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1. 发明专利

JP2005240049A Room temperature curing composition and manufacturing method therefor 审中-公开
标题翻译：室温固化组合物及其制备方法
公开(公告)号：JP2005240049A
公开(公告)日：2005-09-08
申请号：JP2005155523
申请日：2005-05-27
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： WATABE TAKASHI , DOI TAKAO
IPC分类号： C08L71/02
摘要： PROBLEM TO BE SOLVED: To obtain a curing composition which gives a curing material having enough flexibility and which has a low viscosity.
SOLUTION: A high-molecular polymer (I) having a molecular weight of 8000-30000 in which 50% or more of total molecular terminal groups are hydrolyzable silicon group and 1-200 pts.wt. of a high-molecular polymer (II) having a molecular weight of 4000-30000 in which less than 50% of the total molecular terminal groups are hydrolyzable silicon group per 100 pts.wt. of the high-molecular polymer (I) are mixed to make the room temperature curing composition. The room temperature curing composition has the enough low viscosity and does not deteriorate the flexibility of its curing material even if an inorganic filler is used.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：获得具有足够的柔性并且具有低粘度的固化材料的固化组合物。解决方案：分子量为8000-30000的高分子量聚合物（I），其中总分子端基的50％或更多是可水解硅基团和1-200重量份。的分子量为4000-30000的高分子聚合物（II），其中小于总分子端基的50％是每100重量份可水解的硅基团。的高分子聚合物（I）混合以制成室温固化组合物。室温固化组合物具有足够的低粘度，并且即使使用无机填料也不会降低其固化材料的柔韧性。版权所有（C）2005，JPO＆NCIPI

2. 发明专利

JP2003082222A Curable composition 有权
标题翻译：可固化组合物
公开(公告)号：JP2003082222A
公开(公告)日：2003-03-19
申请号：JP2001300141
申请日：2001-09-28
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： FUKAZAWA TOMOYOSHI , KASHIWAME KIYOTERU , KONDO SATOSHI , WATABE TAKASHI
IPC分类号： C09K3/10 , C08K5/06 , C08K5/10 , C08K5/17 , C08L71/02
摘要： PROBLEM TO BE SOLVED: To provide a curable composition having excellent stain resistance. SOLUTION: This curable composition is characterized by comprising (A) an oxyalkylene polymer having reactive silicon groups at the terminals, (B) an oxyalkylene compound having R -Y group (R is a >=5C hydrocarbon group; Y is a group such as O, COO, or NH) at the terminal, having an oxyethylene group, and not having a reactive silicon group, and (C) a curing accelerator.
摘要翻译：待解决的问题：提供耐污染性优异的固化性组合物。解决方案：该可固化组合物的特征在于包含（A）末端具有反应性硅基的氧化烯聚合物，（B）具有R 0 -Y基团的氧化烯化合物（R 0 = 5℃; Y是具有氧乙烯基，不具有反应性硅基的末端的O，COO或NH基等，（C）固化促进剂。

3. 发明专利

JP2003055451A Curing composition 审中-公开
标题翻译：固化组合物
公开(公告)号：JP2003055451A
公开(公告)日：2003-02-26
申请号：JP2002153939
申请日：2002-05-28
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： YAMAMOTO HIROSHI , TANAKA HIDEAKI , KASHIWAME KIYOTERU , SUZUKI KAZUTOSHI , WATABE TAKASHI , SUGIYAMA KAYOKO
IPC分类号： C08G65/336 , C08G77/46
摘要： PROBLEM TO BE SOLVED: To provide a curing composition excellent in adhesiveness.
SOLUTION: This curing composition contains a curing promoter and an oxyalkylene polymer of which the main chain is obtained by open-ring polymerization of a cyclic ether with a compound containing an active hydrogen as an initiator, and the polymer has at least a reactive silicon group on the end of its molecule and its molecular weight per its end group is not less than 5,000 and Mw/Mn is not less than 1.5, and the polymer comprises only structures based on the initiator and the cyclic ether.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供粘合性优异的固化组合物。解决方案：该固化组合物含有固化促进剂和氧化烯聚合物，其主链通过环醚与含有活性氢作为引发剂的化合物开环聚合而获得，并且该聚合物至少具有反应性硅基其分子末端及其端基的分子量不小于5,000，Mw / Mn不小于1.5，聚合物仅包含基于引发剂和环醚的结构。

