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1. 发明专利

JP2010144180A Polyolefin 有权
标题翻译：聚烯烃
公开(公告)号：JP2010144180A
公开(公告)日：2010-07-01
申请号：JP2010003965
申请日：2010-01-12
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： KAWAI KOJI , YAMASHITA MASAHIRO , DOI YASUSHI , KAWAHARA NOBUO , MICHIGAMI KENJI , KANEYOSHI HIROMU , MORI RYOJI
IPC分类号： C08F10/00 , C07F17/00 , C08F4/64 , C08F4/659 , C08F4/6592 , C08F110/06
CPC分类号： C07F17/00 , C08F4/65912 , C08F4/65916 , C08F10/00 , C08F110/06 , Y10S526/943 , C08F4/65927 , C08F2500/12 , C08F2500/03 , C08F2500/15 , C08F210/16 , C08F210/08 , C08F2500/17
摘要： PROBLEM TO BE SOLVED: To provide a polyolefin suitable for use in a nonwoven fabric, a film, a sealant, an industrial material, transparent injection, a block polymer, an alloy, a modifying material, or the like and specifically, broadly available for applications, such as sanitary materials, civil engineering materials, automobile materials, home electric appliances, food containers, packaging materials, or miscellaneous goods. SOLUTION: The polyolefin contains a repeating unit (U 1 ) derived from one α-olefin selected from a 3-8C α-olefin and optionally a repeating unit (U 2 ), other than the repeating unit (U 1 ), derived from at least one olefin selected from a 2-20C α-olefin, wherein (i) both 2, 1-insertion and 1, 3-insertion are 0.2% or less, (ii) a molecular weight distribution (Mw/Mn) obtained by gel permeation chromatography is 1-3, and (iii) an amount of dissolvable component in decane is 2 wt.% or less. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：为了提供适用于无纺布，膜，密封剂，工业材料，透明注射剂，嵌段聚合物，合金，改性材料等的聚烯烃，具体地说，可广泛应用于卫生材料，土木工程材料，汽车材料，家用电器，食品容器，包装材料或杂项用途。解决方案：聚烯烃包含衍生自选自3-8Cα-烯烃和任选的重复单元的一种α-烯烃的重复单元（U 1 ）（U SB'），除了选自2-20℃α-烯烃中的至少一种烯烃以外的重复单元（U 1 ），其中（i）2,1-插入和1， 3-插入量为0.2％以下，（ii）通过凝胶渗透色谱法得到的分子量分布（Mw / Mn）为1-3，（iii）癸烷中可溶成分的含量为2重量％以下。版权所有（C）2010，JPO＆INPIT

2. 发明专利

JP2010144035A Method of manufacturing high molecular weight olefin polymer 有权
标题翻译：制备高分子量烯烃聚合物的方法
公开(公告)号：JP2010144035A
公开(公告)日：2010-07-01
申请号：JP2008322484
申请日：2008-12-18
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： YUKITA TAKASHI , YAMASHITA MASAHIRO , YAMADA KO , KANEYOSHI HIROMU
IPC分类号： C08F4/6592 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing an olefin polymer, having a sufficiently high molecular weight and a low melting point even under the high temperature condition, at excellent polymerization activity.
SOLUTION: In the method of manufacturing the olefin polymer, an α-olefin is polymerized in the presence of a catalyst for olefin polymerization containing (A) a crosslinked metallocene compound represented by general formula (1) and (B) a compound such as (b-1) an organic aluminum oxy compound. In the formula (1), R
1 -R
12 each independently represent a hydrogen atom or the like, and at least one of R
1 and R
5 and at least one of R
8 and R
12 represent a hydrocarbon group, and R
13 and R
14 each independently represent an organic group represented by general formula (2).
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：即使在高温条件下，提供具有足够高分子量和低熔点的烯烃聚合物的制备方法，具有优异的聚合活性。解决方案：在制备烯烃聚合物的方法中，在烯烃聚合催化剂存在下聚合α-烯烃，该催化剂含有（A）由通式（1）表示的交联金属茂化合物和（B）化合物例如（b-1）有机铝氧基化合物。在式（1）中，R 1和R 2各自独立地表示氢原子等，并且R 1 SP / 和R 5 ，R SP＆lt; SP＆gt;和＆lt; SP＆gt; 12＆lt; SP＆gt;中的至少一个表示烃基，R 13和 R 14各自独立地表示由通式（2）表示的有机基团。版权所有（C）2010，JPO＆INPIT

