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21. 发明专利

JPH04120014A COMPOSITION FOR ORAL CAVITY 失效
公开(公告)号：JPH04120014A
公开(公告)日：1992-04-21
申请号：JP24040990
申请日：1990-09-10
申请人： KAO CORP
发明人： OSHINO KAZUSHI , NAKAI RYOZO , TSUJITA SATOSHI , YOSHINO KOJI , KAWAMATA AKIRA
IPC分类号： A61K8/00 , A61K8/89 , A61K8/891 , A61Q11/00 , C08G77/392 , C08L83/08
摘要： PURPOSE:To obtain a composition for oral cavity useful for preventing dental caries and periodontosis, having excellent inhibitory effects on formation of bacterial plaque, containing a silicone derivative having automatically film- forming ability on the surface of teeth. CONSTITUTION:A composition for oral cavity containing 0.01-30wt.% silicone derivative shown by formula I, formula II or formula III (X is 1-10C alkylene; Y is COOH, o-PO3H2, SO3H, salt thereof or -N (CH3)3 Cl ; m and an are positive integer). The composition is properly mixed with an abradant, a binder, a foaming agent, a purified oil, a perfume, a sweetener, an antiseptic, etc., used for a composition for oral cavity and prepared by a conventional procedure to give the objective substance. The substance made into a form such as toothpaste, tooth powder, liquid dentifrice, mouthwash, tablet for gargling, gingiva massaging cream, chewing gum, troche or paste for oral cavity. The compound shown by formula I or formula II has a ratio of man of 1/100-100/1.

22. 发明专利

JPH04112813A HAIR-TREATMENT AGENT COMPOSITION 失效
公开(公告)号：JPH04112813A
公开(公告)日：1992-04-14
申请号：JP23299790
申请日：1990-09-03
申请人： KAO CORP
发明人： KAWASE JIRO , OGURA YOSHIKO , YOSHINO KOJI , KAWAMATA AKIRA
IPC分类号： A61K8/00 , A61K8/40 , A61K8/41 , A61K8/89 , A61K8/891 , A61Q5/00 , C08L83/08
摘要： PURPOSE:To provide the subject hair-treatment agent composition containing a silicone modified with a cyclic Bunte salt, used by adjusting pH to a prescribed value when the composition is used and capable of giving a split hair- preventing effect and luster over a long period. CONSTITUTION:A silicone modified with a cyclic Bunte salt of formula I (X is alkaline metal, alkaline earth metal, ammonia, amine or quaternary ammonium salt; n is 4-10; m is 3-11) is used in an amount of 0.01-50wt.%. A compound preferably represented by formula II or III (R is H, 1-4C alkyl, etc.; Y is H or OH; p, q or r is 0-5; R3 is 8-18C alkyl) is mixed therein in an amount of 0.1-50wt.% and a commonly used polymer compound, an oil component, polyhydric alcohol, a perfume, a pigment, a germicide, an ultraviolet absorber, etc., are mixed therewith as necessary, thus giving the objective composition. When the composition is used, pH of the composition is adjusted to 2-4 using circuit acid, etc., or to 8-11 using an alkaline solution. This composition can be applied to a shampoo, a rinse, a treatment, a styling, a permanent wave treatment, a hair color, a bleaching agent, etc.

23. 发明专利

JPH04108795A NEW SILOXANE DERIVATIVE, ITS PRODUCTION THEREOF AND COSMETIC CONTAINING THE SAME DERIVATIVE 失效
公开(公告)号：JPH04108795A
公开(公告)日：1992-04-09
申请号：JP22895890
申请日：1990-08-30
申请人： KAO CORP
发明人： TAKEUCHI MASARU , YOSHINO KOJI , SUZUKI YUJI , KAWAMATA AKIRA
IPC分类号： A61K8/63 , A61K8/72 , A61K8/89 , A61Q1/00 , A61Q1/12 , B01F17/54 , C07F7/18 , C08G77/14 , C08G77/22 , C08G77/38 , C08L83/06
摘要： NEW MATERIAL:A compound expressed by formula I [at least one of R to R is a group expressed by formula II (Q is 3-20C bifunctional hydrocarbon; R and R are H or 1-5C hydrocarbon with a proviso that one is H) and the residual is hydrocarbon or group expressed by formula III (X is bifunctional hydrocarbon containing ether bonding or ester bonding; R is 1-30C hydrocarbon); (l), (m) and (n) are 0-2000, at least one of R to R and R to R is expressed by formula II for l+m+n=0, with removing a case that one of the R to R is expressed by formula II in which Q is trimethylene and R and R are simultaneously H and whole of the residual is methyl]. EXAMPLE:3-(3-hexyl-1,1,3,3-tetramethyl disiloxanyl) propyl glyceryl ether. USE:Useful as an emulsifier for cosmetics, etc. PREPARATION:Organohydrogen polysiloxane expressed by formula IV (at least one of R to R is H and residual is 1-30C hydrocarbon) is made to react with alkenyl glyceryl ether expressed by formula V (Q' is 3-20C hydrocarbon having double bond).

