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61. 发明授权

EP1569872B1 PROCESS FOR MIXING AN ACIDIC AQUEOUS SOLUTION COMPRISING HYDROXYLAMMONIUM AND PHOSPHATE WITH NITRIC ACID 有权
标题翻译：方法合剂酸性溶液中含硝酸羟胺和磷酸盐
公开(公告)号：EP1569872B1
公开(公告)日：2006-05-24
申请号：EP03786406.3
申请日：2003-12-10
申请人： DSM IP Assets B.V.
发明人： BENNEKER, Arno, Herald , OEVERING, Hendrik
IPC分类号： C01B21/14 , C07C249/08
CPC分类号： C07C249/08 , C01B21/1418
摘要： The invention relates to a process for mixing a first acidic aqueous solution comprising hydroxylammonium and phosphate with a second acidic aqueous solution comprising nitric acid at a temperature between 20 and 80 °C resulting in a third acidic aqueous solution comprising hydroxylammonium, phosphate and nitric acid, wherein in the third acidic aqueous solution the total acid concentration minus the phosphate concentration is lower than 0.523 * ln([hydroxylammonium]/1.25) + 422/(T + 81) whereby [hydroxylammonium] is the concentration of hydroxylammonium in the third acidic aqueous solution, T is the temperature of the third acidic aqueous solution expressed in °C and all concentrations are expressed in mol/l.

62. 发明授权

EP1451100B1 PROCESS FOR TREATING AN AQUEOUS MEDIUM CONTAINING PHOSPHATE SALT AND ORGANIC COMPOUNDS 有权
标题翻译：方法磷酸盐的处理和有机化合物的含水介质
公开(公告)号：EP1451100B1
公开(公告)日：2006-04-05
申请号：EP02783844.0
申请日：2002-12-02
申请人： DSM IP Assets B.V.
发明人： BENNEKER, Arno , OEVERING, Henk , BROUWERS, Johannes, Antonius, Leonardus
IPC分类号： C01B21/40 , C07C249/08
CPC分类号： C01B21/40 , C01B21/1418
摘要： The invention relates to a process for preparing nitric acid by treating an aqueous medium containing organic compounds and phosphate, said process comprising: feeding the aqueous medium to a nitric acid synthesis zone, forming nitric acid by contacting the aqueous medium with a gaseous medium in said nitric acid synthesis zone, said gaseous medium containing NO2; discharging an off-gas from said nitric acid synthesis zone; wherein the total organic carbon concentration in the aqueous medium entering the nitric acid synthesis zone is less than 0.03 wt %.

63. 发明公开

EP1468986A1 Method for producing cyclohexanone oxime 审中-公开
标题翻译： Verfahren zur Herstellung von Cyclohexanonoxim
公开(公告)号：EP1468986A1
公开(公告)日：2004-10-20
申请号：EP04008446.9
申请日：2004-04-07
申请人： Sumitomo Chemical Company, Limited
发明人： Oikawa, Miyuki , Fukao, Masami
IPC分类号： C07C249/04 , C07C249/08 , B01J29/89 , C07C251/44
CPC分类号： C07C249/04 , B01J29/89 , B01J29/90 , Y02P20/584 , C07C251/44
摘要： In producing cyclohexanone oxime by a method comprising the step of reacting cyclohexanone, hydrogen peroxide and ammonia in the presence of titanium silicate, a brand-new titanium silicate and a recycled titanium silicate which has been recovered from a production method of cyclohexanone oxime are used. In accordance with the present invention, cyclohexanone is subjected to ammoximation by hydrogen peroxide and ammonia with suppressing the degradation of titanium silicate as a catalyst, to produce cyclohexanone oxime with a high yield.
摘要翻译：通过包括在硅酸钛存在下使环己酮，过氧化氢和氨反应的方法制备环己酮肟的方法，使用从环己酮肟的制备方法中回收的全新钛硅酸盐和再循环的硅酸钛。根据本发明，通过过氧化氢和氨对环己酮进行氨肟化，抑制硅酸钛作为催化剂的降解，以高产率制备环己酮肟。