3. 发明专利

JP2014177508A Method of producing catalyst containing novel fluorene derivative and method of producing olefin polymer 审中-公开
标题翻译：含有新型荧光素衍生物的催化剂的生产方法和生产烯烃聚合物的方法
公开(公告)号：JP2014177508A
公开(公告)日：2014-09-25
申请号：JP2013050390
申请日：2013-03-13
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： KITAGAWA HIDEO , YAMASHITA MASAHIRO , KANEYOSHI HIROMU
IPC分类号： C08F4/6592 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To provide an advantageous production method with high productivity which provides a polypropylene having a low melting point and a high molecular weight.SOLUTION: An olefin is polymerized at 40°C or higher in the presence of catalyst which contains a crosslinked metallocene compound of formula [1] and an organic aluminum oxy compound. In the formula [1], Rand Rare 6-20C aryl group optionally containing a halogen; Rand Rare derivatives of the phenyl group; Y is a crosslinking group; and M is Zr.
摘要翻译：要解决的问题：提供一种高生产率的有利的生产方法，其提供具有低熔点和高分子量的聚丙烯。解决方案：烯烃在40℃或更高的温度下在催化剂存在下聚合，所述催化剂含有交联式[1]的茂金属化合物和有机铝氧基化合物。在式[1]中，任选含有卤素的兰德稀土6-20C芳基; 兰德稀有衍生物的苯基; Y是交联基团; M为Zr。

4. 发明专利

JP2010047629A Manufacturing method for high melting point olefin polymer 审中-公开
标题翻译：高熔点烯烃聚合物的制造方法
公开(公告)号：JP2010047629A
公开(公告)日：2010-03-04
申请号：JP2008210482
申请日：2008-08-19
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： YAMASHITA MASAHIRO , YUKITA TAKASHI
IPC分类号： C08F4/6592
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method for an olefin polymer using a polymerization catalyst capable of performing polymerization at a high temperature, being excellent in polymerization activity and indicating a high melting point and a high molecular weight by the obtained polymer. SOLUTION: In the manufacturing method for the olefin polymer, 2C or more α-olefin is polymerized in the presence of the catalyst containing a crosslinked metallocene compound (A) represented by general formula [1]: and one kind or more of the compound (B) selected from an organic aluminumoxy compound (b-1), etc. (wherein M is Ti, Zr or Hf). COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种使用能够在高温下进行聚合的聚合催化剂的烯烃聚合物的制造方法，聚合活性优异，通过所得聚合物表现出高熔点和高分子量。解决方案：在烯烃聚合物的制造方法中，在含有由通式[1]表示的交联金属茂化合物（A）的催化剂存在下，将2种以上的α-烯烃聚合：选自有机铝氧化合物（b-1）等的化合物（B）（其中M为Ti，Zr或Hf）。版权所有（C）2010，JPO＆INPIT

5. 发明专利

JP2014159591A Method of producing olefin polymer particles 有权
标题翻译：生产烯烃聚合物颗粒的方法
公开(公告)号：JP2014159591A
公开(公告)日：2014-09-04
申请号：JP2014092925
申请日：2014-04-28
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： FUNATANI MUNEHITO , SAKUMA ATSUSHI , YAMASHITA MASAHIRO
IPC分类号： C08F2/44 , C08F4/6592
CPC分类号： C08F10/00 , C08F4/6592 , C08F4/65927 , C08F210/06 , C08F210/16 , C08F4/65916 , C08F4/65912 , C08F2500/26
摘要： PROBLEM TO BE SOLVED: To provide a method of efficiently producing olefin polymer particles having an excellent particulate morphology without fouling accompanied.SOLUTION: A solid catalyst (K) for olefin polymerization contains a specific Zr-based metallocene-based compound and simultaneously meets the following requirements [1] and [2]: [1] the loss of ignition is 30 wt.% or less as measured on a differential thermobalance; and [2] after normal-temperature steam treatment and contact with acetonitrile, an eluted component contains a compound having a molecular skeleton of the specified general formula [I], where R is a hydrogen atom or an alkyl group having 1 to 12 carbon atoms.
摘要翻译：要解决的问题：提供一种有效地生产具有优异的颗粒形状而没有结垢的烯烃聚合物颗粒的方法。溶液：用于烯烃聚合的固体催化剂（K）含有特定的基于Zr的茂金属类化合物，同时满足以下要求[1]和[2]：[1]通过差示热平衡测量，点火损失为30重量％以下; 和[2]经常温蒸汽处理并与乙腈接触后，洗脱组分含有具有特定通式[I]的分子骨架的化合物，其中R是氢原子或具有1至12个碳原子的烷基。