4. 发明专利

JP2003034750A Curable composition 有权
标题翻译：可固化组合物
公开(公告)号：JP2003034750A
公开(公告)日：2003-02-07
申请号：JP2001222003
申请日：2001-07-23
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： KASHIWAME KIYOTERU , KONDO SATOSHI , FUKAZAWA TOMOYOSHI , WATABE TAKASHI
IPC分类号： C08L101/00 , C08K5/00 , C08L71/02
摘要： PROBLEM TO BE SOLVED: To obtain a curable composition capable of giving a cured product having stain resistant property. SOLUTION: This composition contains (A) at least one reactive curing polymer selected from among a silicone polymer having a reactive group, a polysulfide polymer having a reactive group, a modified polysulfide polymer having a reactive group, an acrylic urethane polymer having a reactive group, a fluorine-containing polymer having a polymerization unit based on fluoroolefin and a reactive group, a saturated hydrocarbon polymer having a hydrolyzable silicon group and an acrylic polymer having a hydrolyzable silicon group and (B) an oxyalkylene compound having a R -Y terminal group (wherein, R is a hydrocarbon group having 5 or more carbons; Y denotes -O-, -COO-, -NH- or -N=), an oxyethylene group but no reactive silicon group.
摘要翻译：要解决的问题：获得能够得到具有防污性的固化产物的固化性组合物。解决方案：该组合物含有（A）至少一种选自具有反应性基团的硅氧烷聚合物，具有反应性基团的多硫化物聚合物，具有反应性基团的改性多硫化物聚合物，具有反应性基团的丙烯酸聚氨酯聚合物具有基于氟烯烃和反应性基团的聚合单元的含氟聚合物，具有可水解硅基团的饱和烃聚合物和具有可水解硅基团的丙烯酸类聚合物，和（B）具有R 0 - Y末端基（其中，R 0为碳原子数5以上的烃基，Y表示-O-，-COO-，-NH-或-N =），氧化乙烯基团，无反应性硅基团。

5. 发明专利

JP2003013040A Method for producing substrate/sealant joined product 有权
标题翻译：生产基材/密封剂加工产品的方法
公开(公告)号：JP2003013040A
公开(公告)日：2003-01-15
申请号：JP2001202364
申请日：2001-07-03
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： WATABE TAKASHI , KASHIWAME KIYOTERU
IPC分类号： B05D1/36 , B05D7/24 , C09D5/00 , C09D175/04 , C09D183/04 , C09D201/10 , C09J5/02 , C09J123/18 , C09K3/10
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a substrate/sealant joined product, by which the joint between the substrate and the sealant can be strengthened.
SOLUTION: This method for producing the substrate/sealant joined product is characterized by comprising a process for coating the substrate with the first primer composition containing a urethane-based compound to form the first primer layer, a process for coating the first primer layer with the second primer composition containing a silane coupling agent and/a reactive silicone resin to form the second primer layer, and a process for coating the second primer layer with the sealant containing a polyisobutylene-based polymer having reactive silicon groups.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供一种用于生产基材/密封剂接合产品的方法，通过该方法可以增强基材和密封剂之间的接合。解决方案：该基板/密封剂接合产品的制造方法的特征在于包括用含有氨基甲酸酯类化合物的第一底漆组合物涂布基材以形成第一底漆层的方法，用第含有硅烷偶联剂和/或反应性硅氧烷树脂以形成第二底漆层的第二底漆组合物，以及用含有具有反应性硅基团的聚异丁烯类聚合物的密封剂涂覆第二底涂层的方法。