64. 发明公开

EP0945431A3 Verfahren und Zwischenprodukte zur Herstellung von Phenylessigsäurederivaten 失效
标题翻译： Verfahren und Zwischenprodukte zur Herstellung vonPhenylessigsäurederivaten
公开(公告)号：EP0945431A3
公开(公告)日：2004-08-18
申请号：EP99107871.8
申请日：1995-01-03
申请人： BASF AKTIENGESELLSCHAFT
发明人： Bayer, Herbert, Dr. , Sauter, Hubert, Dr. , Müller, Ruth, Dr. , Grammenos, Wassilios, Dr. , Harreus, Albrecht, Dr. , Kirstgen, Reinhard, Dr. , Röhl, Franz, Dr. , Ammermann, Eberhard, Dr. , Lorenz, Gisela, Dr.
IPC分类号： C07C249/08 , C07C251/48 , C07C251/38
CPC分类号： C07D207/333 , A01N37/36 , A01N37/50 , A01N43/08 , A01N43/36 , A01N43/40 , A01N43/54 , A01N43/76 , A01N43/78 , A01N43/80 , A01N43/88 , C07C249/08 , C07C251/38 , C07C251/48 , C07C251/60 , C07C327/58 , C07C2601/02 , C07C2601/04 , C07C2601/08 , C07C2601/14 , C07D213/53 , C07D213/64 , C07D239/34 , C07D239/36 , C07D261/08 , C07D261/10 , C07D263/32 , C07D271/06 , C07D277/24 , C07D307/12
摘要： Verfahren und Zwischenprodukte zur Herstellung von Phenylessigsaurederivaten der Formel I in der die Substituenten und der Index die folgende Bedeutung haben: X NOCH 3 , CHOCH 3 , CHCH 3 und CHCH 2 CH 3 ; R 1 Wasserstoff und Alkyl; R 2 Cyano, Nitro, Trifluormethyl, Halogen, Alkyl und Alkoxy; m 0, 1 oder 2, wobei die Reste R 2 verschieden sein können, wenn m für 2 steht; R 3 Wasserstoff, Cyano, Nitro, Hydroxy, Amino, Halogen, Alkyl, Halogenalkyl, Alkoxy, Halogenalkoxy, Alkylthio, Alkylamino oder Dialkylamino; R 4 Wasserstoff, Cyano, Nitro, Hydroxy, Amino, Halogen, ggf. subst. Alkyl, Alkoxy, Alkylthio, Alkylamino, Dialkylamino, Alkenyl, Alkenyloxy, Alkenylthio, Alkenylamino, N-Alkenyl-N-alkylamino, Alkinyl, Alkinyloxy, Alkinylthio, Alkinylamino, N-Alkinyl-N-alkylamino; ggf. subst. Cycloalkyl, Cycloalkyloxy, Cycloalkylthio, Cycloalkylamino, N-Cycloalkyl-N-alkylamino, Cycloalkenyl, Cycloalkenyloxy, Cycloalkenylthio, Cycloalkenylamino, N-Cycloalkenyl-N-alkylamino, Heterocyclyl, Heterocyclyloxy, Heterocyclylthio, Heterocyclylamino, N-Heterocyclyl-N-alkylamino, Aryl, Aryloxy, Arylthio, Arylamino, N-Aryl-N-alkylamino, Hetaryl, Hetaryloxy, Hetarylthio, Hetarylamino, N-Hetaryl-N-alkylamino; R 5 Wasserstoff, ggf. subst. Alkyl, Cycloalkyl, Alkenyl, Alkinyl, Alkylcarbonyl, Alkenylcarbonyl, Alkinylcarbonyl oder Alkylsulfonyl; ggf. subst. Aryl, Arylcarbonyl, Arylsulfonyl, Hetaryl, Hetarylcarbonyl oder Hetarylsulfonyl.
摘要翻译：苯乙酸衍生物。式（I）化合物及其盐。 X = NOMe CHOMe，CHMe或CHEt; R 1 = H或Q; m = 0,1或2; R 2 = CN，NO 2，CF 3，卤素，Q或QO; R 3 = H，CN，NO 2，OH，NH 2，卤素，Q，QO，QS，QNH; R 4 = H，Cy，CyO，CyS，CyNH，Ar，ArO，ArS; Q = 1-4C烷基; Cy = 3-6C环烷基; Ar =芳基; R 5 = H，1-10C烷基，Cy，2-10C烯基，2-10C炔基，2-10C烯基羰基，1-10C烷基羰基，3-10C炔基羰基或1-10C烷基磺酰基。

