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1. 发明授权

EP1805162B1 VERFAHREN ZUR HERSTELLUNG VON TRIOXAN DADURCH GEKENNZEICHNET, DASS BEI DER ERSTEN DESTILLATIONSTUFE EIN WASSERHALTIGER SEITENSTROM ABGEZOGEN WIRD 有权
标题翻译：用于生产三氧杂环己烷，其中所述第一级蒸馏的水 - 侧流扣将
公开(公告)号：EP1805162B1
公开(公告)日：2008-01-23
申请号：EP05798084.9
申请日：2005-10-20
申请人： BASF AKTIENGESELLSCHAFT
发明人： SIEGERT, Markus , LANG, Neven , STROEFER, Eckhard , STAMMER, Achim , FRIESE, Thorsten
IPC分类号： C07D323/06
CPC分类号： C07D323/06
摘要： The invention relates to a trioxane production method comprising the following stages: catalysed reaction in an acid medium of an aqueous highly concentrated formaldehyde solution (1) in a reactor (R) for obtaining a trioxane/formaldehyde/water mixture (2) (stage I); distillation of said trioxane/formaldehyde/water mixture (2) of the stage I for obtaining a raw trioxane as a head flow (3) (stage II), distillation treatment of the raw dioxane of the stage II in one or several stages for obtaining a pure dioxane (8), wherein a side aqueous flow (4) is deducted during the stage II.

2. 发明公开

EP1699776A1 VERFAHREN ZUR ABTRENNUNG VON TRIOXAN AUS EINEM TRIOXAN/FORMALDEHYD/WASSER-GEMISCH MITTELS DRUCKWECHSEL-REKTIFIKATION 有权
标题翻译：方法分离三恶烷的三恶烷/甲醛/水混合物在压力变化精馏的方式
公开(公告)号：EP1699776A1
公开(公告)日：2006-09-13
申请号：EP04804133.9
申请日：2004-12-21
申请人： BASF Aktiengesellschaft
发明人： SIEGERT, Markus , LANG, Neven , STROEFER, Eckhard , STAMMER, Achim , FRIESE, Thorsten , HASSE, Hans
IPC分类号： C07D323/06
CPC分类号： C07D323/06
摘要： The invention relates to a method for separating trioxane from an inlet flow (I) consisting of formaldehyde, trioxane and water. Said method consists in a) preparing an inlet flow (I), which contains formaldehyde as the main component and trioxane and water as auxiliary components, b) mixing the inlet flow (I) with a return flow (VII) containing trioxane as the main component and formaldehyde and water as auxiliary components. An inlet flow (Ia), which contains formaldehyde as the main component and trioxane and water as the auxiliary components, is obtained. Said method also consists in c) distilling the inlet flow (Ia) in a first distillation step at a pressure of between 0.1 2.5 bars, thus enabling a flow (II), which contains formaldehyde as the main component and water as the auxiliary component, and a flow (III), which contains trioxane as the main component and water and formaldehyde as the auxiliary components, to be obtained, d) distilling the flow (III), optionally after separating materials at a low-boiling point from the flow (III) in a low-boiling separation step and in a second distillation step at a pressure of between 0.2 17.5 bars, whereby the pressure in the second distillation step is 0.1 - 15 bars higher than the pressure in the first distillation step. A flow (IV) is obtained which is essentially made of trioxane, and also a flow V which contains trioxane as the main component and water and formaldehyde as the auxiliary components, e) optionally mixing the flow (V) with a flow (IX), which contains water as the main component, in order to obtain a flow (Va) having a higher water content than flow (V), whereby flow (Va) contains trioxane as the main component and water and formaldehyde as the auxiliary components, f) distilling the flow (V) and/or flow (Va) in a third in distillation step at a pressure of between 1 - 10 bars, whereby a flow (VI), which is essentially made of water, and the return flow (VII), which contains trioxane as the main component and water and formaldehyde as the auxiliary components, are obtained.

3. 发明公开

EP1699551A1 VERFAHREN ZUR HERSTELLUNG VON FORMALDEHYD 审中-公开
标题翻译：用于生产甲醛
公开(公告)号：EP1699551A1
公开(公告)日：2006-09-13
申请号：EP04804266.7
申请日：2004-12-23
申请人： BASF Aktiengesellschaft
发明人： OLBERT, Gerhard , JOHANN, Thorsten , WEBER, Markus , LANG, Neven , HARTH, Klaus , STRÖFER, Eckhard , FIENE, Martin , SIEGERT, Markus
IPC分类号： B01J8/02
CPC分类号： F28D9/0031 , B01J8/0214 , B01J8/0285 , B01J8/0415 , B01J8/0419 , B01J8/0496 , B01J19/249 , B01J2208/0015 , B01J2208/00513 , B01J2208/025 , B01J2219/1923 , B01J2219/2453 , B01J2219/2455 , B01J2219/2458 , B01J2219/2459 , B01J2219/2462 , B01J2219/2481 , B01J2219/2485 , C07C45/38 , F28F2250/104 , C07C47/04
摘要： The invention relates to a method for the production of formaldehyde by gas phase oxidation of methanol vapour with a gas flow containing a molecular oxygen in the presence of solid bed catalyst containing iron and molybdenum. The invention is characterised in that the method is carried out in a reactor (1) comprising thermal sheet metal plates (2) which are arranged at a distance from each other and in the longitudinal direction of the reactor (1), said thermal sheet metal plates being cross-flown by a heat carrier. The reactor also comprises devices for supplying and withdrawing (3, 4) the heat carrier to/from the thermal sheet steel plates (2), and gaps (5), which are disposed between the thermal sheet steel metal plates (2) and which are filled with the solid bed catalyst and are introduced into the gas flow containing the methanol vapour and the molecular oxygen.