6. 发明专利

JP2014073983A Novel metallocene compound, olefin polymerization catalyst, and production process of olefin polymer 审中-公开
标题翻译：新型金属化合物，烯烃聚合催化剂和烯烃聚合物的生产工艺
公开(公告)号：JP2014073983A
公开(公告)日：2014-04-24
申请号：JP2012221368
申请日：2012-10-03
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： YAMASHITA MASAHIRO , HIBARA MAYUMI , SHIMAZAKI TOSHIYUKI , YUKITA TAKASHI , KANEYOSHI HIROMU
IPC分类号： C07F17/00 , C07F7/00 , C08F4/6592 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To provide a novel metallocene compound having a catalytic activity capable of producing an olefin polymer having high melting point and high molecular weight even under high temperature conditions which are advantageous in industrial production processes.SOLUTION: There is provided a metallocene compound represented by following formula for example. There are provided a catalyst for olefin polymerization containing the novel metallocene compound, and a production process of olefin polymers using the catalyst.
摘要翻译：要解决的问题：提供具有能够生产具有高熔点和高分子量的烯烃聚合物的催化活性的新颖的茂金属化合物，即使在有利于工业生产方法的高温条件下也是有利的。提供了茂金属化合物以下列公式表示。提供了含有新型金属茂化合物的烯烃聚合催化剂和使用该催化剂的烯烃聚合物的生产方法。

7. 发明专利

JP2011122118A Method of manufacturing olefin polymer 审中-公开
标题翻译：制备烯烃聚合物的方法
公开(公告)号：JP2011122118A
公开(公告)日：2011-06-23
申请号：JP2009283038
申请日：2009-12-14
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： YUKITA TAKASHI , YAMADA KO , YAMASHITA MASAHIRO , KANEYOSHI HIROMU
IPC分类号： C08F4/6592 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing polymer which has a fully wide molecular weight distribution and a high melting point of the polymer in a high-temperature condition which can be industrialized when polymerizing olefins such as propylene. SOLUTION: The method of manufacturing an olefin polymer is characterized in that at least one monomer chosen from two or more-carbon number α-olefins is polymerized at least at 40°C under the presence of an olefin polymerization catalyst containing (A) a crosslinking metallocene compound expressed by formula [1], and (B) a compound chosen from (b-1) an organoaluminumoxy compound or the like. R 1 -R 12 each independently denote a hydrogen atom, halogen atom, hydrocarbon group or the like, and at least a pair mutually adjacent two groups chosen from R 1 -R 5 and R 8 -R 12 may be jointed to form a ring. However, at least one of R 1 , R 2 , R 3 , R 4 , R 5 , R 8 , R 9 , R 10 , R 11 , and R 12 denotes a fluorine atom. R 13 and R 14 each independently denote a hydrogen atom, halogen atom, hydrocarbon group or the like, and R 13 and R 14 may be jointed to form a ring. M denotes Ti, Zr or Hf; Y denotes a carbon atom or silicon atom; and Q denotes a halogen atom, hydrocarbon group, at most 10C neutral conjugated or nonconjugated diene, anion ligand or neutral ligand in which coordination is possible by a lone electron pair. j denotes an integer of 1-4, and two or more Q may be the same or different mutually when j is two or more. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种在聚合烯烃如丙烯时可以工业化的高温条件下聚合物具有完全宽分子量分布和高熔点的聚合物的方法。解决方案：制备烯烃聚合物的方法的特征在于，至少一种选自两个或多个碳数α-烯烃的单体在至少40℃下在含有（A ）由式[1]表示的交联茂金属化合物和（B）选自（b-1）有机铝氧化合物等的化合物。 R“SP”12各自独立地表示氢原子，卤素原子，烃基等，以及至少一对相互相邻的两个选自R“ 1 -R 5 和R 8 -R 12 可以连接形成环。然而，R 1 ，R 2 ，R 3 ，R 4 ，R 5 ，R 8 ，R 9 ，R 10 ，R SP SP 11， > 12 表示氟原子。 R 13和R 14各自独立地表示氢原子，卤素原子，烃基等，R 13和R 14均为氢， 14 可以连接成环。 M表示Ti，Zr或Hf; Y表示碳原子或硅原子; Q表示卤素原子，烃基，至多10个中性共轭或非共轭二烯，阴离子配位体或中性配体，其中可通过单电子对进行配位。 j表示1-4的整数，当j为2以上时，两个以上的Q可以相同或不同。版权所有（C）2011，JPO＆INPIT