24. 发明专利

JPH03263431A SILICON-CONTAINING DENDRIMER 失效
公开(公告)号：JPH03263431A
公开(公告)日：1991-11-22
申请号：JP6224990
申请日：1990-03-13
申请人： KAO CORP
发明人： UCHIDA HIROAKI , KABE YOSHIO , YOSHINO KOJI
IPC分类号： C08G77/44 , C08G77/42
摘要： PURPOSE:To provide the subject dendrimer having silicon-containing functional groups and a large functional group density per molecular units, capable of having a space therein when several generations are overlapped, having physical properties characteristic to silicon compounds and useful as a gelling agent, etc. CONSTITUTION:A dendrimer of the formula [X Y (Z )Ni is the same in one generation; X Y (Z )Nt is the same; I is multifunctional nucleus; Z is a functional group bonded to the nucleus and the first generation X group; Nc is the number of functional groups bonded to the nucleus; X is an i generation repeating unit functional group bonded to Y and (i+1) generation X group; Ni is at least two corresponding to the number of multifunctional head portions of Y ; N is at least two corresponding to the number of multifunctional head portions of Y ; X is the monofunctional tail portion of the final generation repeating unit Y ; Z is an end group bonded to Y ; Nt is an end group bonded to Y ; Nt is the number of Z groups; i is the number of specific generations continued from 1 to t-1; either one of I-Z is a Si-containing functional group].

25. 发明专利

JPH0390089A NEW CYCLIC ORGANOPOLYSILOXANE AND PRODUCTION THEREOF 失效
公开(公告)号：JPH0390089A
公开(公告)日：1991-04-16
申请号：JP22621389
申请日：1989-08-31
申请人： KAO CORP
发明人： UCHIDA HIROAKI , KABE YOSHIO , YOSHINO KOJI
IPC分类号： C07F7/08 , C07F7/21 , C08G77/38
摘要： NEW MATERIAL:Compounds of formula I (R -R are each alkyl, alkenyl, aryl or halogenated alkyl; n is 7-9). EXAMPLE:Pentadecamethylcyclooctasiloxane. USE:A silylation agent and a raw material of a silicone oil and a silicone rubber. PREPARATION:Palladium carbon is acted on an alpha,omega-dihydrodieneorganopolysiloxane represented by formula II (m is 5-7) to obtain an alpha,omega- dihydroxyorganopolysiloxane shown by formula III. With the resultant compound dichlorosilane expressed by formula IV is then reacted.

26. 发明专利

JP2000191603A FLUORINE CONTAINING ALKYL CARBONATE 失效
公开(公告)号：JP2000191603A
公开(公告)日：2000-07-11
申请号：JP37066098
申请日：1998-12-25
申请人： KAO CORP
发明人： MIZOOKU TAKASHI , YOSHINO KOJI , YANO SHINJI
IPC分类号： A61K8/30 , A61K8/00 , A61K8/04 , A61Q1/00 , A61Q1/02 , A61Q1/04 , A61Q1/06 , A61Q1/10 , A61Q1/12 , A61Q5/00 , C07C68/02 , C07C69/96 , A61K7/00 , A61K7/021 , A61K7/027 , A61K7/035 , A61K7/06
摘要： PROBLEM TO BE SOLVED: To obtain a fluorine containing alkyl carbonate having characteristic properties such as water repellency, oil repellency or the like and excellent in compatibility with other materials, solubility in various solvents, adhesion to hair and skin, useful as a wax base. SOLUTION: This compound is expressed by formula I [Rf is a 1-20C perfluoroalkyl, ω-H-perfluoro alkyl expressed by formula H(CF2)k (k is 1-20); n is 2-8; R is a natural sterol, residue of hydrogenated sterol excluding OH group], for example, cholesteryl 2-(perfluorohexyl)ethyl carbonate. The prescribed compound is obtained by reacting chloroformate ester of the sterol with fluorine containing alcohol in a solvent practically free from water and alcohol (e.g.; chloroform or the like), in the presence of a basic substance such as pyridine or the like, at a reaction temperature of -10-40 deg.C, for 1-3 hours.

27. 发明专利

JPH10168044A NEW AMINOCARBOXYLIC ACID ESTER SALT DERIVATIVE 失效
公开(公告)号：JPH10168044A
公开(公告)日：1998-06-23
申请号：JP32972996
申请日：1996-12-10
申请人： KAO CORP
发明人： YOSHINO KOJI , SUGAI YOSHIYA , YAMAMURO AKIRA
IPC分类号： C07C227/18 , C07C227/22 , C07C229/08 , C07C303/24 , C07C305/06
摘要： PROBLEM TO BE SOLVED: To obtain a new aminocarobxylic acid ester salt derivative that is liquid in room temperature and useful as an intermediate for production of amidocarboxylic acids. SOLUTION: This aminocarboxylic acid ester derivative of formula I [R and R are each H or a 1-6C straight chain alkyl; R is a 2-40C alkyl; (OR ) is an ester from which one H ion is eliminated; -AO is a moiety of a divalent or trivalent acid from which one H ion is eliminated; (n) is 1-16; (m) is 0-1], for example, 12-aminododecanoic isobutyl ester-hyudrosulfate-isobutyl sulfate, is obtained by reacting an aminocarboxylic acid of formula II or a cyclic lactam of formula III with a 2-40C monohydric alcohol (R OH) in the presence of a divalent or trivalent inorganic acid (AOH) at temperature in the range of room temperature to 200 deg.C, and distilling off unreacted alcohol.

