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141. 发明专利

JPS5754197A Preparation of d-ribose 失效
标题翻译：空值
公开(公告)号：JPS5754197A
公开(公告)日：1982-03-31
申请号：JP12914280
申请日：1980-09-19
申请人： Towa Kasei Kogyo Kk
发明人： EBISU TAKASHI , TATENO YOSHIAKI , TAKEUCHI HIROSUKE , KATAURA KOICHI , TAKESAWA MASAHIRO , FUSE MASAAKI
IPC分类号： C07H3/02
摘要： PURPOSE: To obtain the titled compound useful as a raw material for a nucleic acid seasoning, etc. industrially and advantageously, by epimerizing an aqueous solution of D-arabinose in the presence of molybdenum ions under heating, and separating the reaction solution with a muitivaient metallic cation exchanger column.
CONSTITUTION: An aqueous solution of D-arabinose is subjected to the epimerization in the presence of molydbenum ions, e.g. anion exchanger fibers supporting the molybdenum ions, under heating and filtered. The resultant filtrate is then desalted with an ion exchange resin to give a transparent aqueous solution containing a mixture of D-ribose with pentose. The resultant aqueous solution is then passed through a column of a di- or trivalent metallic cation exchanger, e.g. an ion exchanger prepared by treating a polyvinylsulfonic acid type cation exchange resin with an aqueous solution of calcium chloride, to separate D-arabinose (I), D- ribose (II) and D-xylose and D-lyxose (III).
COPYRIGHT: (C)1982,JPO&Japio
摘要翻译：目的：通过加热在钼离子的存在下，通过差异化D-阿拉伯糖的水溶液，得到可用作核酸调味料的原料的标题化合物，并将其与亲和剂分离金属阳离子交换柱。构成：D-阿拉伯糖的水溶液在钼离子存在下进行差向异构化，例如，负载钼离子的阴离子交换纤维，加热过滤。然后将所得滤液用离子交换树脂脱盐，得到含有D-核糖与戊糖的混合物的透明水溶液。然后将所得水溶液通过二价或三价金属阳离子交换剂的柱，例如通过用氯化钙水溶液处理聚乙烯磺酸型阳离子交换树脂来分离D-阿拉伯糖（I），D-核糖（II）和D-木糖和D-赖索糖（III）制备的离子交换剂。

142. 发明专利

JPS5576894A EPIMERIZATION OF ALDOSE 失效
公开(公告)号：JPS5576894A
公开(公告)日：1980-06-10
申请号：JP14968778
申请日：1978-12-05
申请人： MITSUBISHI RAYON CO , TOWA KASEI KOGYO KK
发明人： TAKEMURA MOTOHIRO , EBISU TAKASHI , TATENO YOSHIAKI
IPC分类号： C07H3/02
摘要： PURPOSE:The epimerization of aldoses is effected by heating an aqueous aldose in the presence of a molybdenic acid catalyst supported on anion exchange fibers, thus producing epimerized isomers with industrial advantage because the catalyst- removing process becomes unncessary and the catalyst activity is maintained. CONSTITUTION:An aldose as D-xylose is heated at a temperature higher than 70 deg.C in the presence of a catalyst of (C) molybdenic acid supported on (B) anion exchange fibers, which are prepared by impregnating polyethylene fibers with vinylbenzyl chloride and divinylbenzene, polymerizing them and introducing tertiary amino groups to give the objective epimerized isomer. For example, D-xylose is continuously made to react, thus giving D-lyxose. The concentration of the aldose used is 40-80% and the anion exchange fibers preferably have less than 200 micron diameter and 3-5000 aspect ratio.

