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    • 1. 发明公开
    • Toner manufacturing method, image forming method, image forming apparatus, and process cartridge
    • Verfahren zum Herstellen von Tonern,Bilderzeugungsverfahren und-vorrichtung sowie Prozesskartusche
    • EP1640809A1
    • 2006-03-29
    • EP05018515.6
    • 2005-08-25
    • Ricoh Company, Ltd.
    • Takahashi, HiroshiKuroda, NoboruKadota, TakahiroNishizaki, ToshinobuKohzu, Osamu
    • G03G9/08B01F7/16
    • B01F3/088B01F3/0811B01F5/0602B01F7/16B01F13/103B01F2215/0481G03G9/0806G03G9/0819
    • A method of manufacturing a toner including forming an emulsion by mixing and stirring an aqueous phase and an oil phase in an emulsification mechanism by a stirring blade. The oil phase contains a dissolved material or a dispersed material which contains an organic phase formed of at least one of a resin, a resin precursor, and a monomer.
      The emulsification mechanism includes an emulsification circulation route formed of pipes having a main portion, and an emulsification device located in the middle of the emulsification circulation route.
      A stirring blade is provided in the emulsification device. In addition, the stirring Reynolds number (Stirring Re) during the stirring is from 3,000 to 15,000 when calculated based on the following relationship (1): Stirring Reynolds number (stirring Re) = ρnd 2 /µ (1). In the relationship (1), ρ represents the density of the emulsion (kg/m 3 ), n represents the rotation number (rps) of the stirring blade, d represents the blade diameter (m) of the stirring blade, and µ represents the viscosity (Pa s) of the emulsion.
    • 一种制造调色剂的方法,包括通过搅拌叶片混合并搅拌乳化机构中的水相和油相来形成乳液。 油相含有溶解材料或含有由树脂,树脂前体和单体中的至少一种形成的有机相的分散材料。 乳化机构包括由具有主要部分的管形成的乳化循环路线和位于乳化循环路线中间的乳化装置。 在乳化装置中设置搅拌叶片。 另外,当根据以下关系式(1)计算搅拌时的搅拌时的雷诺数(搅拌Re)为3,000至15,000:搅拌雷诺数(搅拌Re)=和/ 2(1)。 在关系式(1)中,Á表示乳液的密度(kg / m 3),n表示搅拌叶片的转数(rps),d表示搅拌叶片的叶片直径(μm),μ表示 乳液的粘度(Pa s)。
    • 9. 发明公开
    • Method of manufacturing toner
    • Verfahren zur Herstellung eines Toners
    • EP1703331A1
    • 2006-09-20
    • EP06005080.4
    • 2006-03-13
    • Ricoh Company, Ltd.
    • Miyakawa, MasashiKuroda, NoboruTakahashi, HiroshiMatsui, KazuyukiKadota, Takahiro
    • G03G9/08
    • G03G9/08755G03G9/0804G03G9/0806G03G9/0819G03G9/0827
    • A method of manufacturing a toner including dissolving or dispersing a toner component containing a colorant and a resin in an organic solvent to obtain a solution or dispersion, continuously emulsifying and dispersing the dissolved or the dispersed liquid in an aqueous medium containing a particulate dispersant to obtain emulsified primary particles, controlling cohesion and agglomeration of the emulsified primary particles and removing the organic solvent. Additionally, the ratio (T1/T2) of the arithmetic mean accumulation time (T1) of the emulsified primary particles obtained in the controlling to the arithmetic mean accumulation time (T2) of the emulsified primary particles obtained in the continuous emulsification or dispersion is from 1 to 5.
    • 一种制造调色剂的方法,包括将含有着色剂和树脂的调色剂组分溶解或分散在有机溶剂中以获得溶液或分散体,将溶解的或分散的液体连续乳化并分散在含有颗粒分散剂的水性介质中,得到 乳化的一次粒子,控制乳化的一次粒子的内聚和附聚并除去有机溶剂。 另外,在控制中获得的乳化一次粒子的算术平均累积时间(T1)与在连续乳化或分散中获得的乳化一次粒子的算术平均累积时间(T2)的比率(T1 / T2)来自 1〜5。