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1. 发明公开

EP3262142A1 EXTRACTIVE DISTILLATION FOR AROMATICS RECOVERY 有权转让
标题翻译：用于芳香剂回收的萃取蒸馏
公开(公告)号：EP3262142A1
公开(公告)日：2018-01-03
申请号：EP16708534.9
申请日：2016-02-12
申请人： Allnew Chemical Technology Company
发明人： LEE, Fu-Ming
IPC分类号： C10G21/28 , C10G7/08
CPC分类号： C07C7/08 , B01D3/143 , B01D3/40 , B01D5/006 , B01D5/009 , B01D11/0488 , B01D11/0492 , C07C15/02 , C10G21/16 , C10G21/27 , C10G21/28 , C10G2400/30
摘要： Extractive distillation for recovering aromatic hydrocarbons employs an extractive distillation column with a novel overhead system including a partial condenser. The process enables (i) efficient removal of heavy non-aromatics, particularly C8 naphthenic compounds, from the EDC bottom stream to increase the purity of aromatic products, especially of the mixed xylenes and (ii) reduction (or better control) of benzene loss to the raffinate product stream to maintain its quality as a gasoline blend stock and, as a result, enhance benzene recovery in the aromatic products. Feedstock includes a full-range feedstock, such as pyrolysis gasoline, or a narrow-range feedstock, such as reformate.

2. 发明授权

EP2409971B1 METHOD FOR SEPARATING HEXAFLUOROPROPYLENE OXIDE FROM HEXAFLUOROPROPYLENE 有权
标题翻译：从六氟丙烯中分离六氟环氧丙烷的方法
公开(公告)号：EP2409971B1
公开(公告)日：2017-05-10
申请号：EP10753360.6
申请日：2010-02-18
申请人： Daikin Industries, Ltd.
发明人： NAKAYA, Hideki , ICHIHARA, Kazuyoshi , SENBA, Yasuhide , NAKAGOSHI, Mikio , MORIMOTO, Kazunori
IPC分类号： C07D301/32 , C07C17/386 , C07C21/18 , C07D303/08 , B01D3/40
CPC分类号： C07C21/18 , B01D3/40 , C07C17/386 , C07D301/32 , C07D303/08

3. 发明公开

EP3082988A1 EXTRAKTIONSKOLONNE UND VERFAHREN ZUM EXTRAHIEREN EINES BESTANDTEILS AUS EINEM FLUID 审中-公开
标题翻译： VERFAHREN ZUM EXTRAHIEREN EINES BESTANDTEILA AUS EINEM FLUID EXTRAKTIONS KOLONNE
公开(公告)号：EP3082988A1
公开(公告)日：2016-10-26
申请号：EP14821589.0
申请日：2014-12-17
申请人： BASF SE
发明人： HAMMON, Ulrich , PFEIFFER, Daniel , WALTER, Jonathan
IPC分类号： B01D11/04 , B01D3/14 , B01D3/40
CPC分类号： C07C51/48 , B01D3/141 , B01D3/40 , B01D11/0426 , B01D11/043 , B01D2011/002
摘要： The present invention relates to an extraction column (1) comprising, at least in sections, a cylindrical, vertically orientated column body (2), said column body forming a hollow column space (3) having a maximum horizontal extension, wherein within the column body (2) are arranged at least one first inlet (4) for an extractant, at least one second inlet (5) for the fluid to be extracted, and at least one outlet (6) for the extractant mixture and at least one outlet for the raffinate. The extraction column (1) according to the invention is characterized in that a vertically oriented dividing device (7) is arranged within the hollow column space (3) that divides the hollow column space (3) into several vertically oriented and horizontally separated areas, wherein the maximum horizontal extent of each area is smaller than the maximum horizontal extent of the hollow column space (3). The invention further relates to a method for extracting a component from a fluid by means of such an extraction column (1).
摘要翻译：本发明涉及一种具有垂直排列的柱体2的抽取塔1，塔柱本体2至少是圆柱形的并且形成具有水平最大程度的柱形空腔3，在柱体2中设置有至少一个第一进料4，用于萃取剂，用于待萃取的流体的至少一个第二进料5和用于萃取混合物的至少一个出口6和用于萃余液的至少一个出口。在本发明的提取塔1中，布置在柱腔3内的垂直排列的分隔件7将柱腔3细分为多个垂直排列和水平分割的区域，每个区域的水平最大程度小于水平最大范围柱腔3.本发明还涉及通过这种提取塔1从流体中提取成分的方法。

