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1. 发明授权

US06743303B2 Process for treating adhesion promoted metal surfaces with an organo-silcon post-treatment 失效
标题翻译：用于处理粘合的方法利用有机硅氧烷后处理促进金属表面
公开(公告)号：US06743303B2
公开(公告)日：2004-06-01
申请号：US10003625
申请日：2001-11-02
申请人： Joseph R. Montano , John P. Cahalen
发明人： Joseph R. Montano , John P. Cahalen
IPC分类号： C23C2282
CPC分类号： C09D4/00 , C23C22/08 , C23C22/68 , C23C22/83 , C23C2222/20 , H05K3/383 , H05K3/389 , C08G77/00
摘要： A method for treating a micro-roughened metal surface to improve bonding between the metal surface and a polymer material. The method involves post-treating the micro-roughened conversion coated metal surface with an aqueous organo-silicon wetting composition after having formed the micro-roughened conversion coated metal surface with an adhesion promotion composition. Suitable organo-silicons include organosilanes, organosiloxanes, organosilizanes and the like. The method can be employed in the circuit board industry to improve bonding between layers in multilayer circuit boards.
摘要翻译：一种用于处理微粗化金属表面以改善金属表面和聚合物材料之间的结合的方法。该方法包括在用粘合促进组合物形成微粗糙化转化涂覆的金属表面后，用含水有机硅润湿组合物对微粗糙化转化涂覆的金属表面进行后处理。合适的有机硅包括有机硅烷，有机硅氧烷，有机硅烷等。该方法可用于电路板工业中以改善多层电路板中的层之间的结合。

2. 发明授权

US06503343B1 Controlled plating on reactive metals 有权
标题翻译：对活性金属的控制电镀
公开(公告)号：US06503343B1
公开(公告)日：2003-01-07
申请号：US09658643
申请日：2000-09-11
申请人： D. Morgan Tench , Leslie F. Warren, Jr. , John T. White
发明人： D. Morgan Tench , Leslie F. Warren, Jr. , John T. White
IPC分类号： C23C2282
CPC分类号： H01L21/288 , C23C18/1651 , C23C18/1653 , C23C18/32 , C23C18/42 , C23C18/54 , H01L24/11 , H01L2224/13099 , H01L2224/45144 , H01L2924/01004 , H01L2924/01005 , H01L2924/01006 , H01L2924/01012 , H01L2924/01013 , H01L2924/01015 , H01L2924/01016 , H01L2924/01022 , H01L2924/01027 , H01L2924/01029 , H01L2924/0103 , H01L2924/01033 , H01L2924/01039 , H01L2924/01044 , H01L2924/01045 , H01L2924/01046 , H01L2924/01072 , H01L2924/01073 , H01L2924/01074 , H01L2924/01075 , H01L2924/01076 , H01L2924/01077 , H01L2924/01078 , H01L2924/01079 , H01L2924/014 , H01L2924/04953 , H01L2924/10253 , H01L2924/14 , H01L2924/30107 , H01L2924/00
摘要： A direct displacement plating process provides a uniform, adherent coating of a relatively stable metal (e.g., nickel) on a highly reactive metal (e.g., aluminum) that is normally covered with a recalcitrant oxide layer. The displacement reaction proceeds, preferably in a nonaqueous solvent, as the oxide layer is dissolved by a fluoride activator. Halide anions are used to provide high solubility, to serve as an anhydrous source of stable metal ions, and to control the rate of the displacement reaction. A low concentration of activator species and little or no solution agitation are used to cause depletion of the activator species within pores in the surface oxide so that attack of the reactive metal substrate is minimized. Used in conjunction with electroless nickel deposition to thicken the displacement coating, this process can be used to render aluminum pads on IC chips solderable without the need for expensive masks and vacuum deposition operations. Such coatings can also be used to preserve or restore wire bondability, or for corrosion protection of aluminum and other reactive structural metals and alloys. A thin layer of immersion gold can be used to protect the thickened coating from oxidation. The solderable aluminum IC chip pads provide the basis for a maskless bumping process for flip chip attachment.
摘要翻译：直接移位电镀方法提供了在通常被顽固氧化物层覆盖的高反应性金属（例如铝）上的相对稳定的金属（例如镍）的均匀涂层。随着氧化物层被氟化物活化剂溶解，置换反应优选在非水溶剂中进行。卤化阴离子用于提供高溶解度，用作稳定金属离子的无水源，并控制置换反应的速率。使用低浓度的活化剂物质和很少或不用溶液搅拌来引起表面氧化物中的孔隙内的活化剂物质的耗尽，从而使反应性金属底物的侵蚀最小化。与无电镍沉积结合使用以增加位移涂层，该工艺可用于使IC芯片上的铝焊盘可焊接，而无需昂贵的掩模和真空沉积操作。这种涂层也可用于保护或恢复线焊接性，或用于铝及其他反应性结构金属和合金的腐蚀保护。浸金的薄层可用于保护增厚涂层免受氧化。可焊接铝IC芯片焊盘为倒装芯片安装的无掩模凸块工艺提供了基础。