8. 发明专利

JP2010174254A Automobile part obtained by injection-molding polypropylene resin composition 有权
标题翻译：通过注塑成型聚丙烯树脂组合物获得的汽车部件
公开(公告)号：JP2010174254A
公开(公告)日：2010-08-12
申请号：JP2010087077
申请日：2010-04-05
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： KAWAI KOJI , YAMASHITA MASAHIRO , DOI YASUSHI , ITAKURA KEITA , SAKAI IKUNORI , HASHIMOTO MIKIO , MINODA TAKESHI , NAITO MASAMICHI , TAKAOKA TORU , KAWAHARA NOBUO , KANEYOSHI HIROMU
IPC分类号： C08L23/12 , C08F110/06 , C08J5/00 , C08K3/00 , C08L23/08 , C08L23/14 , C08L23/16 , C08L53/00 , C08L53/02 , C08L101/00
CPC分类号： C08L53/00 , C08F110/06 , C08L23/12 , C08L23/16 , C08L53/025 , C08L2666/04 , C08L2666/02 , C08L2666/24 , C08F2500/03 , C08F2500/12
摘要： PROBLEM TO BE SOLVED: To provide automobile parts excellent in balance of stiffness and impact resistance, in particular, injection-molded automobile parts. SOLUTION: The injection-molded automobile parts are composed of a polypropylene resin composition comprising a propylene homopolymer (A1), an elastomer (B) and an inorganic filler (C), or a propylene-based block copolymer (A2) and (C) the inorganic filler and if necessary, the elastomer (B). The polypropylene homopolymer (A1) or the propylene-based block copolymer (A2) exhibits the following characteristics (i)-(iii): (i) an MFR (230°C) of 20 to 300 g/10 min; (ii) a 0.2% or less of a ratio of position irregular units derived from 2,1-insertion or 1,3-insertion of propylene monomer relative to all propylene structural units, determined from a 13 C-NMR spectrum; and (iii) an Mw/Mn of 1 to 3. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供刚性和抗冲击性的平衡优异的汽车部件，特别是注射成型的汽车部件。注塑汽车部件由包含丙烯均聚物（A1），弹性体（B）和无机填料（C）的聚丙烯树脂组合物或丙烯类嵌段共聚物（A2）和（C）无机填料，如有必要，弹性体（B）。聚丙烯均聚物（A1）或丙烯类嵌段共聚物（A2）具有以下特性（i） - （iii）：（i）20-300g / 10min的MFR（230℃）（ii）相对于所有丙烯结构单元，衍生自丙烯单体的2,1-插入或1,3-插入的位置不规则单元的比例为0.2％或更小，由 C -NMR光谱; （iii）Mw / Mn为1〜3。版权所有（C）2010，JPO＆INPIT

9. 发明专利

JP2010120878A Method for producing fluorene derivative 有权
标题翻译：生产氟代衍生物的方法
公开(公告)号：JP2010120878A
公开(公告)日：2010-06-03
申请号：JP2008295828
申请日：2008-11-19
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： YAMADA KO , YUKITA TAKASHI , YAMASHITA MASAHIRO , KANEYOSHI HIROMU
IPC分类号： C07C1/32 , B01J31/04 , B01J31/24 , C07B61/00 , C07C15/60 , C07C17/263 , C07C22/08 , C07C25/22 , C07C41/30 , C07C43/205
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a fluorene derivative in excellent reactivity with good yield. SOLUTION: The method for producing the fluorene derivative is the one for producing a specific fluorene derivative by reacting a specified fluorene compound (A) with a specific boron compound (B) in the presence of a base (C), and includes carrying out the reaction in a water-containing solvent (F) by using a phosphorus compound (D) represented by formula [6] and a palladium compound (E) as catalysts. COPYRIGHT: (C)2010,JPO&INPIT

10. 发明专利

JP2010047628A Manufacturing method for olefin polymer by highly active catalyst 审中-公开
标题翻译：通过高活性催化剂制备烯烃聚合物的制备方法
公开(公告)号：JP2010047628A
公开(公告)日：2010-03-04
申请号：JP2008210481
申请日：2008-08-19
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： YAMASHITA MASAHIRO , YUKITA TAKASHI , NAKAMURA TATSUYA
IPC分类号： C08F4/6592
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method for an olefin polymer using a polymerization catalyst being excellent in polymerization activity, indicating a high melting point and a high molecular weight by the obtained polymer and capable of performing polymerization at a high temperature.
SOLUTION: In the manufacturing method for the olefin polymer, 2C or more α-olefin is polymerized in the presence of the catalyst containing a crosslinked metallocene compound (A) represented by general formula [1]: and compound (B) selected from an organic aluminumoxy compound (b-1), etc. (wherein M is Ti, Zr or Hf).
COPYRIGHT: (C)2010,JPO&INPIT

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