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1. 发明公开

EP2935366A1 PROCESS FOR SEPARATING VINYL ESTERS FROM A GAS STREAM COMPRISING ETHYLENE AND VINYL ESTERS 有权
标题翻译： VERFAHREN ZUM TRENNEN VON VINYLESTERN AUS EINEM GASSTROM MIT ETHYLEN- UND VINYLESTERN
公开(公告)号：EP2935366A1
公开(公告)日：2015-10-28
申请号：EP13818709.1
申请日：2013-12-16
申请人： Basell Polyolefine GmbH
发明人： NEUMANN, Erich , WOLF, Christoph , LITTMANN, Dieter
IPC分类号： C08F210/02 , C08F2/00 , C07C67/54
CPC分类号： C07C67/52 , C08F210/02 , Y02P20/582 , C08F2/00 , C08F218/08 , C07C69/15
摘要： Process for separating esters of vinyl alcohol from a gas stream comprising from 70 to 99.5% by weight of ethylene and from 0.5 to 30% by weight of esters of vinyl alcohol being at a pressure in the range of from 0.5 MPa to 10 MPa and a temperature in the range of from 5°C to 50°C comprising the steps of a) cooling the gas stream in a first heat exchanger by means of a cooling medium to a temperature of from -5°C to 40°C; b) withdrawing the not condensed part of the gas stream from the first heat exchanger and transferring it to a second heat exchanger; c) cooling the gas stream in the second heat exchanger to a temperature of from -20°C to 5°C; d) withdrawing the not condensed part of the gas stream from the second heat exchanger, reducing the pressure of the gas stream to from 0.5 MPa to 3 MPa and transferring it to a separation vessel; e) withdrawing the not condensed part of the gas stream from the separation vessel and transferring it as cooling medium to the second heat exchanger; and f) withdrawing the cooling medium as ethylene gas stream with a reduced content of esters of vinyl alcohol from the second heat exchanger, and process for copolymerizing ethylene and esters of vinyl alcohol in the presence of free-radical polymerization initiators at pressures in the range of from 110 MPa to 500 MPa and temperatures in the range of from 100°C to 350°C in a continuously operated polymerization apparatus comprising such a process for separating esters of vinyl alcohol from a gas stream comprising from 70 to 99.5% by weight of ethylene and from 0.5 to 30% by weight of esters of vinyl alcohol.
摘要翻译：从乙烯醇的70〜99.5重量％的乙烯和0.5〜30重量％的乙烯醇的酯的压力为0.5MPa〜10MPa的范围内分离乙烯醇的酯的方法，包括以下步骤：a）通过冷却介质将第一热交换器中的气流冷却至-5℃至40℃的温度; b）将来自第一热交换器的气流的未冷凝部分排出并将其转移到第二热交换器; c）将第二热交换器中的气流冷却至-20℃至5℃的温度; d）从第二热交换器排出气流的未冷凝部分，将气流的压力降低至0.5MPa至3MPa并将其转移至分离容器; e）从分离容器中取出气流的未冷凝部分并将其作为冷却介质转移到第二热交换器; 以及f）将来自第二热交换器的乙烯醇酯含量降低的乙烯气流作为乙烯气流排出，以及在自由基聚合引发剂存在下在乙烯醇和乙烯醇酯的存在下共聚乙烯醇的方法在连续操作的聚合装置中，从110MPa至500MPa的温度范围为100℃至350℃，该聚合装置包括将乙烯醇的酯从气流中分离的方法，该气流包含70至99.5重量％乙烯和0.5至30重量％的乙烯醇的酯。

2. 发明公开

EP1562690A1 SAFE REMOVAL OF VOLATILE, OXIDIZABLE COMPOUNDS FROM PARTICLES, IN PARTICULAR POLYMER PARTICLES 有权
标题翻译：作者VOLATILE，可氧化的安全去除化合物OFF颗粒，特别是从聚合物颗粒
公开(公告)号：EP1562690A1
公开(公告)日：2005-08-17
申请号：EP03780027.3
申请日：2003-11-21
申请人： Basell Polyolefine GmbH
发明人： MÄHLING, Frank-Olaf , NEUMANN, Erich , FINETTE, Andre-Armand , NIEKEN, Ulrich
IPC分类号： B01D53/86 , C08F6/00
CPC分类号： B01D53/8687 , B01D53/8668 , C08F6/005 , C08F6/26
摘要： In a method of removing volatile oxidizable compounds from particles present in a container, a gas stream is continuously introduced into the container, the gas stream takes up the oxidizable compound from the particles in the container and a gas stream laden with the oxidizable compound is discharged from the container. In the method of the present invention, oxygen is added to the gas stream which has been discharged and the oxidizable compound present in the discharged gas stream is subsequently at least partly catalytically oxidized by means of the oxygen and this oxidized gas stream forms at least part of the gas stream introduced, so that the gas stream is circulated. This makes safe and inexpensive removal of the oxidizable compounds from the particles possible.

