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1. 发明公开

EP2970068A4 PROCESS AND SYSTEMS FOR OBTAINING 1,4-BUTANEDIOL FROM FERMENTATION BROTHS 有权
标题翻译：用于从发酵剂生产1,4-硼烷的方法和系统
公开(公告)号：EP2970068A4
公开(公告)日：2016-12-21
申请号：EP14768022
申请日：2014-03-14
申请人： GENOMATICA INC
发明人： GARIKIPATI SVB JANARDHAN , JAPS MICHAEL , SONICO ISHMAEL M
IPC分类号： C07C29/76 , B01D1/00 , B01D3/00 , C07C29/74 , C07C29/80 , C07C29/90 , C07C33/046
CPC分类号： C07C29/80 , B01D1/22 , B01D3/002 , B01D3/143 , C07C29/00 , C07C29/74 , C07C29/90 , C07C31/207 , C12P7/18 , C07C33/046
摘要： A process of purifying 1,4-butanediol (1,4-BDO) from a fermentation broth including separating solid materials, salts and water, and subjecting the resulting material to a two, three or four column distillation system, that can include a wiped film evaporator to produce a purified 1,4-butanediol product.

2. 发明公开

EP1926695A1 VERFAHREN ZUR ABTRENNUNG VON POLYMEREN NEBENPRODUKTEN AUS 1,4-BUTINDIOL 有权
标题翻译：制备聚合物副产品从1,4-丁炔二醇的分离
公开(公告)号：EP1926695A1
公开(公告)日：2008-06-04
申请号：EP06778324.1
申请日：2006-08-23
申请人： BASF SE
发明人： LORENZ, Rudolf, Erich , PINKOS, Rolf , STEINIGER, Michael , SCHÄFER, Gerd , DANNER, Thomas
IPC分类号： C07C29/17 , C07C29/76 , C07C31/20 , C07C33/035 , C07C33/046
CPC分类号： C07C29/76 , C07C29/17 , C07C29/172 , C07C33/046 , C07C33/035 , C07C31/207
摘要： The invention relates to a method for purifying 1,4-butynediol, in which 1,4-butynediol is compressed to 50 to 1500 bar and is expanded, one waits for phase separation to end following the expansion process, and the bottom phase is eliminated. Also disclosed is a method for hydrogenating 1,4-butynediol into 1,4-butenediol and 1,4-butanediol with the aid of the purified 1,4-butynediol.

3. 发明公开

EP1055655A3 Verfahren zur Herstellung von Alkindiolen 有权
标题翻译：一种制备炔二醇过程
公开(公告)号：EP1055655A3
公开(公告)日：2004-03-10
申请号：EP00110914.9
申请日：2000-05-24
申请人： BASF AKTIENGESELLSCHAFT
发明人： Kindler, Alois, Dr. , Preiss, Thomas, Dr. , Henkelmann. Jochem, Dr.
IPC分类号： C07C29/42 , C07C33/044
CPC分类号： C07C29/42 , C07C33/044 , C07C33/046
摘要： Das Verfahren zur Herstellung von Alkindiolen der allgemeinen Formel (I)R 1 R 2 C(OH)-C≡C-C(OH)R 1 R 2 mit der Bedeutung R 1 , R 2 unabhängig H oder C 1-20 -Kohlenwasserstoffrest, der ein- oder mehrfach durch C 1-6 -Alkyl substituiert und/oder von nicht benachbarten Heteroatomen unterbrochen sein und/oder C-C-Doppel- oder Dreifachbindungen enthalten kann, durch Umsetzung von Verbindungen der allgemeinen Formel (II)R 1 -C(=O)-R 2 mit Acetylen in einem polar aprotischen Lösungsmittel wird in Gegenwart von basischen Alkalimetallsalzen als Katalysatoren durchgeführt.

4. 发明授权

EP0309915B1 Verfahren zur Entfernung von Formaldehyd aus wässrigen Lösungen von 2-Butindiol-1,4 失效
标题翻译：从2-Y-1,4-二醇的水溶液中除去甲醛的方法
公开(公告)号：EP0309915B1
公开(公告)日：1991-10-16
申请号：EP88115571.7
申请日：1988-09-22
申请人： BASF Aktiengesellschaft
发明人： Merger, Franz, Dr. , Horler, Hans, Dr.
IPC分类号： C07C33/046 , C07C29/88
CPC分类号： C07C33/046 , C07C29/88

5. 发明公开

EP0164977A3 Agglomerates of malachite crystals and method for their preparation 失效
标题翻译： MALACHITE晶体的组成及其制备方法
公开(公告)号：EP0164977A3
公开(公告)日：1989-01-04
申请号：EP85303879.2
申请日：1985-06-03
申请人： E.I. DU PONT DE NEMOURS AND COMPANY
发明人： Fremont, Joseph Melvin
IPC分类号： C01G3/00 , C07C33/046 , B01J31/28
CPC分类号： B01J27/20 , B01J23/8437 , C07C33/046
摘要： Agglomerates of spheroidal masses of malachite crystals are prepared so that they contain silicic acid. These agglomerates can be used to prepare a copper-acetylide _ complex, which in turn can be used as a catalyst for the preparation of 1, 4-butynediol from acetylene and formaldehyde.