6. 发明专利

JP2007146191A Process for producing unsaturated group-containing polyether and hydrolyzable group-containing silicon group-containing polyether using the unsaturated group-containing polyether as raw material 审中-公开
标题翻译：使用不饱和基团的聚合物作为原料生产含不饱和基团的聚合物和含可氢化基团的含硅基团聚合物的方法
公开(公告)号：JP2007146191A
公开(公告)日：2007-06-14
申请号：JP2007070569
申请日：2007-03-19
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： WATABE TAKASHI , HATANO HIROSHI , CHIBA KAZUNORI , DOI TAKAO , UENO TORU , SAKAI ETSUKO , SAIKI SHINYA , YAMADA MINORU , YAMAMOTO HIROTSUGU , HIGUCHI TOSHIHIKO
IPC分类号： C08G65/30
摘要： PROBLEM TO BE SOLVED: To provide a process for purifying a polyether, remaining no salt.
SOLUTION: The process for purifying a polyether is provided, which process comprises adding to a polyether (A) containing a first salt, water (B) and a compound (C) which is capable of reacting with an ion constituting the first salt to form a second salt which is essentially insoluble in the polyether (A), then removing water, followed by removing the second salt from the polyether (A). A surfactant (D) is preferably added together with the water (B) and the compound (C).
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种纯化聚醚的方法，不保留盐。解决方案：提供聚醚的提纯方法，该方法包括加入含有第一盐的聚醚（A），水（B）和化合物（C），其能够与构成第一盐的离子反应盐形成基本上不溶于聚醚（A）的第二盐，然后除去水，然后从聚醚（A）中除去第二种盐。表面活性剂（D）优选与水（B）和化合物（C）一起加入。版权所有（C）2007，JPO＆INPIT

7. 发明专利

JP2006009037A Method for producing hydrolyzable silyl group-containing oxyalkylene polymer and curable composition 有权
标题翻译：生产含可水解的含硅烷基的含亚烷基聚合物和可固化组合物的方法
公开(公告)号：JP2006009037A
公开(公告)日：2006-01-12
申请号：JP2005276856
申请日：2005-09-22
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： OTSUKA IWAHIRO , WATABE TAKASHI , SUGIYAMA KAYOKO
IPC分类号： C08G65/48 , C08K3/00 , C08L71/02
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a hydrolysable silyl group-containing oxyalkylene polymer having a high mol. wt. and a narrow mol. wt. distribution. SOLUTION: This method for producing the hydrolysable silyl group-containing oxyalkylene polymer comprises reacting an alkylene oxide in the presence of a composite metal cyanide complex in which a mixture of t-butyl alcohol with one or more other compounds as organic ligands are coordinated, to obtain the polymer having a total unsaturation degree of ≤0.02 meq/g, and then converting the terminal hydroxyl groups of the polymer into the hydrolysable silyl groups. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供一种制备具有高摩尔比的可水解甲硅烷基氧化烯聚合物的方法。重量。和一个窄的摩尔。重量。分配。解决方案：用于制备可水解甲硅烷基的氧化烯聚合物的方法包括在复合金属氰化物络合物的存在下使环氧烷反应，其中叔丁醇与一种或多种其它化合物作为有机配体的混合物是配位，得到总不饱和度≤0.02meq/ g的聚合物，然后将聚合物的末端羟基转化为可水解的甲硅烷基。版权所有（C）2006，JPO＆NCIPI

8. 发明专利

JP2010168588A Methods for producing hydrolyzable silyl group-containing oxyalkylene polymer and curable composition 有权
标题翻译：生产含可水解的含硅烷基的含亚烷基聚合物聚合物和可固化组合物的方法
公开(公告)号：JP2010168588A
公开(公告)日：2010-08-05
申请号：JP2010051916
申请日：2010-03-09
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： OTSUKA IWAHIRO , WATABE TAKASHI , SUGIYAMA KAYOKO
IPC分类号： C08G65/336 , C08K3/00 , C08K5/00 , C08L71/02 , C09K3/10
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a hydrolyzable silyl group-containing oxyalkylene polymer having a high molecular weight and a narrow molecular weight distribution, and to provide a room temperature curable composition.
SOLUTION: The method for producing a hydrolyzable silyl group-containing oxyalkylene polymer includes reacting an alkylene oxide by using, as a catalyst, a composite metal cyanide complex in which a mixture of t-butyl alcohol and other compounds are coordinated as organic ligands to obtain a polymer having a number average molecular weight of 5,000-30,000 and a total degree of unsaturation of 0.02 meq/g or less and converting a terminal hydroxyl group of the polymer to a hydrolyzable silyl group. There is also disclosed a room temperature curable composition containing the polymer.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供一种生产具有高分子量和窄分子量分布的可水解甲硅烷基的氧化烯聚合物的方法，并提供室温可固化组合物。解决方案：含有水解性甲硅烷基的氧化烯聚合物的制造方法包括使用作为催化剂的叔丁醇与其他化合物的混合物配位的复合金属氰化物配合物作为有机物使环氧烷反应配体，得到数均分子量为5,000〜30,000，总不饱和度为0.02meq / g以下的聚合物，将聚合物的末端羟基转变为水解性甲硅烷基。还公开了含有该聚合物的室温固化性组合物。版权所有（C）2010，JPO＆INPIT

