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1. 发明专利

JPS5019529B1 失效
公开(公告)号：JPS5019529B1
公开(公告)日：1975-07-08
申请号：JP3155066
申请日：1966-05-19
IPC分类号： C08K5/00 , C07C67/00 , C07C407/00 , C07C409/20 , C07C409/22 , C08F4/00 , C08F4/28 , C08J3/20 , C08K5/14 , C10L1/18 , C07C179/00

2. 发明专利

JPS6187659A Aqueous suspension containing organic peroxide 失效
标题翻译：含有机有机过氧化物的水性悬浮液
公开(公告)号：JPS6187659A
公开(公告)日：1986-05-06
申请号：JP20992084
申请日：1984-10-08
申请人： Kayaku Nuurii Kk
发明人： YANAKA TAKUMI , TAKEMOTO HIDEKI , HIRAI YASUO
IPC分类号： C07C407/00 , C07C67/00 , C07C409/00 , C07C178/00 , C07C179/00
摘要： PURPOSE: To obtain an aqueous suspension containing an organic peroxide, useful as a polymerization initiator of polystyrene, etc., and transport able with a pump without causing clogging, by using tribasic calcium phosphate as an active component.
CONSTITUTION: An aqueous suspension containing an organic peroxide is prepared by compounding tribasic calcium phosphate. The liquid can be prepared e.g. by adding a necessary amount of tribasic calcium phosphate to a definite amount of water, dispersing under stirring, optionally adding and dispersing a dispersion stabilizing assistant in the dispersion, adding a required amount of powder (benzoyl peroxide) moistened with water, and stirring the mixture. Even if a partial phase-separation takes place in the above suspension, the suspension can be homogenized easily by the light shaking or stirring, to enable the approach to the practical adoption of the automatic charging system with a pump. In the conventional process, the charge of the peroxide has to be carried out through a manhole and accordingly the operation of a polymerization plant in closed system has been impossible. The present process clears the way for the operation of the plant in closed system.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过使用磷酸三钙作为活性成分，得到含有有机过氧化物的水性悬浮液，其可用作聚苯乙烯等的聚合引发剂，并可通过泵输送而不引起堵塞。构成：含有有机过氧化物的含水悬浮液通过配合磷酸三钙制备。液体可以例如制备。通过向一定量的水中加入必要量的磷酸三钙，在搅拌下分散，任选地在分散体中加入和分散分散体稳定助剂，加入所需量的用水润湿的粉末（过氧化苯甲酰），并搅拌混合物。即使在上述悬浮液中发生部分相分离，也可以通过轻摇或搅拌容易地使悬浮液均质化，从而能够实现采用泵的自动计费系统。在常规方法中，过氧化物的电荷必须通过人孔进行，因此聚合装置在封闭系统中的操作是不可能的。本程序清除了封闭系统中工厂运行的方式。

3. 发明专利

JPS5028939B1 失效
公开(公告)号：JPS5028939B1
公开(公告)日：1975-09-19
申请号：JP12732370
申请日：1970-12-28
IPC分类号： C07B61/00 , B01J21/00 , B01J23/64 , B01J23/74 , C07C67/00 , C07C407/00 , C07C409/38 , C07C179/00 , C07C179/10

4. 发明授权

US4314949A Process for making peroxycarboxylic acids 失效
标题翻译：制备过氧羧酸的方法
公开(公告)号：US4314949A
公开(公告)日：1982-02-09
申请号：US171564
申请日：1980-07-23
申请人： Griscom Bettle, III , Howard Mills , Edward B. Richter
发明人： Griscom Bettle, III , Howard Mills , Edward B. Richter
IPC分类号： C07C409/24 , C11D3/39 , C07C179/00
CPC分类号： C11D3/3945 , C07C407/00 , C07C409/24
摘要： An improved process, preferably continuous, for making a peroxyacid having about 6 to 18, preferably about 8 to 16 carbon atoms and at least one peroxyacid moiety, using as starting materials the corresponding carboxylic acid and hydrogen peroxide and using concentrated acid as the reaction medium, comprising the steps of (a) maintaining a reaction mixture having a liquid component comprising 60 to 80% concentrated acid, 2.5 to 12.5% hydrogen peroxide, and 7.5 to 37.5 % water and a dispersed solid component comprising crystals of the carboxylic acid starting material and peroxyacid product, the ratio of liquid to solids being from about 15:1 to about 49:1. Preferably the carboxylic acid is added as particles having a size of less than #100 mesh to a preformed solution of the concentrated acid and peroxide.
摘要翻译：用于制备具有约6至18个，优选约8至16个碳原子的过氧酸和至少一个过氧酸部分的改进方法，优选连续使用，使用相应的羧酸和过氧化氢作为原料，并使用浓酸作为反应介质包括以下步骤：（a）保持具有包含60至80％浓酸，2.5至12.5％过氧化氢和7.5至37.5％水的液体组分的反应混合物和包含羧酸起始物质晶体的分散固体组分和过氧酸产物，液体与固体的比例为约15:1至约49:1。优选地，将羧酸作为具有小于＃100目的尺寸的颗粒加入到预先形成的浓酸和过氧化物溶液中。

