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1. 发明公开

EP3362427A1 PRODUCTION OF PROPYLENE GLYCOL MONOALKYL ETHER 有权
公开(公告)号：EP3362427A1
公开(公告)日：2018-08-22
申请号：EP16787662.2
申请日：2016-10-11
申请人： Lyondell Chemical Technology, L.P.
发明人： LI, Xiangmin , CANDELA, Lawrence, M. , LEIPA, Mark, A. , LEYSHON, David, W.
IPC分类号： C07C41/03 , C07C43/13
CPC分类号： C07C41/03 , C07C41/42 , C07C41/44 , C07C43/13
摘要： Processes for producing propylene glycol monoalkyl ether are described herein and include contacting propylene oxide and an alcohol in the presence of an alkali or alkaline earth metal alkoxide catalyst to produce an alkoxylation mixture including propylene glycol monoalkyl ether; distilling the alkoxylation mixture to produce a first overhead stream including propylene oxide and the alcohol and a first bottoms stream including propylene glycol monoalkyl ether; distilling the first bottoms stream to produce a second overhead stream including purified propylene glycol monoalkyl ether and a second bottoms stream including heavier byproducts; further distilling the second bottoms stream to form a resulting bottoms stream including caustic and heavier byproducts; introducing an alkali metal borohydride into at least a portion of the resulting bottoms stream to form an alkali metal borohydride containing stream; and introducing the alkali metal borohydride containing stream into one or more distillations upstream of recovery of the second overhead stream.

2. 发明授权

EP3092053B1 VERFAHREN ZUR TRENNTECHNISCHEN BEARBEITUNG EINES PRODUKTSTROMS EINES DIMETHYLETHERREAKTORS 有权
标题翻译：分离处理二甲醚反应器产物流体的方法
公开(公告)号：EP3092053B1
公开(公告)日：2017-10-25
申请号：EP15700038.1
申请日：2015-01-05
申请人： Linde Aktiengesellschaft
发明人： FRITZ, Helmut , PESCHEL, Andreas
IPC分类号： B01D53/14 , B01D3/14 , C07C41/42 , C07C41/40
CPC分类号： C07C41/42 , B01D3/143 , B01D53/1493 , B01D2257/108 , B01D2257/502 , B01D2257/504 , B01D2257/80 , C07C41/40 , Y02A50/2341 , Y02C10/06 , Y02P20/152 , Y02P70/34 , C07C43/043

3. 发明公开

EP3145901A2 PROCESS FOR GENERATING A MIXED MULTICOMPONENT VAPOR FOR PREPARATION OF MONOALKYL ETHERS OF DIPHENOLS 审中-公开
标题翻译：制造方法联合多组分蒸汽用于生产二酚的单烷基醚
公开(公告)号：EP3145901A2
公开(公告)日：2017-03-29
申请号：EP15795324.1
申请日：2015-05-19
申请人： Camlin Fine Sciences Limited
发明人： SHANBHAG, Anil Purushottam , DUKANE, Arjun Sudhakar
IPC分类号： C07C41/09
CPC分类号： C07C41/09 , B01J8/067 , B01J27/16 , B01J35/023 , B01J35/026 , B01J35/1014 , B01J37/0009 , B01J37/0063 , B01J37/009 , B01J37/0236 , B01J37/031 , B01J37/04 , B01J37/08 , B01J2208/00221 , B01J2208/00256 , B01J2208/0053 , C07C41/42 , C07C43/23
摘要： This invention comprises a process and a system thereof comprising apparatuses for developing multi-component vapor mixture by heating of solution of reactants comprising one or more of diphenols, or diphenol derivatives, and an organic compound, wherein the organic compound is one which upon reacting in a vapor state in presence of a catalyst with diphenols, or diphenol derivatives, produces a monoalkyl ether of a dihydric phenolic compound; and wherein the entire solution of reactants completely transforms into a super-heated multi-component vapor using heaters without the use of thin film evaporator. The complete transformation of the entire solution of said reactants in to super-heated multicomponent vapor is achieved by heating the entire solution firstly by a pre-heater followed by further heating by a super-heater, further comprising removal of the unevaporated or condensed high boilers and tar to drain, and subjecting the superheated vapor to vapor phase reaction mediated by catalyst to get monoalkyl ether of a dihydric phenolic compound.
摘要翻译：本发明包括一种方法和其包括用于通过反应物的溶液中包含一种或多种二酚或二酚衍生物的加热显影多组分蒸汽的混合物的装置的系统，以及有机化合物，worin有机化合物是一个，其在在起反应与二酚或二酚衍生物的催化剂存在下的蒸气状态，产生一个二羟基酚化合物的一烷基醚; 和反应物worin的整个溶液完全呼叫转变成使用加热器，而不使用薄膜蒸发器的过热的多组分蒸汽。所述反应物在对过热多组分蒸汽的整个溶液的完全转化是通过首先加热整个溶液达到预加热器进一步加热随之而来的是过热器，其进一步包括除去未蒸发或冷凝的高沸点的和焦油排出，并对该过热蒸汽为蒸汽通过催化剂介导的获得二羟基酚类化合物的单烷基醚相反应。