4. 发明授权

EP1636158B1 VERFAHREN ZUR DESTILLATIVEN TRENNUNG EINES VINYLETHER UND ALKOHOL ENTHALTENDEN GEMISCHS 有权
标题翻译： PROCESS FOR的混合物含醇的乙烯基醚精馏分离和
公开(公告)号：EP1636158B1
公开(公告)日：2007-10-10
申请号：EP04739689.0
申请日：2004-06-08
申请人： BASF Aktiengesellschaft
发明人： KLASS, Katrin , BECKER, Heike , VOGELSANG, Regina , HAUK, Alexander , SIEGERT, Markus , HENKELMANN, Jochem
IPC分类号： C07C43/16 , C07C41/42 , C07C41/08 , C07C29/82
CPC分类号： C07C29/82 , C07C41/08 , C07C41/42 , Y10S203/20 , C07C43/16 , C07C31/08 , C07C31/10 , C07C31/12
摘要： The invention relates to a method for the distillative separation of a mixture containing a vinyl ether of general formula (I) R -O-CH=CH2 and an alcohol of general formula (II) R -OH, in which R and R independently of one another represent a saturated or unsaturated, aliphatic or cycloaliphatic group with between 2 and 10 carbon atoms and the alcohol (II) has a boiling point that is at least 1 DEG C higher than that of the vinyl ether (II), when measured at or extrapolated to 0.1 MPa abs. According to said method a) the mixture is fed into a first distillation column and an azeotrope containing a vinyl ether (I) and an alcohol (II) is extracted as the head product and a stream containing a concentration of alcohol (II) is extracted as the sump product; b) the azeotrope containing the vinyl ether (I) and the alcohol (II) is then fed from the first distillation column into a second distillation column, which is operated at a pressure that is 0.01 to 3 MPa higher than that of the first distillation column, where the vinyl ether (I) is extracted as the sump product or as a gaseous lateral discharge in the stripping section and an azeotrope containing a vinyl ether (I) and alcohol (II) is extracted as the head product; and c) the azeotrope containing the vinyl ether (I) and alcohol (II) is fed back from the second distillation column into the first distillation column.

5. 发明公开

EP1781634A1 VERFAHREN ZUR DESTILLATIVEN ABTRENNUNG VON REIN-TRIOXAN 审中-公开
标题翻译： PROCESS纯三恶烷在蒸馏分离
公开(公告)号：EP1781634A1
公开(公告)日：2007-05-09
申请号：EP05775120.8
申请日：2005-08-18
申请人： BASF Aktiengesellschaft
发明人： SIEGERT, Markus , LANG, Neven , STROEFER, Eckhard , STAMMER, Achim , FRIESE, Thorsten
IPC分类号： C07D323/06 , B01D3/14
CPC分类号： B01D3/146 , B01D3/141 , C07D323/06
摘要： The invention relates to a method for the separation by distillation of pure trioxane from a supply flow (I) containing trioxane in a mass proportion of at least 50 wt. % in relation to the total weight of the supply flow (I), in addition to formaldehyde and water. Said method is characterised in that the supply flow (I) and another flow (II) which contains water but does not contain any constituents foreign to the supply flow, are supplied to a dividing wall column (TWK1) comprising an essentially perpendicular dividing wall TW which divides the inside of the column into a supply region (A1), a delivery region (B1), an upper common column region (C1), and a lower common column region (D1). A bottom flow (III) containing pure trioxane and a lateral flow (IV) containing pure water are removed from the delivery region (B1), at the first dividing wall column (TWK1).

6. 发明授权

EP1625107B1 KONTINUIERLICHES VERFAHREN ZUR HERSTELLUNG VON METHYLVINYLETHER 有权
标题翻译：连续方法生产甲基
公开(公告)号：EP1625107B1
公开(公告)日：2007-12-19
申请号：EP04727886.6
申请日：2004-04-16
申请人： BASF Aktiengesellschaft
发明人： KLASS, Katrin , BECKER, Heike , VOGELSANG, Regina , HAUK, Alexander , SIEGERT, Markus , HENKELMANN, Jochem
IPC分类号： C07C41/08 , C07C43/16
CPC分类号： C07C41/08 , C07C43/16
摘要： The invention relates to a method for continuously producing methyl vinyl ether by reacting methanol with ethyne in the liquid phase in the presence of a basic alkali metal compound or alkaline earth metal compound at a temperature ranging from 40 to 300 DEG C and under a pressure ranging from 0.1 to 5 MPa abs. According to the invention, the reaction is carried out in the absence of a continuous gas phase and with a methyl vinyl ether concentration in the entire liquid phase of = 30 % by weight.