5. 发明授权

US4034047A Process for catalytic oxidation of olefins to form hydroperoxides 失效
标题翻译：催化氧化烯烃以形成氢过氧化物的方法
公开(公告)号：US4034047A
公开(公告)日：1977-07-05
申请号：US656055
申请日：1976-02-17
申请人： Howard P. Angstadt
发明人： Howard P. Angstadt
IPC分类号： C07C29/50 , C07C45/33 , C07C45/34 , C07C409/04 , C07C409/10 , C07C409/14 , C07C29/00 , C07C179/00
CPC分类号： C07C409/14 , B01J23/70 , C07C29/50 , C07C407/00 , C07C409/04 , C07C409/10 , C07C45/53 , B01J23/10 , B01J23/72 , B01J23/75 , B01J23/755 , B01J31/06 , C07C2101/14 , C07C2101/16 , C07C2101/18 , C07C2102/42
摘要： Polymeric complexes formed between a thermally-condensed polyacrylonitrile polymer and transition metal salts, including rare earth metals, have been found to be effective catalysts for the oxidation of compounds containing activated carbon-hydrogen bonds such as olefins, or secondary and tertiary alkylaromatics, to form valuable oxidation products, particularly hydroperoxides or their decomposition products.
摘要翻译：已经发现在热凝聚聚丙烯腈聚合物和过渡金属盐（包括稀土金属）之间形成的聚合物络合物是用于氧化含有活性碳 - 氢键的化合物如烯烃或二级和三级烷基芳烃的有效催化剂，以形成有价值的氧化产物，特别是氢过氧化物或其分解产物。

6. 发明公开

EP0103099A3 Beta-hydroxycyclopentylperoxide compounds and the use thereof 失效
标题翻译： β-羟基环戊二烯氧化物化合物及其用途
公开(公告)号：EP0103099A3
公开(公告)日：1985-04-03
申请号：EP83106794
申请日：1983-07-11
申请人： NIPPON OIL CO. LTD.
发明人： Yuasa, Hitoshi , Matsuno, Mitsuo , Imai, Hirosuke
IPC分类号： C07C179/00 , C07C179/053 , C07C47/12 , C07C45/53 , C07C45/51 , C07C45/59 , C07C45/60 , C07C43/303 , C07C41/50
CPC分类号： C07D317/26 , C07C29/132 , C07C41/50 , C07C45/515 , C07C45/517 , C07C45/53 , C07C45/54 , C07C45/59 , C07C45/60 , C07C409/14 , C07C409/18 , C07C2601/08 , C07D309/10 , Y02P20/582 , C07C47/12 , C07C47/198 , C07C43/315 , C07C43/303 , C07C31/12
摘要： Novel peroxide compounds and the use thereof. In particular, the present invention concerns β-hydroxycyclopentylperoxide compounds of the general formula:
wherein R, represents hydrogen or an organic residue of 1 to 9 carbon atoms. These novel peroxide compounds are useful as an intermediate in the production of glutaraldehydes.
摘要翻译：新型过氧化物化合物及其用途。特别地，本发明涉及以下通式的β-羟基环戊基过氧化物化合物：其中R 1表示氢或1至9个碳原子的有机残基。这些新型过氧化物化合物可用作戊二醛生产中的中间体。

7. 发明公开

EP0002746A1 Perverbindungen und optische Aufheller enthaltendes Bleichmittel und dessen Verwendung als Textilbehandlungsmittel 失效
标题翻译： Perverbindungen und optische Aufheller enthaltendes Bleichmittel und dessen Verwendung als Textilbehandlungsmittel。
公开(公告)号：EP0002746A1
公开(公告)日：1979-07-11
申请号：EP78101708.2
申请日：1978-12-15
申请人： Henkel Kommanditgesellschaft auf Aktien
发明人： Bloching, Helmut, Dr.
IPC分类号： C11D3/42 , C07C179/00 , C11D3/395 , D06L3/06 , D06L3/12
CPC分类号： C11D3/3945 , C11D3/42
摘要： Als Bleichmittel für Textilien eignet sich ein lagerbeständiges Gemisch aus einer bleichend wirkenden Diperoxydicarbonsäure mit 6 bis 12 C-Atomen und einem als optischen Aufheller wirkenden wasserlöslichen Salz des 4,4'-Bis-(3-sulfo-4-chlorstyryl)-diphenyls, wobei auf 1 Gewichtsteil verfügbaren Persauerstoffs 0,01 bis 0,5 Gewichtsteile des optischen Aufhellers entfallen. Das Gemisch wird bei der Textilwäsche anstelle von Chlorbleichlauge verwendet.
摘要翻译：用于纺织品的合适的漂白剂是具有6-12个碳原子的漂白二过氧二羧酸和4,4'-双（3-磺基-4-氯苯乙烯基）二苯基的水溶性盐的储存稳定的混合物，其作为荧光增白剂，每1重量份可用的过氧化物存在0.01至0.5重量份的荧光增白剂。在洗涤中使用混合物代替氯漂白溶液。