65. 发明公开

EP1445248A1 PROCESSES FOR PREPARATION OF CYCLOPROPYLETHANOL, CYCLO-PROPYLACETONITRILE AND INTERMEDIATES OF BOTH 审中-公开
标题翻译：过程对于这两个连接产生与环丙基CYLCOPROPYLACETONITRIL和中间产品
公开(公告)号：EP1445248A1
公开(公告)日：2004-08-11
申请号：EP02779965.9
申请日：2002-10-31
申请人： Kuraray Co., Ltd.
发明人： UJITA, Katsuji
IPC分类号： C07C31/133 , C07C29/14 , C07C45/58 , C07C47/11 , C07C251/38 , C07C249/08 , C07C255/31 , C07C253/00
CPC分类号： C07C29/14 , C07C45/58 , C07C249/08 , C07C251/38 , C07C253/00 , C07C255/31 , C07C2601/02 , C07C47/11 , C07C31/1333
摘要： A process for preparation of cyclopropylethanol, which comprises subjecting a 3-cyclopropyl-2,3-epoxypropionic acid ester to solvolysis, treating the product of the solvolysis with an acid to obtain cyclopropylacetaldehyde, and reducing the obtained cyclopropylacetaldehyde; and a process for preparation of cyclopropylacetonitrile, which comprises subjecting a 3-cyclopropyl-2,3-epoxypropionic acid ester to solvolysis in the presence of a base, treating the product of the solvolysis with an acid to obtain cyclopropylacetaldehyde, reacting the obtained cyclopropylacetaldehyde with hydroxylamine or salts thereof to obtain cyclopropaneacetaldehyde oxime, and reacting the obtained cyclopropaneacetaldehyde oxime with acetic anhydride. According to the present invention, cyclopropylethanol and cyclopropylacetonitrile can be prepared at low costs and industrially advantageously.

66. 发明公开

EP1421061A1 OXIME DERIVATIVES FOR THE TREATMENT OF DYSLIPIDEMIA AND HYPERCHOLESTEREMIA 审中-公开
标题翻译： OXIMDERIVATEFÜRDIE BEHANDLUNG VONDYSLIPIDÄMIEUNDHYPERCHOLESTERINÄMIE
公开(公告)号：EP1421061A1
公开(公告)日：2004-05-26
申请号：EP02794929.6
申请日：2002-08-19
申请人： Incyte San Diego Incorporated
发明人： PFAHL, Magnus , TACHDJIAN, Catherine , AL-SHAMMA, Hussien, A.
IPC分类号： C07C249/08 , C07C251/48 , C07D213/30 , C07D215/06 , C07D215/14 , C07D241/42 , C07D307/81 , C07D317/54 , C07D471/02 , A01N33/24 , A01N43/08 , A01N43/30 , A01N43/40 , A01N43/58 , A01N43/60
CPC分类号： C07D213/64 , C07C251/48 , C07C2602/10 , C07D213/48 , C07D213/74 , C07D215/227 , C07D241/42 , C07D241/44 , C07D307/79 , C07D317/58
摘要： The present invention relates to compounds of Formula (I) which may be useful in the treatment of diseases, such as, metabolic disorders, dyslipidemia and/or hypercholesteremia: (I).
摘要翻译：本发明涉及式（I）化合物，其可用于治疗疾病如代谢紊乱，血脂异常和/或高氯全身风险：

67. 发明公开

EP1417168A2 2-(HYDROXYPHENYL) -2-(ALKOXYIMINO) -N-METH YLACETAMID-DERIVATE UND DEREN HERSTELLUNGSVERFAHREN 审中-公开
标题翻译： 2-（羟基苯基）-2-（烷氧基亚氨基）-N-甲基乙酰胺衍生物和其制造过程
公开(公告)号：EP1417168A2
公开(公告)日：2004-05-12
申请号：EP02758383.0
申请日：2002-07-24
申请人： Bayer CropScience AG
发明人： WEINTRITT, Holger , LANTZSCH, Reinhard , MÜH, Thorsten
IPC分类号： C07C249/08 , C07C251/48 , C07C249/04
CPC分类号： C07C249/04 , C07C251/48
摘要： The invention relates to a novel method for producing 2-(hydroxyphenyl)-2-(alkoxyimino)-N-methylacetamide derivatives.