7. 发明授权

EP1654215B1 VERFAHREN ZUR HERSTELLUNG VON ETHYLENAMINEN 有权
公开(公告)号：EP1654215B1
公开(公告)日：2006-11-02
申请号：EP04741043.6
申请日：2004-07-15
申请人： BASF Aktiengesellschaft
发明人： FRAUENKRON, Matthias , KRUG, Thomas , EVERS, Holger , MELDER, Johann-Peter , RÖTTGER, Roderich , SIEGERT, Markus , GERLACH, Till , NOUWEN, Jan , DAHLHOFF, Ellen , MILLER, Christian
IPC分类号： C07C209/64 , C07C211/14
CPC分类号： C07C209/64 , C07C211/14
摘要： The invention relates to a method for producing ethylene-amines, in particular, diethylenetriamine (DETA), by continuous reaction of ethylenediamine (EDA) in the presence of a heterogeneous catalyst, wherein said reaction is carried out in a reaction column.
摘要翻译：本发明涉及通过乙二胺（EDA）在非均相催化剂存在下的连续反应生产乙烯胺，特别是二亚乙基三胺（DETA）的方法，其中所述反应在反应塔中进行。

8. 发明公开

EP1680393A1 VERFAHREN ZUR DESTILLATIVEN AUFTRENNUNG VON GEMISCHEN ENTHALTEND ETHYLENAMINE 失效转让
标题翻译：法将混合物分离乙撑胺含
公开(公告)号：EP1680393A1
公开(公告)日：2006-07-19
申请号：EP04765964.4
申请日：2004-10-15
申请人： BASF Aktiengesellschaft
发明人： SIEGERT, Markus , MELDER, Johann-Peter , KRUG, Thomas , NOUWEN, Jan
IPC分类号： C07C209/84 , C07C209/86 , B01D3/32 , B01J19/32 , C07D295/02
CPC分类号： C07D295/023 , B01D3/141 , B01D3/146 , C07C209/86 , C07C213/10 , C07C211/10 , C07C211/14 , C07C215/14 , C07C215/08
摘要： Disclosed is a method for the distillative separation of mixtures containing ethyleneamines, the separation process being carried out in one or several fractionation columns. The ethyleneamines particularly represent ethylenediamine (EDA), piperazine (PIP), diethylenetriamine (DETA), aminoethylethanolamine (AEEA), and/or monoethanolamine (MEOA).

9. 发明公开

EP1625107A2 KONTINUIERLICHES VERFAHREN ZUR HERSTELLUNG VON METHYLVINYLETHER 有权
标题翻译：连续方法生产甲基
公开(公告)号：EP1625107A2
公开(公告)日：2006-02-15
申请号：EP04727886.6
申请日：2004-04-16
申请人： BASF Aktiengesellschaft
发明人： KLASS, Katrin , BECKER, Heike , VOGELSANG, Regina , HAUK, Alexander , SIEGERT, Markus , HENKELMANN, Jochem
IPC分类号： C07C41/08 , C07C43/16
CPC分类号： C07C41/08 , C07C43/16
摘要： The invention relates to a method for continuously producing methyl vinyl ether by reacting methanol with ethyne in the liquid phase in the presence of a basic alkali metal compound or alkaline earth metal compound at a temperature ranging from 40 to 300 °C and under a pressure ranging from 0.1 to 5 MPa abs. According to the invention, the reaction is carried out in the absence of a continuous gas phase and with a methyl vinyl ether concentration in the entire liquid phase of ≤ 30 % by weight.

10. 发明授权

EP1654214B1 VERFAHREN ZUR HERSTELLUNG VON ETHYLENAMINEN 有权转让
标题翻译：工艺生产乙烯AMINES
公开(公告)号：EP1654214B1
公开(公告)日：2007-03-28
申请号：EP04740778.8
申请日：2004-07-08
申请人： BASF Aktiengesellschaft
发明人： FRAUENKRON, Matthias , EVERS, Holger , MELDER, Johann-Peter , RÖTTGER, Roderich , SIEGERT, Markus , GERLACH, Till , NOUWEN, Jan , KRUG, Thomas
IPC分类号： C07C209/16 , C07C211/10 , C07C211/14
CPC分类号： C07C209/16 , C07C211/10 , C07C211/14
摘要： The invention relates to the production ethyleneamines by reacting monoethanolamine (MEOA) with ammonia in the presence of a catalyst inside a reactor (1) and by separating the resulting reaction discharge. During separation, the ethylenediamine (EDA) obtained is reacted inside a separate reactor (2) in the presence of a catalyst to form diethylenetriamine (DETA), and the resulting reaction discharge is fed to the separation of the reaction discharge resulting from the reactor (1).

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