28. 发明专利

JPH09278732A AMIDE DERIVATIVE AND AGENT COMPOSITION FOR EXTERNAL USE CONTAINING THE SAME 失效
公开(公告)号：JPH09278732A
公开(公告)日：1997-10-28
申请号：JP23643196
申请日：1996-09-06
申请人： KAO CORP
发明人： SUGAI YOSHIYA , YOSHINO KOJI , YAMAMURO AKIRA , ARAI YOICHI , MEGURO SHINICHI
IPC分类号： A61K8/30 , A61K8/00 , A61K8/42 , A61Q19/00 , C07C235/08 , C07C237/22 , A61K7/00 , A61K7/48
摘要： PROBLEM TO BE SOLVED: To obtain a new amide derivative expressed by specific formula, having effect of essentially improving (maintaining, reinforcing) the horny layer barrier function, good in the solubility and stability to basal agent, and useful as e.g. a preparation for external use for skin. SOLUTION: This new amide derivative is expressed by formula I [R is a 1-40C hydrocarbon; R is a 1-6C alkylene; R is H, hydroxyl or a (substituted) 1-12C alkoxy; R is a 1-39C divalent hydrocarbon; R is formula II (R is H or a 1-6C hydrocarbon; R is a 1-40C hydrocarbon), etc.]. The compound is obtained, pref. for example, by reaction of (A) an aminoalcohol derivative of formula III prepared from (i) glycidyl ether and (ii) an amine with (B) an amidocarboxylic acid derivative of formula IV prepared from (iii) an aminocorboxylic acid derivative and (iv) a carboxylic acid derivative or an acid chloride, in the presence of a dehydrating agent or a base catalyst.

29. 发明专利

JPH09208513A PRODUCTION OF ALLYL PERFLUOROALKYL ETHER 失效
公开(公告)号：JPH09208513A
公开(公告)日：1997-08-12
申请号：JP1391696
申请日：1996-01-30
申请人： KAO CORP
发明人： SUGIYAMA MITSURU , OKADA JOJI , YOSHINO KOJI , YAMAMURO AKIRA , NAKAMURA KOICHI
IPC分类号： B01J23/04 , C07B61/00 , C07C41/16 , C07C43/17
摘要： PROBLEM TO BE SOLVED: To produce a high-purity allyl perfluoroalkyl ether useful as an intermediate for producing surfactants and oilproof and waterproof treating agents in high yield in a short time without causing wastes. SOLUTION: A perfluoroalkyl alcohol represented by the formula Rf -(CH2 )n - OH [Rf is a perfluoroalkyl; (n) is a number of 1-12] (e.g. 2,2,2-trifluoroethanol) is reacted with an allyl halide (e.g. allyl chloride) in the presence of a solid alkali (NaOH having 0.01-1mm particle diameter) without using a solvent to afford an allyl perfluoroalkyl ether represented by the formula Rf -(CH2 )n -O-CH2 - CH=CH2 , e.g. allyl ((perfluorooctyl)ethyl) ether.

30. 发明专利

JPH0987157A OILY SOLID COSMETIC 失效
公开(公告)号：JPH0987157A
公开(公告)日：1997-03-31
申请号：JP24205295
申请日：1995-09-20
申请人： KAO CORP
发明人： SHIMIZU MOMOKO , DAIJIMA KAZUHIKO , YOSHINO KOJI
IPC分类号： A61K8/30 , A61K8/00 , A61K8/72 , A61K8/89 , A61K8/92 , A61Q1/00 , A61Q1/10 , A61Q1/12 , A61Q19/00 , C08L83/08 , C08L83/12 , A61K7/48 , A61K7/00
摘要： PROBLEM TO BE SOLVED: To obtain an oily solid cosmetic excellent in any of feeling to user, finishing property and makeup adhesiveness. SOLUTION: This oily solid cosmetic contains (A) 0.5-50wt.% of a modified organopolysiloxane compound of the formula [R is a 1-18C hydrocarbon; R is a 2-16C hydrocarbon; Rf ' is a 1-20C perfluoroalkyl; (m) is 2-16; (n) is 1-6; (x) 0-50], etc., having perfluoroalkyl and polyoxyalkylene at side chain, (B) 1-90wt.% solid, simi-solid or liquid oily raw material (e.g. paraffin wax or squalane) and (C) 1-95wt.% powder for cosmetic (e.g. pigment). The cosmetic is prepared by blending these components with surfactant, ingredient having pharmacodynamic effects, other oily raw materials, antiseptic, antioxidant, humectant, ultrabviolet light absorber, perfume, etc., and heating, mixing and stirring the mixture. The cosmetic can be prepared in makeup cosmetic such as lipstick, foundation, eye shadow or eye liner.

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