9. 发明专利

JP2007070641A Curable composition 审中-公开
标题翻译：可固化组合物
公开(公告)号：JP2007070641A
公开(公告)日：2007-03-22
申请号：JP2006312804
申请日：2006-11-20
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： DOI TAKAO , YAMAMOTO HIROTSUGU , WATABE TAKASHI , HIGUCHI TOSHIHIKO
IPC分类号： C08L71/02 , C08F290/06
摘要： PROBLEM TO BE SOLVED: To provide a curable composition that is excellent in storage stability and gives a cured article having excellent mechanical strength.
SOLUTION: The curable composition comprises an organic polymer (A) having a hydrolyzable silicon group represented by the formula (1): -R- SiX
a R
1
3-a (wherein R is a divalent organic group, R
1 is an optionally substituted monovalent 1-20C hydrocarbon group, X is a hydrolyzable group, and a is 1, 2, or 3) and having a total content of ionic impurities of 50 ppm or lower, and a polymer (B) of a monomer having a polymerizable unsaturated group.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种存储稳定性优异的固化性组合物，其具有优异的机械强度。解决方案：可固化组合物包含具有由式（1）表示的可水解硅基团的有机聚合物（A）：-R-SiX R SB> 3-a （其中R是二价有机基团，R 1 SP 1是任选取代的一价1-20C烃基，X是可水解基团，a是1,2 ，或3），并且离子杂质的总含量为50ppm以下，和具有聚合性不饱和基团的单体的聚合物（B）。版权所有（C）2007，JPO＆INPIT

10. 发明专利

JPH11279425A Hardenable composition 失效
标题翻译：可怕的组合物
公开(公告)号：JPH11279425A
公开(公告)日：1999-10-12
申请号：JP7971998
申请日：1998-03-26
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： YOKOTA MIKIO , WATABE TAKASHI , MATSUMOTO TOMOKO , ONOGUCHI TATSUO
IPC分类号： C08L101/10 , C08K5/54 , C09J201/10
摘要： PROBLEM TO BE SOLVED: To obtain a hardenable composition capable of providing a hardened product having excellent mechanical strengths and an adhesive strength, and capable of maintaining the properties even after a long term preservation with water by including a specific organic polymer and a specified urea derivative.
SOLUTION: This hardenable composition comprises (A) an organic polymer having at least one of silicon-containing group having a silicon atom bound to a hydroxy group or a hydrolyzable group, and (B) a urea derivative having the silicon-containing group containing the silicon atom bound to the hydroxy group or the hydrolyzable group [e.g. N-(3-trimethoxysilylpropyl)urea], regulated so that the weight ratio of the components A/B may be (100/0.1)-(100/40). A group of the formula; SiX
a R
1
3-a [R
1 is a 1-20C (substituted) monovalent hydrocarbon; X is OH or a monovalent hydrolyzable group; (a) is 1-3] is preferable as the silicon-containing group containing the silicon atom bound to the hydroxy group or the hydrolyzable group.
COPYRIGHT: (C)1999,JPO
摘要翻译：要解决的问题：为了获得能够提供具有优异的机械强度和粘合强度的硬化产物的可硬化组合物，并且即使在通过包括特定的有机聚合物和特定的尿素衍生物在长期保存水后也能够保持其性能。解决方案：该可硬化组合物包含（A）具有至少一个具有与羟基或可水解基团结合的硅原子的含硅基团的有机聚合物，和（B）含有含硅基团的脲衍生物，结合到羟基或可水解基团的硅原子[例如， N-（3-三甲氧基甲硅烷基丙基）脲]，使得成分A / B的重量比可以为（100 / 0.1） - （100/40）。一组公式; SiXa R 1-a [R 1]是1-20C（取代的）一价烃; X是OH或一价可水解基团; （a）为1-3]优选含有与羟基或可水解基团结合的硅原子的含硅基团。

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