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    • 5. 发明公开
    • KOLONNE ZUR THERMISCHEN BEHANDLUNG EINES FLUIDS MIT EINER RÜCKFLUSSLEITUNG
    • KOLONNE ZUR THERMISCHEN BEHANDLUNG EINES FLUIDS MIT EINERRÜCKFLUSSLEITUNG
    • EP3177379A1
    • 2017-06-14
    • EP15747794.4
    • 2015-08-04
    • BASF SE
    • HAMMON, UlrichWALTER, Thomas
    • B01D3/22B01D3/32
    • F25J3/0271B01D3/20B01D3/22B01D3/32B01D3/4261C07C45/783C07C45/80C07C45/82C07C51/44C07C51/48C07C67/54C07C47/22C07C57/04C07C69/54
    • The invention relates to a column (1) for the thermal treatment of a fluid, comprising: a cylindrical, vertically oriented column body (2) forming a column hollow chamber (3); and a material exchange base (4) arranged in the column hollow chamber (3), forming a collecting surface (5). The column (1) according to the invention is characterised by a circulation device (9) comprising: at least one outlet opening (10) formed in the column body (2) above the collecting surface (5); a circulation line (11) in fluid connection with the outlet opening (10); and at least one recirculation opening (14; 14-1 to 14-3) which is in fluid connection with the circulation line (11), and which is formed in the column body (2) above the collection surface (5). The invention also relates to a thermal separation method, wherein a column (1) of this type is used. With this separation method, a gas rises in the column and a liquid falls in the column, wherein the gas and/or the liquid contains in particular (meth)acrylmonomers.
    • 本发明涉及一种用于流体热处理的塔(1),该塔具有形成柱空腔(3)的圆柱形垂直柱体(2)和设置在该柱中的传质塔盘(4) 空腔(3)并形成收集区域(5)。 本发明的塔(1)的特征在于循环装置(9),其具有在收集区域(5)上方的柱体(2)中形成的至少一个排放孔口(10),循环管线(11) 排放孔(10)和至少一个循环孔(14; 14-1至14-3),所述循环孔与循环管线(11)流体连通并形成在塔体(2)中的收集区域上方 5)。 本发明还涉及一种使用这种塔(1)的热分离方法。 在该分离过程中,气体在塔内上升并且液体在塔内下降,所述气体和/或液体尤其包含(甲基)丙烯酸单体。