4. 发明授权

EP2872241B8 VERFAHREN ZUR VERBESSERUNG DER TRANSPORTFÄHIGKEIT VON SCHWEREM ROHÖL 有权
标题翻译： VERFAHREN ZUR VERBESSERUNG DERTRANSPORTFÄHIGKEITVON SCHWEREMROHÖL
公开(公告)号：EP2872241B8
公开(公告)日：2017-03-29
申请号：EP13782649.1
申请日：2013-08-22
申请人： Wagner, Ulrich, Dr. , Balthasar, Wolff , Müller, Dierk
发明人： WAGNER, Ulrich , BALTHASAR, Wolff , MÜLLER, Dierk
IPC分类号： C07C29/78 , C10G29/20 , C10G3/00 , C07C41/09 , C07C41/42 , F17D1/16 , F17D1/17 , C07C29/151
CPC分类号： C07C41/42 , C07C29/1518 , C07C29/78 , C07C41/09 , C10G3/42 , C10G29/20 , C10G2300/302 , F17D1/16 , F17D1/17 , Y02P30/20 , C07C31/04 , C07C43/043

5. 发明公开

EP3137446A1 PROCESS FOR PURIFYING METHYL ACETATE MIXTURES 审中-公开
标题翻译：纯化甲酸甲酯混合物的方法
公开(公告)号：EP3137446A1
公开(公告)日：2017-03-08
申请号：EP15728013.2
申请日：2015-06-12
申请人： BP Chemicals Limited
发明人： BRISTOW, Timothy Crispin
IPC分类号： C07C67/37 , C07C67/54 , C07C41/16 , C07C41/42 , C07C51/09 , C07C43/04 , C07C53/08 , C07C69/14
CPC分类号： C07C67/54 , B01D3/143 , B01D3/4205 , C07C41/16 , C07C41/42 , C07C51/09 , C07C67/37 , C07C43/043 , C07C53/08 , C07C69/14
摘要： A process for removing acetaldehyde from a mixture of methyl acetate, dimethyl ether and acetaldehyde comprising distilling mixtures derived from carbonylating dimethyl ether in the presence of a zeolite catalyst to generate an overhead stream depleted in acetaldehyde as compared to the feed mixture, a base stream depleted in acetaldehyde as compared to the feed mixture and a sidedraw stream enriched in acetaldehyde as compared to the feed mixture and withdrawing from the column the sidedraw stream enriched in acetaldehyde at a point above the feed point of the feed mixture to the column. Purified mixtures may be utilised as feedstock to processes for the co-production of acetic acid and dimethyl ether.
摘要翻译：一种从乙酸甲酯，二甲醚和乙醛的混合物中除去乙醛的方法，该方法包括在沸石催化剂存在下蒸馏衍生自羰基化二甲醚的混合物以产生与进料混合物相比贫化乙醛的塔顶物流，贫化的碱流在乙醛中与进料混合物和富含乙醛的侧馏分流相比，与进料混合物相比并且从塔中排出的侧馏分流在塔进料混合物进料点之上的点处富含乙醛。纯化的混合物可以用作乙酸和二甲醚联产的方法的原料。