8. 发明授权

US4790952A Alkyl monoperoxysuccinic acid precursors and method of synthesis 失效
公开(公告)号：US4790952A
公开(公告)日：1988-12-13
申请号：US897152
申请日：1986-08-14
申请人： Dale S. Steichen , Hao Ku , Sheldon N. Lewis
发明人： Dale S. Steichen , Hao Ku , Sheldon N. Lewis
IPC分类号： C07D233/80 , C11D3/39 , D06L3/02 , C07C178/00 , C07C179/00
CPC分类号： C11D3/3907 , C07D233/80
摘要： A number of novel peracid precursors each have the general structure: ##STR1## wherein: Z is a leaving group, the conjugate acid of the leaving group being in the range of from about 4 to 15; R is a substituted or unsubstituted alkyl or alkenyl group having from about 1 to 18 carbon atoms; and M is hydrogen or an alkali or alkaline earth metal. A method is also disclosed for synthesizing a product as represented above wherein succinic anhydride, including an R constituent as defined above is dissolved in a water-miscible, non-nucleophilic solvent and an acid including a Z constituent as defined above is neutralized and deprotonated to form a nucleophile, the substituted anhydride and the nucleophile being combined to form the product. The product is a component in a dry bleach product, optionally including other adjuncts.

9. 发明授权

US4376218A Organic peroxide compositions 失效
标题翻译：有机过氧化物组合物
公开(公告)号：US4376218A
公开(公告)日：1983-03-08
申请号：US254164
申请日：1981-04-14
申请人： Keith J. Izzard , Reginald W. Stephenson , Keith C. P. Stanistreet , Iain R. Keeling
发明人： Keith J. Izzard , Reginald W. Stephenson , Keith C. P. Stanistreet , Iain R. Keeling
IPC分类号： C07C409/00 , C08F4/32 , C08F4/34 , C07C179/00
CPC分类号： C08F4/32
摘要： A solid organic peroxide composition comprises from 50% to below 70% by weight of a solid organic peroxide, such as benzoyl peroxide, at least 10% preferably at least 15% of a liquid desensitizer such as a liquid ester of phthalic acid, benzoic acid or phosphoric acid, a silicone oil or a liquid chlorinated hydrocarbon and a solid organophilic compound such as a solid ester of phthalic acid, benzoic acid or phosphoric acid a solid chlorinated hydrocarbon or a salt of a higher fatty acid in, preferably, less than 20% by weight. The compositions are particularly insensitive to impact.
摘要翻译：固体有机过氧化物组合物包含50重量％至低于70重量％的固体有机过氧化物，例如过氧化苯甲酰，至少10重量％，优选至少15％的液体脱敏剂，例如邻苯二甲酸的液体酯，苯甲酸或磷酸，硅油或液体氯化烃和固体亲有机化合物如苯二甲酸，苯甲酸或磷酸的固体酯，固体氯化烃或高级脂肪酸的盐，优选小于20 重量％。组合物对冲击特别不敏感。

10. 发明授权

US3928465A Organic peroxides, their preparation, and their applications 失效
标题翻译：有机过氧化物，它们的制备及其应用
公开(公告)号：US3928465A
公开(公告)日：1975-12-23
申请号：US37393473
申请日：1973-06-27
申请人： GOODRICH CO B F
发明人： SACRINI EGEO , CAVALLOTTI CLAUDIO
IPC分类号： C07C409/22 , C08F4/36 , C08K5/14 , C07C179/00
CPC分类号： C07C409/22 , C08F4/36 , C08K5/14
摘要： Tetraperoxides of the formula

where X is a bivalent radical such as alkylene; R1 is hydrogen or an organic radical; R2 is alkylene alkoxy carbonyl; and R3 is an organic radical. Method of preparing tetraperoxides by addition reaction between a bis-hydroperoxide and a carbonyl compound to form a dihydroxy diperoxide, followed by condensation of the dihydroxy diperoxide with a tertiary monohydroxide. The tetraperoxides are useful for vulcanizing saturated elastomers, crosslinking plastomers, and initiating radical polymerization.
摘要翻译：式R1R1 || R 3- OO-C-OO-X-O-C-R3 | | R2R2的四环氧化物，其中X是二价基团如亚烷基; R1是氢或有机基团; R2是亚烷基烷氧基羰基; 并且R 3是有机基团。通过双氢过氧化物和羰基化合物之间的加成反应制备四
氧化物以形成二羟基二过氧化物，然后二羟基二过氧化物与叔氢氧化物的缩合制备方法。四元素可用于硫化饱和弹性体，交联塑性体和引发自由基聚合。

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