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1. 发明公开

EP1055452A3 Pressurized reaction block 有权
标题翻译： Druckreaktionsblock
公开(公告)号：EP1055452A3
公开(公告)日：2001-09-19
申请号：EP00110336.5
申请日：2000-05-13
申请人： Mettler-Toledo GmbH
发明人： Harness, James R. , Haidle, Rudy H. , Markus, Larry W. , Gallup, David A. , Grzybowski, Andrew J.
IPC分类号： B01J19/00 , B01J3/04 , G01N11/14
CPC分类号： G01N11/14 , B01F13/0818 , B01F15/00123 , B01F15/00246 , B01F2013/1091 , B01J3/04 , B01J3/048 , B01J19/0046 , B01J2219/00283 , B01J2219/00308 , B01J2219/00335 , B01J2219/00337 , B01J2219/00344 , B01J2219/00373 , B01J2219/00389 , B01J2219/00481 , B01J2219/00495 , B01J2219/00585 , B01J2219/0059 , B01J2219/00596 , B01J2219/00601 , B01L7/00 , C40B60/14 , G01N2035/00534
摘要： A reaction block assembly (11) of reaction vessels (13) for conducting chemical reactions under pressure. The assembly (11) includes a heat conductive reactive block (31,131) having reaction vessel (13) receiving openings (41,133) formed in the block (31,131). A heat exchanger (49) is mounted in heat transfer engagement with some of the exterior walls (39) of the reaction block (31,131). The heat exchangers (49) can operate in different modes, to provide a heat differential across the reaction block (31,131). A reaction vessel (13) is positioned in each reaction vessel receiving opening (41,133) in the block (31,131). A cap (81) is attached to each reaction vessel (13) and a cannula opening is formed in each cap (81). A cannula passage (111) is connected at one end to a cannula opening in each cap (81) and it has a septum (203) at the other end. A valve (193) controls each cannula passage (111). An operating mechanism is provided for opening and closing each cannula passage controlling valve (193). The reaction block assembly (11) may be used to determine when the reaction of a solution in a reaction vessel (13) is completed. This is accomplished by using a calibration curve comparing the frequency of rotation of the stirring bar (73) with the viscosity of the reaction solution in which the frequency is inversely proportional to the viscosity. The time interval at which the stir bar (73) decouples from rotation with the driving magnet is determined. This time interval of decoupling is compared with the calibration table to determine the viscosity of the solution at the time the reaction was completed which takes place at the time the stir bar (73) was decoupled.
摘要翻译：用于在压力下进行化学反应的反应容器的反应块组件。该组件包括具有形成在块中的反应容器接收开口的导热反应性块。热交换器安装成与反应块的一些外壁传热接合。热交换器可以以不同的模式操作，以在反应块上提供热差。反应容器位于块体中的每个反应容器接收开口中。在每个反应容器上连接一个盖子，并且在每个盖子中形成套管开口。套管通道在一端连接到每个帽中的套管开口，并且在另一端具有隔膜。一个阀门控制每个插管通道。提供了用于打开和关闭每个插管通道控制阀的操作机构。反应块组件可用于确定反应容器中溶液的反应何时完成。这通过使用将搅拌棒的旋转频率与其中频率与粘度成反比的反应溶液的粘度进行比较的校准曲线来实现。确定搅拌棒与驱动磁体与旋转分离的时间间隔。将该去耦的时间间隔与校准表进行比较，以确定在搅拌棒解耦时发生的反应完成时溶液的粘度。

2. 发明公开

EP0963791A3 Modular reaction block assembly with thermoelectric cooling and heating 有权
标题翻译：具有热电冷却和加热模块化反应块组件
公开(公告)号：EP0963791A3
公开(公告)日：2000-09-06
申请号：EP99201812.7
申请日：1999-06-08
申请人： Mettler-Toledo GmbH
发明人： Harness, Ph.D. James R. , Markus, Larry W. , Grzybowski, Andrew J. , Haidle, Rudy H. , Turewicz, Marek
IPC分类号： B01L7/00
CPC分类号： B01L7/52 , B01J19/0046 , B01J2219/00283 , B01J2219/00308 , B01J2219/0031 , B01J2219/00346 , B01J2219/00481 , B01J2219/00495 , B01J2219/00585 , B01J2219/00689 , C40B60/14
摘要： An array of reaction assemblies for heating and cooling a plurality of reaction vessels. Each reaction vessel assembly including a heat conductive reaction block having an exterior wall and a reaction vessel receiving cavity formed in the block inwardly of the exterior wall. A thermoelectric module is mounted in heat transfer engagement with the exterior wall of the heat conductive reaction block. A fluid heat exchange element is mounted in heat transfer engagement with the thermoelectric module. The thermoelectric module has its junctions to selectively remove heat from the exterior wall of the reaction block or to supply heat to this exterior wall. Each thermoelectric module has thermoelectric junctions cascaded for increased heating and cooling range and a plurality of these junctions to increase capacity.

