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1. 发明公开

EP3239215A4 METHOD FOR MANUFACTURING FLUORINE-CONTAINING POLYMER PARTICLES 有权转让
公开(公告)号：EP3239215A4
公开(公告)日：2018-07-25
申请号：EP15872947
申请日：2015-12-18
申请人： ASAHI GLASS CO LTD
发明人： SAITO SUSUMU , HASHIMOTO WAKAKO , SHIMOHIRA TETSUJI , HAMAZAKI KAZUO , OTSUGU SATOSHI , MATOBA HIROKI
IPC分类号： C08J3/16 , C08F6/12
CPC分类号： C08F6/12 , C08F2/06 , C08F6/003 , C08J3/16 , C08L27/12
摘要： To provide a method capable of producing fluorinated polymer particles in which formation of fine particles or formation of large aggregates is sufficiently suppressed even in the case of a fluorinated polymer having high solubility in a solvent. The method comprises the following steps (i) and (ii), being a method for producing particles of a fluorinated polymer (A) which has either one or both of structural units (u1) derived from tetrafluoroethylene and structural units (u2) having no sulfonic acid type functional group and having a cyclic structure and fluorine atoms, and which has structural units (u3) having a sulfonic acid type functional group, wherein the proportion of the structural units (u1) is from 0 to 82 mol% in all structural units (100 mol%) in the fluorinated polymer (A): (i) a step of preparing solution or dispersion of the fluorinated polymer (A) having the above fluorinated polymer (A) dissolved or dispersed in a solvent (B), wherein the following conditions (i-1) and (i-2) are satisfied: (i-1) the solvent (B) contains a good solvent (B2) wherein the solubility of the fluorinated polymer (A) is at least 30%, (i-2) even when the above solution or dispersion of the fluorinated polymer (A) is passed through a filter of 200 mesh made of stainless steel, no residue remains on the filter, (ii) a step of mixing the above solution or dispersion of the fluorinated polymer (A) and a solvent (C) to aggregate the fluorinated polymer (A) to form particles of the fluorinated polymer (A), wherein the following conditions (ii-1) to (ii-3) are satisfied: (ii-1) the solvent (C) contains a poor solvent (C1) whereby the degree of swelling of the fluorinated polymer (A) is at most 100%, (ii-2) the degree of swelling of the fluorinated polymer (A) by a mixed solvent (BC) of the solvent (B) and the solvent (C) is from 70 to 250%, (ii-3) the ratio of the mass (Wc) of the solvent (C) to the mass (W B ) of the solvent (B) is from 1 to 5.

3. 发明公开

EP3172249A4 ULTRAPURE COPOLYMERS 审中-公开
公开(公告)号：EP3172249A4
公开(公告)日：2018-03-28
申请号：EP15824371
申请日：2015-07-21
申请人： ARLANXEO SINGAPORE PTE LTD
发明人： SIEGERS CONRAD , THOMPSON DAVID
IPC分类号： C08F210/12 , C08F6/04 , C08F6/12 , C08F8/20 , C08K5/098 , C08L9/00 , C08L15/02 , C08L23/28
CPC分类号： C08F6/04 , C08F8/20 , C08F210/12 , C08K5/098 , C08L9/00 , C08L15/02 , C08L2205/025 , C08L23/28
摘要： The invention relates to a method to reduce or prevent agglomeration of particles of optionally halogenated rubbers in aqueous media by LCST compounds, their purification as well as ultrapure optionally halogenated rubbers. The invention further relates to (halogenated) copolymer products comprising the same or derived therefrom.