6. 发明公开

EP3092053A1 VERFAHREN ZUR TRENNTECHNISCHEN BEARBEITUNG EINES PRODUKTSTROMS EINES DIMETHYLETHERREAKTORS 有权
公开(公告)号：EP3092053A1
公开(公告)日：2016-11-16
申请号：EP15700038.1
申请日：2015-01-05
申请人： Linde Aktiengesellschaft
发明人： FRITZ, Helmut , PESCHEL, Andreas
IPC分类号： B01D53/14 , B01D3/14 , B01D5/00 , C07C41/34 , C07C41/42 , C07C43/04 , F25J3/06
CPC分类号： C07C41/42 , B01D3/143 , B01D53/1493 , B01D2257/108 , B01D2257/502 , B01D2257/504 , B01D2257/80 , C07C41/40 , Y02A50/2341 , Y02C10/06 , Y02P20/152 , Y02P70/34 , C07C43/043
摘要： The invention relates to a separation processing method for a product stream (g) of a reactor (4) used for the synthesis of dimethyl ether (z) from synthesis gas (e), said product stream containing at least dimethyl ether, methanol, water, carbon dioxide, carbon monoxide and hydrogen. The product stream (g) is fed into a liquid reflux-operated absorption column (6) at least partially in a gaseous state, wherein a gaseous top stream (m) is removed from the absorption column (6) at the top end, and a liquid bottom stream (p) is removed at the bottom end of the absorption column. At least part of the bottom stream (p) is fed into a first distillation column (5), wherein a gaseous transfer stream (q) containing dimethyl ether, and a stream (r) predominantly containing methanol and/or water are removed from the first distillation column (5). At least part of the top stream (m) is first cooled to a first temperature level and subsequently further cooled to one or more additional temperature levels, wherein a first condensate stream (n) is formed after the cooling to the first temperature level, and one or more additional condensate streams (s, t) are formed after the further cooling to the additional temperature level(s). Part of the first condensate stream (n) is used to form the liquid reflux, and at least part of the additional condensate stream(s) (s, t) are fed into an additional distillation column (9), from which a liquid stream (z) is removed at the bottom end, said liquid stream substantially containing dimethyl ether and having little or no carbon dioxide. The invention also relates to a corresponding separation plant and a plant (100) for producing dimethyl ether.
摘要翻译：通过分离技术从用于合成二甲醚的反应器（4）中处理至少含有二甲醚，甲醇，水，二氧化碳，一氧化碳和氢气的产物流（g）的方法（ z）由合成气（e）提出。将产物流（g）以至少部分气态形式进料到用液体回流操作的吸收塔（6）中，从顶部的吸收塔（6）除去气态顶部流（m）液底池（p）在底部被移除。贮槽料流（p）至少部分地进料到第一蒸馏塔（5）中，含有二甲醚的气态转移料流（q）和主要含有甲醇和/或水的料流（r）从第一蒸馏塔（5）。顶部流（m）至少部分地冷却至第一温度水平，随后进一步冷却至一个或多个其它温度水平，第一冷凝物流（n）在冷却至第一温度水平之后形成，并且一个或多个在进一步冷却到另外的温度水平或水平之后形成另外的冷凝物流（s，t）。第一冷凝物流（n）被部分地用于形成液体回流，并且另外的冷凝物流（s，t）至少部分地进料到另外的蒸馏塔（9）中，液体流），主要含有二甲醚，二氧化碳不足或不含二氧化碳。本发明还涉及相应的分离装置和用于生产二甲醚的装置（100）。

7. 发明公开

EP2780309A1 VERFAHREN ZUR GEWINNUNG VON DI-TRIMETHYLOLPROPAN UND MIT TRIMETHYLOLPROPAN ANGEREICHERTEN PRODUKTSTRÖMEN AUS DEN NEBENSTRÖMEN DER TRIMETHYLOLPROPANHERSTELLUNG 有权
标题翻译： VERFAHREN ZUR GEWINNUNG VON DI-TRIMETHYLOLPROPAN UND MIT TRIMETHYLOLPROPAN ANGEREICHERTENPRODUKTSTRÖMENAUS DENNEBENSTRÖMENDER TRIMETHYLOLPROPANHERSTELLUNG
公开(公告)号：EP2780309A1
公开(公告)日：2014-09-24
申请号：EP12783114.7
申请日：2012-10-24
申请人： OXEA GmbH
发明人： FREY, Guido, D. , SCHALAPSKI, Kurt , BERMANN, Dirk , NOWOTNY, Norman , STRUTZ, Heinz , RAFF, Donald, K.
IPC分类号： C07C29/10 , C07C29/80 , C07C29/90 , C07C41/42 , C07C41/44 , C07C31/22 , C07C43/13
CPC分类号： C07D319/06 , C07C29/10 , C07C29/80 , C07C29/84 , C07C29/90 , C07C41/42 , C07C41/44 , C07C31/22 , C07C43/132
摘要： The present invention relates to a method for recovering di-trimethylolpropane and trimethylolpropane-enriched product streams from the high-boiling fractions and residues which arise in the purification of trimethylolpropane by distillation, wherein a solution of these fractions and residues is catalytically hydrogenated in the presence of an acid compound and, after separating off solids, the solution is worked up in a three-stage distillation appliance, in which a trimethylolpropane-enriched product is obtained and, separately therefrom, di-trimethylolpropane is recovered as overhead fraction.
摘要翻译：本发明涉及一种从蒸馏提纯三羟甲基丙烷中产生的高沸点馏分和残余物中回收二 - 三羟甲基丙烷和富含三羟甲基丙烷的产物物流的方法，其中这些馏分和残余物的溶液在存在下催化氢化的酸化合物，并且在分离出固体后，将该溶液在三级蒸馏装置中后处理，其中获得富含三羟甲基丙烷的产物，并且分别从中获得二 - 三羟甲基丙烷作为塔顶馏分。