6. 发明公开

EP2969208A1 NOVEL ETHYNYLATION CATALYST AND METHOD OF MAKING SAME 审中-公开
标题翻译：新型乙炔化催化剂及其制备方法
公开(公告)号：EP2969208A1
公开(公告)日：2016-01-20
申请号：EP14769664.5
申请日：2014-03-11
申请人： BASF Corporation
发明人： MADON, Rostam , NAGEL, Peter , HEDRICK, Scott , THAKUR, Deepak
IPC分类号： B01J37/02 , B01J23/72
CPC分类号： B01J23/8437 , B01J21/10 , B01J23/72 , B01J35/0006 , B01J35/008 , B01J35/023 , B01J35/026 , B01J37/035 , B01J37/06 , B01J37/08 , B01J2523/00 , C07C29/42 , C07C33/046 , B01J2523/12 , B01J2523/17 , B01J2523/22 , B01J2523/31 , B01J2523/41 , B01J2523/54
摘要： A novel catalyst useful in the ethynylation of formaldehyde to butynediol is formed by precipitating copper and bismuth from a salt solution of such metals, utilizing an alkali metal hydroxide as the precipitating agent to deposit copper and bismuth hydroxide as a coating around a siliceous carrier particle.
摘要翻译：通过使用碱金属氢氧化物作为沉淀剂沉淀铜和氢氧化铋作为围绕硅质载体颗粒的涂层，通过从这些金属的盐溶液中沉淀铜和铋来形成用于甲醛乙炔化成丁炔二醇的新型催化剂。

7. 发明公开

EP2785672A1 CAUSTIC TREATMENT OF FORMALDEHYDE RECYCLE COLUMN FEED 有权
标题翻译：甲醛再循环塔潮蚀处理
公开(公告)号：EP2785672A1
公开(公告)日：2014-10-08
申请号：EP12766786.3
申请日：2012-09-13
申请人： Invista Technologies S.à.r.l.
发明人： BADAT, Hashim, M. , GAUSE, Jason, C.
IPC分类号： C07C29/80 , C07C29/88 , C07C33/046
CPC分类号： C07C29/80 , C07C29/88 , C07C33/046
摘要： An improved method for removing formaldehyde from a crude butynediol product stream comprising the step of providing a crude butynediol stream containing butynediol and formaldehyde. A pH control agent is then mixed with the crude butynediol stream to form a treated product stream, wherein the pH of the treated product stream is raised to a level that limits the reaction of butynediol and formaldehyde to form acetal complex and decrease the solubility of trace metals. The treated product stream then flows into the inlet of a continuous distillation column. Finally, a concentrated formaldehyde stream from the overhead stream of the distillation column and a concentrated butynediol stream from the distillation bottoms stream that is essentially free of formaldehyde and acetal complex are both recovered.

8. 发明授权

EP1055655B1 Verfahren zur Herstellung von Alkindiolen 有权
标题翻译：一种制备炔二醇过程
公开(公告)号：EP1055655B1
公开(公告)日：2006-06-14
申请号：EP00110914.9
申请日：2000-05-24
申请人： BASF Aktiengesellschaft
发明人： Kindler, Alois, Dr. , Preiss, Thomas, Dr. , Henkelmann. Jochem, Dr.
IPC分类号： C07C29/42 , C07C33/044
CPC分类号： C07C29/42 , C07C33/044 , C07C33/046

9. 发明授权

EP1035917B1 VERFAHREN ZUR HERSTELLUNG EINES KATALYSATORS UND NACH DIESEM VERFAHREN ERHÄLTLICHE KATALYSATOREN 有权
标题翻译：一种用于生产催化剂和这种方法获得的催化剂
公开(公告)号：EP1035917B1
公开(公告)日：2002-03-06
申请号：EP98961246.0
申请日：1998-12-01
申请人： BASF AKTIENGESELLSCHAFT
发明人： BÖTTCHER, Arnd , HENKELMANN, Jochem , PREISS, Thomas , BRUNNER, Melanie
IPC分类号： B01J31/22 , C07C33/042 , C07C209/60
CPC分类号： B01J31/1616 , B01J31/2286 , B01J2231/346 , B01J2531/10 , B01J2531/16 , B01J2531/20 , C07C29/42 , C07C209/60 , C07C213/00 , C07C211/23 , C07C215/24 , C07C33/042 , C07C33/046

10. 发明授权

EP0589977B1 VERFAHREN UND VORRICHTUNG ZUR SYNTHESE VON BUTINDIOL 失效
标题翻译：方法和设备合成丁炔二醇。
公开(公告)号：EP0589977B1
公开(公告)日：1995-03-01
申请号：EP92912341.2
申请日：1992-06-17
申请人： Linde Aktiengesellschaft , YUKONG LIMITED
发明人： WIESSNER, Frank
IPC分类号： C07C33/046 , C07C29/38
CPC分类号： C07C33/046 , C07C29/38 , Y02P20/584
摘要： Formaldehyde and acetylene are usually converted into butynediol in the presence of a suspension catalyst in a cascade of reactors. The catalyst is separated from the product solution after the last reactor in the cascade and fed back into the first reactor. Here, depending on the degree of thickening of the suspension, a considerable proportion of the butynediol produced must also be fed into the first reactor of the cascade. This greatly hinders the conversion reaction into butynediol. Moreover, there is the risk of damage to the catalyst by a lack of acetylene, especially in the lines and the device for separating the catalyst from the product solution. According to the invention, the separation takes place in each individual reactor. This can be done by filters fitted in the reactor or suitable filter apparatuses outside the reactor. In the process of the invention, part of the catalyst in the reactors can be drawn off and replaced by regenerated and/or fresh catalyst. The catalyst drawn off from the reactors can advantageously be subjected to a regeneration. The exchange of the catalyst in the reactor may be intermittent or continuous. A quantity of catalyst of 50 - 200 g, preferably 75 - 125 g, is used in the reactors per litre of reaction solution.

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