4. 发明公开

EP2937329A1 METHOD FOR PRODUCING ACETIC ACID 有权
标题翻译：生产乙酸的方法
公开(公告)号：EP2937329A1
公开(公告)日：2015-10-28
申请号：EP13864464.6
申请日：2013-12-02
申请人： Daicel Corporation
发明人： SHIMIZU, Masahiko , SAITO, Ryuji , MIURA, Hiroyuki
IPC分类号： C07C51/12 , B01J31/16 , C07C51/44 , C07C53/08 , C07B61/00
CPC分类号： C07C51/12 , B01D3/40 , B01J31/16 , C07C51/44 , C07C53/08
摘要： A process for removing acetaldehyde efficiently and producing high-purity acetic acid stably is provided. Methanol is allowed to continuously react with carbon monoxide in a carbonylation reactor 1 in the presence of a catalyst system; the reaction mixture is continuously fed to a flasher 2 to form a volatile phase (2A) containing acetic acid and methyl iodide; the volatile phase (2A) is continuously fed to a splitter column 3 to form an overhead (3A) containing methyl iodide and acetaldehyde and a stream (3B) containing acetic acid; the volatile phase (2A) and/or the overhead (3A) is cooled by a first condenser C1, C3 at a predetermined cooling temperature; and the noncondensed gaseous component is further cooled by a second condenser C2, C4 to form a concentrate having a lower temperature and a higher acetaldehyde concentration. Acetaldehyde is efficiently removed by distilling the concentrate having a high acetaldehyde concentration.
摘要翻译：提供了一种有效去除乙醛并稳定生产高纯度乙酸的方法。使甲醇在催化剂体系存在下在羰基化反应器1中与一氧化碳连续反应; 将反应混合物连续加入闪蒸器2以形成含有乙酸和甲基碘的挥发相（2A）挥发相（2A）连续进料到分流塔3以形成含有甲基碘和乙醛的塔顶馏分（3A）和含有乙酸的物流（3B）; 在预定的冷却温度下，第一冷凝器C1，C3将挥发相（2A）和/或塔顶馏分（3A）冷却; 并且未冷凝的气体组分被第二冷凝器C2，C4进一步冷却以形成具有较低温度和较高乙醛浓度的浓缩物。通过蒸馏具有高乙醛浓度的浓缩物来有效地除去乙醛。

5. 发明公开

EP2928857A1 PROCESS FOR THE ISOLATION OF LEVULINIC ACID AND FORMIC ACID 有权转让
标题翻译： VERFAHREN ZUR ISOLIERUNG VONLÄVULINSÄUREUND AMEISENSURE
公开(公告)号：EP2928857A1
公开(公告)日：2015-10-14
申请号：EP13802369.2
申请日：2013-12-09
申请人： DSM IP Assets B.V.
发明人： PARTON, Rudy Francois Maria Jozef
IPC分类号： C07C51/42 , C07C51/44 , C07C51/47 , C07C51/48 , C07C59/185 , C07C53/02
CPC分类号： C07C51/47 , B01D3/40 , C07C51/42 , C07C51/44 , C07C51/48 , C07C59/185 , C07C53/02
摘要： The invention provides a process for the isolation of levulinic acid and formic acid from a composition comprising formic acid and levulinic acid, said process comprising a solid-liquid separation step, a vapor removal step, and a solvent-solvent extraction step, wherein a vapor condensate vapor and/or an aqueous phase from the solvent extraction is used to wash the solid fraction. Washing with vapor condensate results in higher levulinic acid yields (higher levulinic acid recovery) as compared to washing with normal water. Washing with aqueous phase results in a less compressible filter cake. Washing first with aqueous phase and subsequently with condensate results in even higher levulinic acid yields. The process is suitable for isolating levulinic acid and formic acid from compositions made by acid hydrolysis of a lignocellulosic biomass, and also from compositions made by acid hydrolysis of sugars such as glucose and fructose.
摘要翻译：本发明提供了从包含甲酸和乙酰丙酸的组合物中分离乙酰丙酸和甲酸的方法，所述方法包括固液分离步骤，蒸气去除步骤和溶剂 - 溶剂萃取步骤，其中蒸气使用来自溶剂萃取的冷凝物蒸气和/或水相洗涤固体部分。与普通水洗涤相比，用蒸气冷凝液洗涤导致更高的乙酰丙酸产量（更高的乙酰丙酸回收率）。用水相洗涤会导致较不压缩的滤饼。首先用水相洗涤，随后用冷凝液洗脱得到甚至更高的乙酰丙酸产率。该方法适合于通过木质纤维素生物质的酸水解制备的组合物以及由糖如葡萄糖和果糖的酸水解制备的组合物分离乙酰丙酸和甲酸。