143. 发明专利

JP2967491B2 失效
公开(公告)号：JP2967491B2
公开(公告)日：1999-10-25
申请号：JP5988990
申请日：1990-03-13
申请人： TOWA KASEI KOGYO KK
发明人： YAMAMOTO YASUHIRO , KANEKO YOSHIKIMI , KATO KAZUAKI
IPC分类号： A23L17/00 , A23B4/20 , A23L5/41 , A23L1/325

144. 发明专利

JP2920434B2 失效
公开(公告)号：JP2920434B2
公开(公告)日：1999-07-19
申请号：JP17471291
申请日：1991-06-20
申请人： TOWA KASEI KOGYO KK
发明人： TAKASE SACHIKO , AIDA TOSHIHISA
IPC分类号： A23L1/304 , A23L1/308

145. 发明专利

JP2855285B2 失效
公开(公告)号：JP2855285B2
公开(公告)日：1999-02-10
申请号：JP12902890
申请日：1990-05-21
申请人： TOWA KASEI KOGYO KK
发明人： KANEKO YOSHIKIMI , OKAMOTO NAOKI
IPC分类号： A21D2/14 , A21D13/00

146. 发明专利

JP2845386B2 失效
公开(公告)号：JP2845386B2
公开(公告)日：1999-01-13
申请号：JP3691292
申请日：1992-01-29
申请人： NORINSUISANSHO SHOKUHIN SOGO KENKYUSHOCHO , TOWA KASEI KOGYO KK
发明人： KOBAYASHI SHOICHI , YAMAZAKI MASAYOSHI
IPC分类号： C08B37/16 , C12P19/16 , C12P19/20

147. 发明专利

JP2562334B2 失效
公开(公告)号：JP2562334B2
公开(公告)日：1996-12-11
申请号：JP27480087
申请日：1987-10-30
申请人： TOWA KASEI KOGYO KK
发明人： SHIMAZU KOSHIRO , KAWASHIMA SHIGERU , ISHII YOSHIFUMI
IPC分类号： A23L17/60 , A23L27/10 , A23L1/337 , A23L1/221

148. 发明专利

JP2537401B2 失效
公开(公告)号：JP2537401B2
公开(公告)日：1996-09-25
申请号：JP8799189
申请日：1989-04-10
申请人： TOWA KASEI KOGYO KK
发明人： TATENO YOSHIAKI , YONEDA SUSUMU , OKAMOTO NAOKI , ISHII YOSHIFUMI , KATO KAZUAKI
IPC分类号： C07C29/80 , C07C29/76 , C07C31/27

149. 发明专利

JP2521083B2 失效
公开(公告)号：JP2521083B2
公开(公告)日：1996-07-31
申请号：JP6784687
申请日：1987-03-24
申请人： TOWA KASEI KOGYO KK
发明人： MAEDA MASAYUKI , HARADA NAOKI , SEKIGUCHI MASAYUKI
IPC分类号： C08B37/00 , A61K31/715 , A61K36/02 , A61K36/05 , A61K38/00 , A61P7/02 , A61K31/725 , A61K35/80

150. 发明专利

JPH06192146A PRODUCTION OF 1,4-CYCLOHEXANEDIMETHANOL 失效
公开(公告)号：JPH06192146A
公开(公告)日：1994-07-12
申请号：JP35787192
申请日：1992-12-25
申请人： TOWA KASEI KOGYO KK
发明人： MAGARA MITSUO , ONODA YOSHIMI , YAMAZAKI FUMITO , YONEDA SUSUMU , KATO KAZUAKI
IPC分类号： B01J23/46 , B01J23/86 , C07B61/00 , C07C29/149 , C07C29/19 , C07C31/135 , C07C31/27
摘要： PURPOSE:To enable adoption of a ruthenium catalyst more inexpensive than palladium, to make it possible to carry out hydrogenation reaction of the first stage under a milder condition than the conventional method, in order to produce 1,4-cyclohexanedimethanol more economically and advantageously. CONSTITUTION:1,4-Cyclohexanedimethanol is produced successively through the first process wherein hydrogen is introduced to a stationary bed continuous type hydrogenation device packed with a hydrogenating catalyst of ruthenium, simultaneously the first raw material and the first-stage hydrogenation reactional product are fed to the device, the hydrogenation reaction of the first stage is carried out and the reactional product and excessive hydrogen are discharged from the device and the second process wherein hydrogen is introduced to a stationary bed continuous type hydrogenation device packed with a hydrogenating catalyst of copper chromite, simultaneously the second raw material and the first-stage hydrogenation reactional product are fed to the device, the second- stage hydrogenation reaction is carried out and the reactional product and excessive hydrogen are removed from the device.

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