4. 发明公开

EP3077423A1 PROCESS FOR SEPARATING COMPONENTS OF A REACTION MIXTURE OBTAINED BY HIGH-PRESSURE POLYMERIZATION OF ETHYLENICALLY UNSATURATED MONOMERS 有权
标题翻译： PROCESS FOR通过烯属不饱和单体的高压聚合的反应混合物的组分的分离
公开(公告)号：EP3077423A1
公开(公告)日：2016-10-12
申请号：EP14809799.1
申请日：2014-12-03
申请人： Basell Polyolefine GmbH
发明人： GROOS, Georg , NEUMANN, Erich , DEUERLING,Michael , LITTMANN, Dieter
IPC分类号： C08F6/10 , C08F6/12 , C08J11/02 , C08F10/00 , C08F6/00
CPC分类号： C08F6/12 , C08F2/01 , C08F2/02 , C08F2/34 , C08F6/001 , C08F6/10 , C08J11/02 , Y02P20/582 , C08L23/04 , C08F10/02 , C08F2/00 , C08F110/02 , C08F210/16 , C08F2500/08
摘要： Process for separating polymeric and gaseous components of a reaction mixture obtained by high-pressure polymerization of ethylenically unsaturated monomers in the presence of free-radical polymerization initiators, the process comprising the steps of entering the reaction mixture into a separation vessel; separating the reaction mixture into in a gaseous fraction and a liquid fraction; and withdrawing the gaseous fraction from the top of the separation vessel and withdrawing the liquid fraction from the bottom of the separation vessel, wherein the separation is carried out at a pressure of from 15 MPa to 50 MPa and a temperature of from 120°C to 300°C; the separation vessel has a vertically arranged cylindrical shape with a ratio of length to diameter L/D of from 4 to 10 and is equipped with an inlet pipe for introducing the reaction mixture into the separation vessel; the inlet pipe extends vertically from the top into the separation vessel; and the ratio of the inner diameter of the inlet pipe at its lower end and the inner diameter of the separating vessel in its cylindrical part is in the range of from 0.2 to 0.4 and process for preparing ethylene homopolymers or copolymers from ethylenically unsaturated monomers in the presence of free-radical polymerization initiators at temperatures from 100°C to 350°C and pressures in the range of from 110 MPa to 500 MPa in a polymerization reactor comprising a such process for separating polymeric and gaseous components.
摘要翻译：本公开涉及一种用于在一个气体馏分和液体馏分通过在自由基聚合引发剂的存在下烯属不饱和单体的高压聚合得到的反应混合物的聚合和气态组分分离成，worin分离是在15兆帕至50兆帕的压力和120℃至300℃的在分离容器具有带有长度与直径L的比率的垂直布置的圆筒状的温度下进行从4的出/ D 至10和所有其配备有在从顶到分离容器垂直地延伸进水管; 和在其下端的入口管和分离容器在其筒状部的内径的内径的比率是在0.2至0.4的范围内。

5. 发明公开

EP2774666A1 Steuerung eines Mischkneterns 审中-公开
标题翻译：控制混合揉捏
公开(公告)号：EP2774666A1
公开(公告)日：2014-09-10
申请号：EP14170983.2
申请日：2010-02-05
申请人： LIST Holding AG
发明人： FLEURY, Pierre-Alain , KUNZ, Alfred , Witte, Dr., Daniel , DIENER, Andreas , ISENSCHMID, Thomas , SCHWICK, Alain , STEINER, Manuel
IPC分类号： B01D1/22 , B01D19/00 , B29C47/00 , C08C1/12 , C08C2/02 , C08C3/02 , C08F6/00 , C08F6/10 , C08F6/12 , C08F6/16 , C08F6/20 , C08F6/28 , C08G85/00 , C08C1/02 , C08C2/00 , B01D1/14 , B29C47/10 , B29C47/36 , B29C47/76
CPC分类号： B01D1/226 , B01D1/14 , B01D19/0005 , B01D19/0026 , B29B7/7485 , B29C47/0009 , B29C47/1081 , B29C47/364 , B29C47/366 , B29C47/367 , B29C47/761 , B29C47/762 , B29C2791/006 , C08C1/02 , C08C2/00 , C08F6/003 , Y02P20/123
摘要： Bei einem Verfahren zur kontinuierlichen Behandlung eines zähviskosen, pastösen Produktes in einem Mischkneter mit einem durchgängigen Produkt- und Gasraum soll die Temperatur des Produktes am Austrag über die Drehzahl des Mischkneters bei gegebener Produktzufuhr geregelt werden.
摘要翻译：在具有连续产品和气体空间的混合捏合机中连续处理粘稠糊状产品的方法中，对于给定的产品供应，产品的温度应当控制在混合捏合机速度的输出。