8. 发明授权

EP2285763B1 PROCESS FOR OLEFIN ETHERIFICATION 无效
标题翻译：方法醚化烯烃
公开(公告)号：EP2285763B1
公开(公告)日：2014-05-07
申请号：EP09743269.4
申请日：2009-04-27
申请人： Dow Global Technologies LLC
发明人： DAUGS, Edward, D. , FLICK, Derrick, W. , RAND, Cynthia, L. , TULCHINSKY, Michael, L. , YU, Wanglin
IPC分类号： C07C41/06 , C07C43/12
CPC分类号： C07C41/06 , C07C41/42 , Y02P20/127 , C07C43/12

9. 发明公开

EP2641896A1 SEPARATION METHOD 有权转让
标题翻译： TRENNVERFAHREN
公开(公告)号：EP2641896A1
公开(公告)日：2013-09-25
申请号：EP12829139.0
申请日：2012-03-30
申请人： Asahi Kasei Chemicals Corporation
发明人： SHINOHATA Masaaki , MIYAKE Nobuhisa
IPC分类号： C07C263/18 , C07C41/58 , C07C43/10 , C07C49/203 , C07C49/213 , C07C235/14
CPC分类号： B01D3/009 , C07C37/74 , C07C41/42 , C07C263/20 , C07C269/08 , C07C331/30 , C07C2601/14 , Y02P20/127 , C07C265/14 , C07C271/12 , C07C271/44
摘要： The present invention provides a separation method of separating (A) and (B), comprising: a step of separating at least either an active hydrogen-containing compound (A) or a compound (B) that reversibly reacts with (A) from a mixture containing (A) and (B) by distillation in a multistage distillation column; and a step of supplying the mixture to an inactive region formed within the multistage distillation column.
摘要翻译：本发明提供分离（A）和（B）的分离方法，其包括：将与（A）可逆反应的活性氢化合物（A）或化合物（B）中的至少一种从在多级蒸馏塔中通过蒸馏含有（A）和（B）的混合物; 以及将混合物供给到形成在多级蒸馏塔内的非活性区域的步骤。

10. 发明公开

EP2623488A1 Process for olefin etherification 有权
标题翻译： Verfahren zur Etherifizierung von Olefinen
公开(公告)号：EP2623488A1
公开(公告)日：2013-08-07
申请号：EP13166518.4
申请日：2009-04-27
申请人： Dow Global Technologies LLC
发明人： Daugs, Edward D. , Flick, Derrick W. , Rand, Cynthia L. , Tulchinsky, Michael L , Yu, Wanglin
IPC分类号： C07C41/06 , C07C43/12
CPC分类号： C07C41/06 , C07C41/42 , Y02P20/127 , C07C43/12
摘要： A process for preparing an ether compound, the process comprising: (a) contacting an olefin with an alcohol in the presence of an etherification catalyst, under etherification conditions, to form an ether compound; (b) recovering the ether compound, unreacted alcohol and unconsumed olefin; and (c) using at least a portion of the unconsumed olefin of step (b) in an etherification process conducted according to step (a), wherein the alcohol is linear or branched alcohol alkyl containing one or two alcohol groups, and further substituted with 1, 2, or 3 activating groups independently selected from CN, NO 2 , F, Cl, Br, I, C 1 -C 6 alkoxy, and -C(O)O-alkyl.
摘要翻译：一种制备醚化合物的方法，该方法包括：（a）在醚化条件下，在醚化催化剂存在下，使烯烃与醇接触以形成醚化合物; （b）回收醚化合物，未反应的醇和未消耗的烯烃; 和（c）在根据步骤（a）进行的醚化方法中使用步骤（b）的未消耗烯烃的至少一部分，其中所述醇是含有一个或两个醇基的直链或支链醇烷基，并进一步被 1,2或3个独立地选自CN，NO 2，F，Cl，Br，I，C 1 -C 6烷氧基和-C（O）O-烷基的活化基团。

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