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1. 发明公开

EP3301087A1 PROCESS FOR PREPARING CHIRAL AMINES 审中-公开
标题翻译：制备手性胺的方法
公开(公告)号：EP3301087A1
公开(公告)日：2018-04-04
申请号：EP16191845.3
申请日：2016-09-30
申请人： DPx Fine Chemicals Austria GmbH & Co KG
发明人： de Vries, Andre , Lefort, Laurent , Verzijl, Gerard
IPC分类号： C07D211/56
CPC分类号： C07D211/56
摘要： The invention pertains to a process for the preparation of an amine having at least two chiral centers from a ketone having a chiral center at the α position and an amine comprising the steps of:
(a) contacting a ketone having a chiral center at the α position and a primary amine thereby forming an imine;
(b) contacting the imine with a reducing agent in the presence of an enantioselective catalyst to form an amine having at least two chiral centers,
wherein step (a) and/or step (b) are conducted under racemization-enhancing conditions, wherein the racemization-enhancing conditions are achieved by addition of an acid and/or by addition of a salt of a primary amine and an acid, which salt is added in addition to or instead of the primary amine, and wherein the reducing agent is hydrogen.
摘要翻译：本发明涉及由α位具有手性中心的酮和胺制备具有至少两个手性中心的胺的方法，该方法包括以下步骤：（a）使在α位具有手性中心的酮与α 位置和伯胺从而形成亚胺; （b）使亚胺与还原剂在对映选择性催化剂存在下接触以形成具有至少两个手性中心的胺，其中步骤（a）和/或步骤（b）在外消旋化增强条件下进行，其中通过加入酸和/或通过加入伯胺和酸的盐实现外消旋化增强条件，除了伯胺之外或代替伯胺添加盐，并且其中还原剂是氢。

2. 发明授权

EP2635548B8 CONTINUOUS PRODUCTION AND REACTION OF A DIAZO COMPOUND 有权转让
标题翻译：连续生产和反应FROM重氮CONNECTIONS
公开(公告)号：EP2635548B8
公开(公告)日：2015-02-18
申请号：EP11778584.0
申请日：2011-11-01
申请人： DPx Fine Chemicals Austria GmbH & Co KG
发明人： REINTJENS, Rafael, Wilhelmus, Elisabeth, Ghislain , DIELEMANS, Hubertus, Johannes, Adrianus , THATHAGAR, Mehul , KONINGS, Jeroen, Hubertina, Gerardus , POECHLAUER, Peter
IPC分类号： C07C67/00 , C07C69/78 , C07C245/14 , C07C245/16
CPC分类号： C07C245/16 , C07C67/00 , C07C245/14 , C07D231/06 , C07C69/78

3. 发明公开

EP2882798A1 PROCESS FOR DRYING POLYMERIC MATERIALS 有权转让
标题翻译：过程进行干燥高分子材料
公开(公告)号：EP2882798A1
公开(公告)日：2015-06-17
申请号：EP13750678.8
申请日：2013-08-09
申请人： DPx Fine Chemicals Austria GmbH & Co KG
发明人： HANBAUER, Martin Helmut Friedrich , LANDSCHÜTZER, Herwig
IPC分类号： C08J3/00 , C08F6/00 , F26B3/08 , F26B7/00
CPC分类号： F26B3/00 , A61K31/78 , A61K31/785 , C08F6/008 , C08F220/06 , C08G73/02 , C08J3/00 , C08J2333/02 , C08J2379/02 , F26B1/00 , F26B3/06 , F26B3/08 , F26B5/005 , F26B7/00 , F26B21/14 , F26B2200/08
摘要： The invention relates to a process for drying a moist polymeric material to obtain a dried polymeric material, comprising the steps of: mixing the moist polymeric material with an aqueous solution of a carbohydrate to afford a mixture of the moist polymeric material with the carbohydrate; and heating and/or filtering the mixture of the moist polymeric material with the carbohydrate to remove an amount of volatiles to obtain a predried polymeric material having a volatiles content VCpre-dried (pre-drying step); fluidizing the pre-dried material in a fluidized bed in order to further remove an amount of volatiles to obtain the dried polymeric material having a volatiles content VCdried (fluidized bed drying step); and withdrawing and collecting the dried polymeric material from the fluidized bed; wherein VCpre-dried is higher than VCdried and the moist polymeric material comprises at least a polymeric material, said polymeric material comprises fluorine permanently bonded to said polymeric material. The invention further relates to a dried polymeric material obtainable by the process of the invention. Furthermore, the invention relates to various uses of the process of the invention as well as to various uses of the dried polymeric materials.

4. 发明公开

EP2864286A1 PROCESS FOR THE MANUFACTURE OF ALKYLFLUOROACRYLATE 有权转让
标题翻译：制备烷基氟丙烯酸酯的方法
公开(公告)号：EP2864286A1
公开(公告)日：2015-04-29
申请号：EP13730917.5
申请日：2013-06-25
申请人： DPx Fine Chemicals Austria GmbH & Co KG
发明人： KAPITAN, Peter , SAJTOS, Alexander
IPC分类号： C07C67/343 , C07C69/732 , C07C67/32 , C07C69/653 , C07C67/52 , C07C67/54
CPC分类号： C07C67/54 , C07C67/32 , C07C67/343 , C07C67/52 , C07C69/653 , C07C69/732
摘要： The invention relates to a process for the manufacture of an alkylfluoroacrylate starting from alkylfluoroacetate and an oxalic acid ester, wherein an alkane liquid under the reaction conditions is applied as the solvent in one of the reaction steps.
摘要翻译：本发明涉及从氟代乙酸烷基酯和草酸酯开始制造氟代丙烯酸烷基酯的方法，其中在反应条件之一的烷烃液体作为溶剂在一个反应步骤中使用。

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