6. 发明公开

EP2774665A1 Verfahren zur kontinuierlichen Behandlung von Polymerlösungen 有权转让
标题翻译：一种用于连续处理聚合物溶液的方法
公开(公告)号：EP2774665A1
公开(公告)日：2014-09-10
申请号：EP14170982.4
申请日：2010-02-05
申请人： LIST Holding AG
发明人： FLEURY, Pierre-Alain , KUNZ, Alfred , Witte, Dr., Daniel , DIENER, Andreas , ISENSCHMID, Thomas , SCHWICK, Alain , STEINER, Manuel
IPC分类号： B01D1/22 , B01D19/00 , B29C47/00 , C08C1/12 , C08C2/02 , C08C3/02 , C08F6/00 , C08F6/10 , C08F6/12 , C08F6/16 , C08F6/20 , C08F6/28 , C08G85/00 , C08C1/02 , C08C2/00 , B01D1/14 , B29C47/10 , B29C47/36 , B29C47/76
CPC分类号： B01D1/226 , B01D1/14 , B01D19/0005 , B01D19/0026 , B29B7/7485 , B29C47/0009 , B29C47/1081 , B29C47/364 , B29C47/366 , B29C47/367 , B29C47/761 , B29C47/762 , B29C2791/006 , C08C1/02 , C08C2/00 , C08F6/003 , Y02P20/123
摘要： Bei einem Verfahren zur kontinuierlichen Behandlung von Polymerlösungen in einem Verdampfer und/oder Entgaser mit einem durchgängigen Produkt- und Gasraum soll die Zufuhr an Eingangsprodukt oder rückgeführtem Kondensat in den Produktraum des Mischkneters über die Länge des Produktraumes verteilt werden.
摘要翻译：在用于在蒸发器和/或除气器有稳定的产品和气体空间，饲料产品的供应或再循环的冷凝物连续处理聚合物溶液的方法是在混合捏合机过的产品空间的长度的产品的空间分布。

7. 发明授权

EP1916262B1 METHOD OF TAKING (METH)ACRYLIC ESTER POLYMER OUT OF LIQUID REACTION MIXTURE 有权
标题翻译： METHOD FOR（甲基）丙烯酸酯聚合物在液体反应混合物的分离BASIS
公开(公告)号：EP1916262B1
公开(公告)日：2012-02-15
申请号：EP06768338.3
申请日：2006-07-21
申请人： Kuraray Co., Ltd.
发明人： HAMADA, Kenichi, c/o KURARAY CO., LTD. , MATSUNAGA, Susumu, c/o KURARAY CO., LTD. , KATO, Masaji c/o KURARAY CO., LTD. , NAGAI, Jun c/o KURARAY CO., LTD. , MOROTOMI, Tatsuo c/o KURARAY CO., LTD. , OSHIMA, Hiroshi c/o KURARAY CO., LTD. , WATANABEI, Kazunori c/o KURARAY CO., LTD. , WATANABE, Tatsufumi c/o KURARAY CO., LTD.
IPC分类号： C08F6/12 , C08F20/10
CPC分类号： C08F6/02 , C08F6/12 , C08L33/10 , C08L33/08
摘要： [PROBLEMS] To easily and efficiently obtain a high-quality (meth)acrylic ester polymer which is reduced in the content of residual metallic ingredients (aluminum ingredient, alkali metal ingredient, and other metallic ingredients), has a high purity, and is excellent in properties such as heat resistance and transparency. [MEANS FOR SOLVING PROBLEMS] A method is provided which comprises adding an acid to a liquid reaction mixture containing a (meth)acrylate polymer and obtained by polymerizing a (meth)acrylic ester monomer in a water-insoluble organic solvent in the presence of a metal-containing polymerization initiator and a metal compound such as an organoaluminum compound, subsequently mixing the resultant mixture with water at 90°C or higher to wash it, separating the resultant liquid mixture of the liquid reaction mixture and water into an organic-solvent-solution layer and an aqueous-solution layer, isolating the organic-solvent-solution layer separated, and taking the (meth)acrylic ester polymer out of the solution. Also provided is a (meth)acrylic ester polymer obtained by the method. This polymer has a high purity and excellent transparency.