6. 发明公开

EP2922814A1 METHOD FOR THE PRODUCTION OF POLYETHYLENE TEREPHTHALATE WITH A LOW CARBON FOOTPRINT 审中-公开
标题翻译： PROCEDURE用于生产聚对苯二甲酸乙二醇低碳足迹
公开(公告)号：EP2922814A1
公开(公告)日：2015-09-30
申请号：EP13794818.8
申请日：2013-11-21
申请人： ETH Zurich , Cedar Advanced Technology Group Ltd.
发明人： FARHA, Said , FARHA, Kamal , FARHA, Philip
IPC分类号： C07C63/26 , C07C51/265 , C07C45/49 , C07C47/542 , C01B31/08 , C01B31/10 , C01B31/12 , C01B31/18 , C01B31/20 , C07C1/207 , C07C4/06 , C10B53/00 , C10B53/02 , C10B57/06 , C10G57/00
CPC分类号： C07C51/265 , B01D3/40 , C01B32/324 , C01B32/336 , C01B32/342 , C01B32/40 , C01B32/50 , C07C7/08 , C07C29/1518 , C07C45/49 , C07C45/505 , C08G63/183 , C10B53/02 , C10B57/06 , C10G2300/1003 , C10G2300/1014 , C10G2400/30 , Y02E50/14 , Y02E50/32 , Y02P30/20 , C07C47/542 , C07C63/26
摘要： The present invention relates to a method for producing terephthalic acid from lignocellulosic biomass including the steps of pyrolysis of lignocellulosic biomass in the presence of a catalyst obtaining biochar, crude bio-oil and gases; collecting an aromatic fraction from the crude bio-oil and/or from the gases, extracting toluene from the aromatic fraction by distillation; converting the toluene to a p-tolualdehyde by catalyzed carbonylation; oxidation of the p-tolualdehyde in a liquid phase oxidation to terephthalic acid.

7. 发明公开

EP2909132A1 VERFAHREN ZUM KONZENTRIEREN WÄSSRIGER HALOGENWASSERSTOFFLÖSUNGEN 审中-公开
标题翻译：方式浓缩水溶液卤素氢溶液
公开(公告)号：EP2909132A1
公开(公告)日：2015-08-26
申请号：EP13779555.5
申请日：2013-10-16
申请人： SGL Carbon SE
发明人： PÖLLMANN, Peter , FRANZ, Marcus , BOUCAUT, André , AMBRASSAT, Rolf
IPC分类号： C01B7/07
CPC分类号： C01B7/00 , B01D3/40 , C01B7/0712
摘要： The invention relates to a method for concentrating an aqueous hydrogen halide starting solution, particularly of hydrochloric acid, comprising the following steps: • - extractively distilling the aqueous hydrogen halide starting solution in the presence of an extraction agent in a distillation device (12), • - removing hydrogen halide vapour and/or hydrogen halide gas from the upper section of the distillation device (38), • - removing a solution containing the extraction agent from the lower section of said distillation device (24), • - concentrating the solution which contains the extraction agent, removed from the lower section of the distillation device, in a vaporising device (14) and • - feeding the solution containing the extraction agent, which has been concentrated in the vaporising device, back into the distillation device (22), • said solution which contains the extraction agent removed from the lower section of the distillation device being concentrated in the vaporising device at a pressure which lies above the atmospheric pressure, by means of vaporisation.

