comprising the fluoroolefin units and the polymerizable unsatd. monomer units, the copolymerization is continuously carried out using a tubular reactor equipped with a static mixer. Because said reactor provides an increased area for heat-transfer per unit volume of the reactor, removal of the heat of reaction becomes easy, the reaction rate increases, and the reaction time is reduced.

9. 发明专利

JPS63210149A RECOVERY OF SOLID FLUOROPOLYMER FROM FLUOROPOLYMER SOLUTION 失效
公开(公告)号：JPS63210149A
公开(公告)日：1988-08-31
申请号：JP4291487
申请日：1987-02-27
申请人： ASAHI GLASS CO LTD
发明人： KIMURA HIROSHI , CHIBA KAZUNORI
IPC分类号： B01D1/00 , B29B17/02 , C08J11/00 , C08J11/06
摘要： PURPOSE:To recover a solid fluoropolymer low in a residual solvent safely without any pollution within a short time, by casting a solution of a solvent- soluble fluoropolymer on a support having a nonadhering surface and removing the solvent from the film. CONSTITUTION:For example, a fluoroolefin (e.g., tetrafluoroethylene) is copolymerized with a vinyl ether (e.g., a 1-10C linear alkyl vinyl ether) and, optionally, other comonomers such as (meth)acrylic acid esters to obtain a solvent-soluble fluoropolymer (A) of a glass transition temperature >=30 deg.C and an intrinsic viscosity of 0.05-2.0dl/g (in tetrahydrofuran at 30 deg.C). A solution formed by dissolving component A in a solvent (B) such as xylene, n-butanol or methyl isobutyl ketone is cast on a support (C) having a nonadhering surface comprising a solvent-insoluble fluoropolymer such as a polytetrafluoroethylene resin, and the solvent is removed from the film by application of a vacuum and/or heat to recover a solid fluoropolymer.

10. 发明专利

JPH08176292A PURIFICATION OF POLYETHER 失效
公开(公告)号：JPH08176292A
公开(公告)日：1996-07-09
申请号：JP24492295
申请日：1995-09-22
申请人： ASAHI GLASS CO LTD
发明人： UENO TORU , CHIBA KAZUNORI , SAIKI SHINYA , OKAZAKI SHINOBU
IPC分类号： C08G65/30 , C08G65/02
摘要： PURPOSE: To easily obtain a high-molecular polyether contg. little salt by adjusting the pH of a polyether contg. a first salt, then adding thereto a compd. capable of forming a second salt, removing water from the resulting mixture, and removing the second salt from the polyether. CONSTITUTION: In a process for purifying a polyether (A) contg. a first salt by adding water (B) and a compd. (C) capable of forming a second salt substantially insoluble in the polyether (A) through a reaction thereof with ions constituting the first salt to the polyether (A), removing water from the resulting mixture, and removing the second salt from the polyether (A) ; the pH of the polyether (A) is adjusted to 2 to 12 before the addn. thereto of the compd. (C). This process is pref. as a method of purifying a hydroxyl group-contg. polyether contg. a salt attributed to a catalyst obtd. by reacting an initiator with a monoepoxide in the presence of a catalyst. A purification product of a high-molecular weight polyether can be easily obtd. according to this process.

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