3. 发明授权

EP3377537B1 POLYMERIZATION PROCESS WITH A PARTIAL SHUTDOWN PHASE 有权
公开(公告)号：EP3377537B1
公开(公告)日：2019-03-13
申请号：EP16797866.7
申请日：2016-11-16
申请人： Basell Polyolefine GmbH
发明人： NEUMANN, Erich , WOLFRAM, Sven , WOLF, Christoph , MOHRBUTTER, Juergen , LITTMANN, Dieter
IPC分类号： C08F2/01 , B01J19/00

4. 发明授权

EP3083027B1 VESSEL FOR SEPARATING COMPONENTS OF A REACTION MIXTURE OBTAINED BY HIGH-PRESSURE POLYMERIZATION OF ETHYLENICALLY UNSATURATED MONOMERS WITH INTEGRATED BURSTING DISCS 有权
标题翻译：用于分离具有集成爆破片的乙烯属不饱和单体的高压聚合反应混合物组分的容器
公开(公告)号：EP3083027B1
公开(公告)日：2017-07-12
申请号：EP14812492.8
申请日：2014-12-15
申请人： Basell Polyolefine GmbH
发明人： NEUMANN, Erich , KHAYRULLIN, Danir , FIBLA, Claudio
IPC分类号： B01J3/00
CPC分类号： C08F6/10 , B01D19/0036 , B01D19/0063 , B01J3/002 , B01J19/2415 , B01J2219/185 , B01J2219/1943 , B01J2219/1946 , C08F10/02 , Y02P20/582

5. 发明授权

EP2935366B1 PROCESS FOR SEPARATING VINYL ESTERS FROM A GAS STREAM COMPRISING ETHYLENE AND VINYL ESTERS 有权
标题翻译：法用于与乙烯和乙烯基酯从气流中的乙烯基酯的分离
公开(公告)号：EP2935366B1
公开(公告)日：2017-01-25
申请号：EP13818709.1
申请日：2013-12-16
申请人： Basell Polyolefine GmbH
发明人： NEUMANN, Erich , WOLF, Christoph , LITTMANN, Dieter
IPC分类号： C08F210/02 , C08F2/00 , C07C67/54
CPC分类号： C07C67/52 , C08F210/02 , Y02P20/582 , C08F2/00 , C08F218/08 , C07C69/15

6. 发明公开

EP3898708A1 HIGH-PRESSURE POLYMERIZATION PROCESS OF ETHYLENICALLY UNSATURATED MONOMERS IN A POLYMERIZATION REACTOR 有权
公开(公告)号：EP3898708A1
公开(公告)日：2021-10-27
申请号：EP19818105.9
申请日：2019-12-16
申请人： Basell Polyolefine GmbH
发明人： LITTMANN, Dieter , FINETTE, Andre-Armand , WOLF, Christoph , DEUERLING, Michael , MOHRBUTTER, Juergen , KHAYRULLIN, Danir , MEI, Giulia , NEUMANN, Erich
IPC分类号： C08F2/01 , C08F2/02 , C08F10/02 , B01J19/24 , B01J8/00

7. 发明授权

EP3077423B1 PROCESS FOR SEPARATING COMPONENTS OF A REACTION MIXTURE OBTAINED BY HIGH-PRESSURE POLYMERIZATION OF ETHYLENICALLY UNSATURATED MONOMERS 有权
标题翻译：用于分离乙烯基不饱和单体的高压聚合反应混合物组分的方法
公开(公告)号：EP3077423B1
公开(公告)日：2017-10-04
申请号：EP14809799.1
申请日：2014-12-03
申请人： Basell Polyolefine GmbH
发明人： GROOS, Georg , NEUMANN, Erich , DEUERLING,Michael , LITTMANN, Dieter
IPC分类号： C08F10/02 , C08F6/10 , C08F6/12 , C08J11/02 , C08F10/00 , C08F6/00 , C08F2/00 , C08F2/02 , C08F110/02 , C08F210/16 , C08F2/01 , C08F2/34 , C08L23/04
CPC分类号： C08F6/12 , C08F2/01 , C08F2/02 , C08F2/34 , C08F6/001 , C08F6/10 , C08J11/02 , Y02P20/582 , C08L23/04 , C08F10/02 , C08F2/00 , C08F110/02 , C08F210/16 , C08F2500/08