8. 发明公开

EP2203484A1 PROCESS FOR RECOVERING A POLYMER FROM A SOLUTION 有权
标题翻译：聚合物的方法从溶液中回收
公开(公告)号：EP2203484A1
公开(公告)日：2010-07-07
申请号：EP08804386.4
申请日：2008-09-18
申请人： SOLVAY (Société Anonyme)
发明人： LEPERS, Jean-Christophe , GEETS, Denis , CAILLE, Jean-Raphael
IPC分类号： C08F6/12 , C08J3/14 , C08J11/08
CPC分类号： C08J11/08 , C08F6/12 , C08J2327/06 , Y02W30/701 , C08L27/06
摘要： Process for recovering a polymer by injection of steam, and optionally liquid water, into a solution of this polymer comprising a polar aprotic organic solvent (PAOS) that has an azeotrope with water and an apolar organic compound that is miscible with the PAOS and immiscible with water and that acts as a phase separation agent (PSA), the boiling point of which is below that of the water/PAOS azeotrope, the amount of steam injected being sufficient to give rise to the substantial removal of the PSA via stripping and that of the PAOS via azeotropic distillation, and the total amount of water being sufficient to give rise to the precipitation of the polymer, this process being characterized in that the polymer solution also comprises an alcohol, at least during the precipitation of the polymer.

9. 发明公开

EP2035471A1 PHASE SEPARATION PROCESS UTILIZING A HYDROFLUOROCARBON 有权
标题翻译：相分离使用HFC物质
公开(公告)号：EP2035471A1
公开(公告)日：2009-03-18
申请号：EP07756121.5
申请日：2007-04-27
申请人： ExxonMobil Chemical Patents Inc.
发明人： MC DONALD, Michael, F. , MILNER, Scott, T. , SHAFFER, Timothy, D. , WEBB, Robert, N. , HEMBREE, Richard, D.
IPC分类号： C08F210/12 , C08F6/24 , C08F6/12
CPC分类号： C08F210/12 , C08C1/14 , C08C2/04 , C08C2/06 , C08F6/003 , C08F6/12 , C08F210/16 , C08F236/08
摘要： Provided for herein is a process for separating a hydrocarbon-rubber from a hydrofluorocarbon diluent comprising contacting a polymer slurry comprising the hydrocarbon-rubber dispersed within the hydrofluorocarbon diluent with a hydrocarbon solvent capable of dissolving the hydrocarbon-rubber, to produce a first liquid phase and a second liquid phase, and separating the first liquid phase from the second liquid phase.

10. 发明授权

EP1615715B1 PROCESS FOR REDUCING THE CONTENT OF WATER-SOLUBLE SALTS OF AQUEOUS SOLUTIONS OF POLYMERS CONTAINING VINYLAMINE GROUPS 有权
标题翻译：用于减少内容水，盐，水基乙烯基胺聚合物解决方案
公开(公告)号：EP1615715B1
公开(公告)日：2008-12-31
申请号：EP04722165.0
申请日：2004-03-20
申请人： BASF SE
发明人： BENNETT, Andrea, Karen, 56/39 Railway Villa , MITCHELL, Michael, A. , CARRICO, Peter, W.
IPC分类号： B01D61/14 , A61L15/60 , C08L39/02 , C08F8/12 , C08F6/12 , B01D63/16
CPC分类号： B01D61/145 , B01D61/027 , B01D61/04 , B01D61/16 , B01D2311/04 , B01J2220/68 , C08F6/06 , C08J3/03 , C08J2339/02 , C08L39/02 , B01D2311/18 , B01D2311/12
摘要： Process for reducing the content of water-soluble salts of aqueous solutions of polymers containing vinylamine groups by ultrafiltration to achieve a residual salt content of 1 to 10 % by weight based on total solution solids in the polymer solution comprising feeding an aqueous salt-containing solution of vinylamine group containing polymers at a polymer concentration of at least 7 % by weight to an ultrafiltration unit and removing the water-soluble salts with the permeate from the feed solution by adding thereto less than 4 parts by weight of water per one part by weight of the feed solution, and use of the polymer of the aqueous solutions thus purified as basic water-absorbing resin of multicomponent superabsorbent polymers. Preferably vibratory shear membranes in a diafiltration configuration are used.

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