3. 发明公开

EP1055452A2 Pressurized reaction block 有权
标题翻译：高压反应BLOCK
公开(公告)号：EP1055452A2
公开(公告)日：2000-11-29
申请号：EP00110336.5
申请日：2000-05-13
申请人： Mettler-Toledo GmbH
发明人： Harness, James R. , Haidle, Rudy H. , Markus, Larry W. , Gallup, David A. , Grzybowski, Andrew J.
IPC分类号： B01J19/00
CPC分类号： G01N11/14 , B01F13/0818 , B01F15/00123 , B01F15/00246 , B01F2013/1091 , B01J3/04 , B01J3/048 , B01J19/0046 , B01J2219/00283 , B01J2219/00308 , B01J2219/00335 , B01J2219/00337 , B01J2219/00344 , B01J2219/00373 , B01J2219/00389 , B01J2219/00481 , B01J2219/00495 , B01J2219/00585 , B01J2219/0059 , B01J2219/00596 , B01J2219/00601 , B01L7/00 , C40B60/14 , G01N2035/00534
摘要： A reaction block assembly of reaction vessels for conducting chemical reactions under pressure. The assembly includes a heat conductive reactive block having reaction vessel receiving openings formed in the block. A heat exchanger is mounted in heat transfer engagement with some of the exterior walls of the reaction block. The heat exchangers can operate in different modes, to provide a heat differential across the reaction block. A reaction vessel is positioned in each reaction vessel receiving opening in the block. A cap is attached to each reaction vessel and a cannula opening is formed in each cap. A cannula passage is connected at one end to a cannula opening in each cap and it has a septum at the other end. A valve controls each cannula passage. An operating mechanism is provided for opening and closing each cannula passage controlling valve. The reaction block assembly may be used to determine when the reaction of a solution in a reaction vessel is completed. This is accomplished by using a calibration curve comparing the frequency of rotation of the stirring bar with the viscosity of the reaction solution in which the frequency is inversely proportional to the viscosity. The time interval at which the stir bar decouples from rotation with the driving magnet is determined. This time interval of decoupling is compared with the calibration table to determine the viscosity of the solution at the time the reaction was completed which takes place at the time the stir bar was decoupled.

4. 发明授权

EP1055452B1 Pressurized reaction block 有权
标题翻译：压力反应块
公开(公告)号：EP1055452B1
公开(公告)日：2006-02-15
申请号：EP00110336.5
申请日：2000-05-13
申请人： Mettler-Toledo GmbH
发明人： Harness, James R. , Haidle, Rudy H. , Markus, Larry W. , Gallup, David A. , Grzybowski, Andrew J.
IPC分类号： B01J19/00 , B01J3/04 , G01N11/14
CPC分类号： G01N11/14 , B01F13/0818 , B01F15/00123 , B01F15/00246 , B01F2013/1091 , B01J3/04 , B01J3/048 , B01J19/0046 , B01J2219/00283 , B01J2219/00308 , B01J2219/00335 , B01J2219/00337 , B01J2219/00344 , B01J2219/00373 , B01J2219/00389 , B01J2219/00481 , B01J2219/00495 , B01J2219/00585 , B01J2219/0059 , B01J2219/00596 , B01J2219/00601 , B01L7/00 , C40B60/14 , G01N2035/00534

5. 发明授权

EP0963791B1 Modular reaction block assembly with thermoelectric cooling and heating 有权
标题翻译：具有热电冷却和加热模块化反应块组件
公开(公告)号：EP0963791B1
公开(公告)日：2004-09-22
申请号：EP99201812.7
申请日：1999-06-08
申请人： Mettler-Toledo GmbH
发明人： Harness, Ph.D. James R. , Markus, Larry W. , Grzybowski, Andrew J. , Haidle, Rudy H. , Turewicz, Marek
IPC分类号： B01L7/00 , B01J19/00
CPC分类号： B01L7/52 , B01J19/0046 , B01J2219/00283 , B01J2219/00308 , B01J2219/0031 , B01J2219/00346 , B01J2219/00481 , B01J2219/00495 , B01J2219/00585 , B01J2219/00689 , C40B60/14

6. 发明公开

EP0963791A2 Modular reaction block assembly with thermoelectric cooling and heating 有权
标题翻译： Modulare Reaktionsblockanordnung mit thermoelektrischerKühlungund Heizung
公开(公告)号：EP0963791A2
公开(公告)日：1999-12-15
申请号：EP99201812.7
申请日：1999-06-08
申请人： Mettler-Toledo GmbH
发明人： Harness, Ph.D. James R. , Markus, Larry W. , Grzybowski, Andrew J. , Haidle, Rudy H. , Turewicz, Marek
IPC分类号： B01L7/00
CPC分类号： B01L7/52 , B01J19/0046 , B01J2219/00283 , B01J2219/00308 , B01J2219/0031 , B01J2219/00346 , B01J2219/00481 , B01J2219/00495 , B01J2219/00585 , B01J2219/00689 , C40B60/14
摘要： An array of reaction assemblies for heating and cooling a plurality of reaction vessels. Each reaction vessel assembly including a heat conductive reaction block having an exterior wall and a reaction vessel receiving cavity formed in the block inwardly of the exterior wall. A thermoelectric module is mounted in heat transfer engagement with the exterior wall of the heat conductive reaction block. A fluid heat exchange element is mounted in heat transfer engagement with the thermoelectric module. The thermoelectric module has its junctions to selectively remove heat from the exterior wall of the reaction block or to supply heat to this exterior wall. Each thermoelectric module has thermoelectric junctions cascaded for increased heating and cooling range and a plurality of these junctions to increase capacity.
摘要翻译：用于加热和冷却多个反应容器的反应组件阵列。每个反应容器组件包括导热反应块，其具有形成在外壁内部的块体中的外壁和反应容器容纳空腔。热电模块安装成与导热反应块的外壁传热接合。流体热交换元件安装成与热电模块传热接合。热电模块具有从反应块的外壁选择性地去除热量的接头或者向该外壁供应热量。每个热电模块具有级联的热电连接以增加加热和冷却范围，以及多个这些结点以增加容量。

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