8. 发明公开

EP2906519A1 FLEXIBLE BUTADIENE EXTRACTION PROCESS 有权转让
标题翻译：柔性丁二烯萃取工艺
公开(公告)号：EP2906519A1
公开(公告)日：2015-08-19
申请号：EP13845575.3
申请日：2013-09-19
申请人： Lummus Technology Inc.
发明人： BRUMMER, Robert, John , DWYER, Thomas, Alexander
IPC分类号： C07C7/04 , C07C11/167 , B01J19/24
CPC分类号： C07C7/005 , B01D3/141 , B01D3/143 , B01D3/40 , C07C7/04 , C07C7/08 , C07C7/10 , C07C11/167
摘要： A butadiene extraction processes designed for flexible operations, with or without a compressor, is disclosed. The ability to run at both high and low pressures provides added process flexibility.
摘要翻译：公开了一种设计用于灵活操作的丁二烯萃取方法，具有或不具有压缩机。在高压和低压下运行的能力提供了额外的流程灵活性。

9. 发明公开

EP2788457A1 VERFAHREN ZUR BEREITSTELLUNG EINER DAMPFFÖRMIGEN GEREINIGTEN ROH-C4-FRAKTION ALS ZUFUHRSTROM FÜR EIN EXTRAKTIONSDESTILLATIONSVERFAHREN MIT EINEM SELEKTIVEN LÖSUNGSMITTEL 有权
标题翻译：一种使用选择性溶剂具体的萃取蒸馏，与蒸汽CLEANED SHAPED ROH-C4馏分作为用电
公开(公告)号：EP2788457A1
公开(公告)日：2014-10-15
申请号：EP12794723.2
申请日：2012-12-04
申请人： BASF SE
发明人： HEIDA, Bernd , HUGO, Randolf
IPC分类号： C10G21/28 , C10G21/14 , C10L3/12 , B01D3/14
CPC分类号： C10L3/12 , B01D3/40 , C10G21/14 , C10G21/28
摘要： The invention relates to a method for providing a vaporous purified crude C
4 fraction as a feed stream for an extractive distillation process using a selective solvent, having the method steps of 1) separating the C
3 -hydrocarbons, 2) separating the C
4 -oligomers and -polymers as well as the C
5+ -hydrocarbons up to the respective residual content specified above for the vaporous purified crude C
4 fraction, and 3) evaporating the liquid crude C
4 fraction. The method is characterized in that all the method steps 1), 2), and 3) are carried out in a single distillation column which is fed the liquid crude C
4 fraction in the upper third of the column thereby forming a rectifying section and a stripping section and from which a head stream containing the C
3 -hydrocarbons and a bottom stream containing the C
4 -oligomers and -polymers as well as the C
5+ -hydrocarbons are drawn, and the vaporous purified crude C
4 fraction is drawn from the stripping section as a side stream.
摘要翻译：本发明涉及一种用于使用选择性溶剂在萃取蒸馏过程中提供的蒸气状纯化粗C4馏分作为进料流为，具有1的方法步骤）分离C3烃，2）分离所述C4-低聚物和 - 聚合物以及将C5 + - 烃到上述用于蒸气纯化粗C 4馏分中指定的respectivement残余含量，以及3）蒸发液体粗C4馏分。该方法是在没有所有的方法步骤1），2）和3）在一个单一的蒸馏塔中进行的所有被馈送在塔的上部三分之一的液体粗C4馏分，从而形成一个精馏段和汽提为特征的部和从该源头通过含有C 3烃和含有C4低聚物的塔底物流和 - 聚合物以及所述C5 + - 烃被绘制，并且蒸气纯化粗C4馏分从汽提部分作为侧引出流。

10. 发明授权

EP2496539B1 VERFAHREN ZUR AUFTRENNUNG EINES C4-SCHNITTES DURCH EXTRAKTIVDESTILLATION MIT EINEM SELEKTIVEN LÖSUNGSMITTEL 有权
标题翻译： PROCESS FOR使用选择性溶剂通过萃取蒸馏的C4馏分的分离
公开(公告)号：EP2496539B1
公开(公告)日：2014-09-03
申请号：EP10779266.5
申请日：2010-11-02
申请人： BASF SE
发明人： HUGO, Randolf , PESCHEL, Werner , STABEL, Uwe , ZACHMANN, Harry , JÄGER, Michael
IPC分类号： C07C7/08 , C07C11/167 , C10G7/08 , C10G21/20 , B01D3/40
CPC分类号： C10G21/20 , B01D3/40 , C07C7/08 , C10G7/08 , C10G2300/44 , C07C11/167

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