68. 发明公开

EP1301468A1 PROCESS FOR THE PRODUCTION OF CYCLOHEXANONE OXIME 有权
标题翻译：生产环己酮肟的方法
公开(公告)号：EP1301468A1
公开(公告)日：2003-04-16
申请号：EP01938832.1
申请日：2001-05-31
申请人： DSM N.V.
发明人： BLAAUW, Marc , SIMONS, Antonius, Jacobus, Franciscus , RIESTHUIS, Theodorus, Friederich, Maria , PIT, Alex , OEVERING, Henk
IPC分类号： C07C249/08
CPC分类号： C07C249/08 , C01B21/1418 , C07C2601/14 , C07C251/44
摘要： Process for the production of cyclohexanone oxime in which a phosphate-containing aqueous reaction medium is cycled from a hydroxylammonium synthesis zone to a cyclohexanone oxime synthesis zone and back to the hydroxylammonium synthesis zone, in which hydroxylammonium synthesis zone hydroxylammonium is fomed by catalytic reduction of nitrate with hydrogen, and in which cyclohexanone oxime synthesis zone hydroxylammonium is reacted with cyclohexanone to form cyclohexanone oxime, wherein the phosphate concentration in the acqueous reaction medium entering the cyclohexanone oxime synthesis zone is higher than 3.0 mol/l.
摘要翻译：生产环己酮肟的方法，其中将含磷酸盐的含水反应介质从羟基铵合成区循环到环己酮肟合成区并返回到羟铵合成区，其中羟铵合成区羟铵通过催化还原硝酸盐而形成其中环己酮肟合成区羟胺与环己酮反应形成环己酮肟，其中进入环己酮肟合成区的水性反应介质中的磷酸盐浓度高于3.0mol / l。

69. 发明公开

EP1296939A1 VERFAHREN ZUR HERSTELLUNG VON TRIOXIMDERIVATEN 有权
公开(公告)号：EP1296939A1
公开(公告)日：2003-04-02
申请号：EP01947442.8
申请日：2001-07-04
申请人： BASF AKTIENGESELLSCHAFT
发明人： KRAMER, Andreas , KIEFER, Matthias , HENNINGSEN, Michael , SIEGEL, Wolfgang , SCHRÖDER, Jochen
IPC分类号： C07C249/08 , C07C251/60 , C07C49/12
CPC分类号： C07C249/06 , C07C249/08 , C07C251/40
摘要： The invention relates to a method for the production of trioxime derivatives of formula (I): where R?1 and R2¿ = independently, cyano, alkyl, haloalkyl or cycloalkyl and R?3 and R4¿ = independently, alkyl, haloalkyl, cycloalkyl, alkylcarbonyl or arylalkyl. Said method comprises the following reaction steps, without isolation of the intermediate products: A) nitrosation of 1,3 diketones of formula (II), to give monooximes of formula (III): B) oximation of (III) with hydroxylamine derivatives of formula (IV): H¿2N-OR?3', where R3' = H or R3 to give bisoximes of formula (V): C) alkylation of (V) with alkylating agents, or acylation of (V) with acylating agents to give compounds of formula (VI) and D) finally, oximation of (VI) with hydroxylamine to give compounds of formula (I).
摘要翻译：本发明涉及制备式（I）三肟衍生物的方法：其中R 1和R 2独立地为氰基，烷基，卤代烷基或环烷基，R 3和R 4独立地为烷基，卤代烷基，环烷基，烷基羰基或芳基烷基。所述方法包括以下反应步骤，不分离中间产物：A）式（II）的1,3-二酮的亚硝化，得到式（III）的单肟：B）用式（III）的羟胺衍生物（V）的烷基化（C）：用烷基化剂将（V）烷基化或用酰化剂将（V）酰化成（IV）：其中R3'= H或R3以生成式（V）的双肟：最后给出式（VI）化合物和D），用羟胺肟化（VI）得到式（I）化合物。

70. 发明授权

EP0885878B1 Verfahren zur Herstellung von O-substituierten Hydroxylammoniumsalzen 失效
标题翻译：一种用于制备O-取代的羟铵盐过程
公开(公告)号：EP0885878B1
公开(公告)日：2003-03-12
申请号：EP98115428.9
申请日：1995-10-16
申请人： BASF AKTIENGESELLSCHAFT
发明人： Keil, Michael Dr. , Wahl, Josef , Klein, Ulrich, Dr. , Will, Wolfgang Dr.
IPC分类号： C07C249/08
CPC分类号： C07C249/12 , C07C239/20 , C07C249/08 , Y02P20/125 , C07C251/38

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