8. 发明公开

EP3077422A1 PROCESS FOR SEPARATING COMPONENTS OF A REACTION MIXTURE OBTAINED BY HIGH-PRESSURE POLYMERIZATION OF ETHYLENICALLY UNSATURATED MONOMERS WITH IMPROVED LEVEL CONTROL 有权
标题翻译：方法由具有改进的电平控制器的烯属不饱和单体的高压聚合的反应混合物的组分的分离
公开(公告)号：EP3077422A1
公开(公告)日：2016-10-12
申请号：EP14806288.8
申请日：2014-12-03
申请人： Basell Polyolefine GmbH
发明人： KHAYRULLIN, Danir , DEUERLING, Michael , WOLF, Christoph , NEUMANN, Erich , FIBLA, Claudio
IPC分类号： C08F6/00 , C08F6/10 , C08F6/12 , C08J11/02 , C08F10/00 , G01F23/288 , G01N9/24
CPC分类号： C08F6/10 , B01J4/002 , C08F6/001 , C08F6/12 , C08F10/02 , G01F23/2885 , C08L23/04 , C08F2/00
摘要： The present disclosure generally relates to a process for separating polymeric and gaseous components of a reaction mixture obtained by high-pressure polymerization of ethylenically unsaturated monomers in the presence of free-radical polymerization initiators into a gaseous fraction and a liquid fraction in a separation vessel, wherein the filling level of the liquid fraction in the separation vessel is measured by a radiometric level measurement system comprising at least two radioactive sources and at least three radiation detectors, and the filling level is controlled by a product discharge valve which operates based on data coming from the level measurement system.
摘要翻译：本发明基因的反弹涉及一种方法，用于在分离容器通过在自由基聚合引发剂的存在下烯属不饱和单体的高压聚合得到的反应混合物的聚合和气态组分分离成气体馏分和液体馏分， worin在分离容器中的液体级分的填充电平由辐射电平测量系统，包括至少两个辐射源和至少三个辐射检测器和所述填充水平是通过其操作基于数据来产品排放阀控制测量从电平测量系统。

9. 发明授权

EP1562690B1 SAFE REMOVAL OF VOLATILE, OXIDIZABLE COMPOUNDS FROM PARTICLES, IN PARTICULAR POLYMER PARTICLES 有权
标题翻译：作者VOLATILE，可氧化的安全去除化合物OFF颗粒，特别是从聚合物颗粒
公开(公告)号：EP1562690B1
公开(公告)日：2007-06-13
申请号：EP03780027.3
申请日：2003-11-21
申请人： Basell Polyolefine GmbH
发明人： MÄHLING, Frank-Olaf , NEUMANN, Erich , FINETTE, Andre-Armand , NIEKEN, Ulrich
IPC分类号： B01D53/86 , C08F6/00
CPC分类号： B01D53/8687 , B01D53/8668 , C08F6/005 , C08F6/26
摘要： In a method of removing volatile oxidizable compounds from particles present in a container, a gas stream is continuously introduced into the container, the gas stream takes up the oxidizable compound from the particles in the container and a gas stream laden with the oxidizable compound is discharged from the container. In the method of the present invention, oxygen is added to the gas stream which has been discharged and the oxidizable compound present in the discharged gas stream is subsequently at least partly catalytically oxidized by means of the oxygen and this oxidized gas stream forms at least part of the gas stream introduced, so that the gas stream is circulated. This makes safe and inexpensive removal of the oxidizable compounds from the particles possible.

10. 发明公开

EP3377537A1 POLYMERIZATION PROCESS WITH A PARTIAL SHUTDOWN PHASE 有权
公开(公告)号：EP3377537A1
公开(公告)日：2018-09-26
申请号：EP16797866.7
申请日：2016-11-16
申请人： Basell Polyolefine GmbH
发明人： NEUMANN, Erich , WOLFRAM, Sven , WOLF, Christoph , MOHRBUTTER, Juergen , LITTMANN, Dieter
IPC分类号： C08F2/01 , B01J19/00
CPC分类号： C08F2/01 , B01J19/242
摘要： A process for polymerizing ethylene to obtain an ethylene-based polymer in a plant, wherein the plant includes a reactor in fluid communication with a recycle connection, wherein the process comprises a polymerization phase, a partial shutdown phase, and the steps of reducing the pressure in the reactor for entering from the polymerization phase into the partial shutdown phase; and increasing the pressure in the reactor for exiting from the partial shutdown phase and re-entering the polymerization phase.

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