3. 发明授权

US06475301B1 Conversion coatings on aluminum from KF solutions 有权
标题翻译：来自KF溶液的铝上的转化涂层
公开(公告)号：US06475301B1
公开(公告)日：2002-11-05
申请号：US09565749
申请日：2000-05-08
申请人： Gerald Adam Grab , Kimberly A. Lazarz , Matthew John Zaluzec , Timothy Van Evans
发明人： Gerald Adam Grab , Kimberly A. Lazarz , Matthew John Zaluzec , Timothy Van Evans
IPC分类号： C23C2282
CPC分类号： B23K35/3605 , C23C22/68
摘要： The invention is a method of forming a conversion coating on an aluminum surface. According to the method, the aluminum surface is conversion coated by first treating the surface with thermal degreasing or aqueous alkaline degreasing and then contacting the treated surface with an aqueous bath solution of KF. The concentration of KF in the solution is 2.0-25.0 wt. % and the temperature is 90-212° F. for at least 5 seconds. The conversion coating consists essentially of: (a) substantially all K3AlF6 or (b) a mixture comprising a major proportion of K3AlF6 and a minor proportion of KAlF4
摘要翻译：本发明是在铝表面上形成转化涂层的方法。根据该方法，通过首先用热脱脂或碱性脱脂水处理表面，然后使处理过的表面与KF的水浴溶液接触，将铝表面转化成涂层。溶液中KF的浓度为2.0-25.0wt。％，温度为90-212°F至少5秒钟。转化涂层基本上由以下组成：（a）基本上所有的K 3 AlF 6或（b）包含主要比例的K 3 AlF 6和少量KAlF 4的混合物

4. 发明授权

US06406562B1 Method of increasing corrosion resistance of metals and alloys by treatment with rare earth elements 失效
标题翻译：通过稀土元素处理提高金属和合金的耐腐蚀性的方法
公开(公告)号：US06406562B1
公开(公告)日：2002-06-18
申请号：US09572699
申请日：2000-05-16
申请人： Yucheng Lu , Michael Brian Ives
发明人： Yucheng Lu , Michael Brian Ives
IPC分类号： C23C2282
CPC分类号： C23C22/56 , C23C22/48 , C23C22/50 , C23C22/52 , C23C22/68
摘要： There is provided a method for treating the surface of metals such as nickel based or high alloy steels, austenitic and ferritic stainless steels, copper and aluminum alloys to increase their corrosion resistance by modification of the metal surfaces to inhibit cathodic corrosion processes. In a single step treatment process the metals are immersed into a heated aqueous composition containing a rare earth salt substantially free of any halide compound. Increased corrosion resistance is obtained using nitrates of yttrium, gadolinium, cerium, europium, terbium, samarium, neodymium, praseodymium, lanthanum, holmium, ytterbium, dysprosium, and erbium nitrates. The rare earth salt is present in the range from about 2% by weight to saturation of the solution. The composition includes a pH-modifying substance such as nitric acid to adjust the pH in the range 0.5 to about 6.5 to attack the surface to remove oxides facilitating deposition of the rare earth.
摘要翻译：提供了一种用于处理镍基或高合金钢，奥氏体和铁素体不锈钢，铜和铝合金等金属表面的方法，通过改变金属表面以抑制阴极腐蚀过程来提高其耐腐蚀性。在单步处理工艺中，将金属浸入含有基本上不含任何卤化物的稀土盐的加热含水组合物中。使用钇，钆，铈，铕，铽，钐，钕，镨，镧，钬，镱，镝和硝酸铒的硝酸盐可以获得提高的耐腐蚀性。稀土盐以约2重量％至溶液饱和的范围存在。组合物包括pH调节物质如硝酸，以将pH调节在0.5至约6.5的范围内以侵蚀表面以除去促进稀土沉积的氧化物。

5. 发明授权

US06231687B1 Lubrication treatment method for cold working of steel 失效
标题翻译：钢的冷加工润滑处理方法
公开(公告)号：US06231687B1
公开(公告)日：2001-05-15
申请号：US09413931
申请日：1999-10-07
申请人： Naoyuki Kobayashi , Masahiko Kawakami
发明人： Naoyuki Kobayashi , Masahiko Kawakami
IPC分类号： C23C2282
CPC分类号： B21J3/00 , C23C22/12 , C23C22/22 , C23C22/367 , C23C22/83
摘要： A phosphating solution that contains from 3 to 30 g/l of zinc ions, from 0.1 to 20 g/l of ferrous ions, from 5 to 60 g/l of phosphate ions, from 5 to 60 g/l of nitrate ions, and a source of hydroxylamine in a concentration corresponding stoichiometrically to from 0.5 to 4 g/l of hydroxylamine and in which there is a weight ratio of zinc to phosphate that is from 0.1:1 to 1:1 deposits on steel to be cold worked a phosphate conversion coating suitable as a lubricant carrier. This phosphating solution, which may optionally contain one or more of calcium, nickel, cobalt, and copper cations and simple and complex fluorine-containing anions, makes it possible to lower the temperature of the treatment solution, reduce the amount of sludge, improve the quality of the coating film, and allow single-liquid type replenishment to be used. Preferably the surface to be phosphated is immersed in the phosphating solution, maintained at a temperature of 35 to 80° C., for 2 to 20 minutes.
摘要翻译：含有3〜30g / l的锌离子，0.1〜20g / l的亚铁离子，5〜60g / l的磷酸盐离子，5〜60g / l的硝酸根离子的磷化液，以及羟胺浓度相当于0.5至4g / l羟胺的化学计量浓度，其中锌与磷酸盐的重量比为0.1：1至1：转化涂层适合作为润滑剂载体。该磷酸盐溶液可以任选地含有一种或多种钙，镍，钴和铜阳离子和简单和复杂的含氟阴离子，使得可以降低处理溶液的温度，减少污泥的量，改善涂膜的质量，并允许使用单液体补充。优选将要磷化的表面浸入磷酸盐溶液中，保持在35至80℃的温度下2至20分钟。

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