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1. 发明申请

US20050027088A1 Production process for vinyl chloride polymer 有权
标题翻译：氯乙烯聚合物的生产工艺
公开(公告)号：US20050027088A1
公开(公告)日：2005-02-03
申请号：US10834978
申请日：2004-04-30
申请人： Yoshinori Nakahara , Masatsugu Takano , Yasuhiro Takahashi , Tadashi Amano
发明人： Yoshinori Nakahara , Masatsugu Takano , Yasuhiro Takahashi , Tadashi Amano
IPC分类号： C08F2/00 , C08F14/06
CPC分类号： C08F14/06 , C08F2/16
摘要： A production process for a vinyl chloride polymer is proposed in which either vinyl chloride, or a monomer mixture comprising vinyl chloride, is polymerized in an aqueous medium inside a polymerization vessel, while heat removal is conducted using a reflux condenser. In this process, the liquid level of the contents inside the polymerization vessel is monitored using an electric wave liquid level gauge, which is disposed on the polymerization vessel and radiates microwaves with a frequency of 4 to 20 GHz. The operating efficiency of the reflux condenser can be improved, and the quantity of heat removed by the reflux condenser can be increased. Furthermore, the time required to complete the process, including the raw material addition step and/or the washing step conducted following completion of the polymerization, can be shortened.
摘要翻译：提出了氯乙烯聚合物的制备方法，其中氯乙烯或包含氯乙烯的单体混合物在聚合容器内部的水性介质中聚合，同时使用回流冷凝器进行除热。在该过程中，使用设置在聚合容器上的电波液位计并辐射频率为4至20GHz的微波来监测聚合容器内部的内容物的液面。可以提高回流冷凝器的运行效率，并且可以提高由回流冷凝器除去的热量。此外，可以缩短完成该方法所需的时间，包括在聚合完成后进行的原料添加步骤和/或洗涤步骤。

2. 发明授权

US06977288B2 Production process for vinyl chloride polymer 有权
公开(公告)号：US06977288B2
公开(公告)日：2005-12-20
申请号：US10834978
申请日：2004-04-30
申请人： Yoshinori Nakahara , Masatsugu Takano , Yasuhiro Takahashi , Tadashi Amano
发明人： Yoshinori Nakahara , Masatsugu Takano , Yasuhiro Takahashi , Tadashi Amano
IPC分类号： C08F2/00 , C08F14/06
CPC分类号： C08F14/06 , C08F2/16
摘要： A production process for a vinyl chloride polymer is proposed in which either vinyl chloride, or a monomer mixture comprising vinyl chloride, is polymerized in an aqueous medium inside a polymerization vessel, while heat removal is conducted using a reflux condenser. In this process, the liquid level of the contents inside the polymerization vessel is monitored using an electric wave liquid level gauge, which is disposed on the polymerization vessel and radiates microwaves with a frequency of 4 to 20 GHz. The operating efficiency of the reflux condenser can be improved, and the quantity of heat removed by the reflux condenser can be increased. Furthermore, the time required to complete the process, including the raw material addition step and/or the washing step conducted following completion of the polymerization, can be shortened.

3. 发明授权

US5763545A Polymerization apparatus and a method for producing polymer using the same 失效
标题翻译：聚合装置及使用其的聚合物的制造方法
公开(公告)号：US5763545A
公开(公告)日：1998-06-09
申请号：US527903
申请日：1995-09-14
申请人： Masatsugu Takano , Tadashi Amano , Yoshihiko Hirai , Yoshitaka Okuno
发明人： Masatsugu Takano , Tadashi Amano , Yoshihiko Hirai , Yoshitaka Okuno
IPC分类号： B01J19/00 , B01J19/18 , C08F2/38 , C08F14/06
CPC分类号： B01J19/0066 , B01J19/006 , B01J19/18 , C08F14/06 , B01J2219/00094 , B01J2219/00101 , B01J2219/00162 , B01J2219/00768 , B01J2219/00779 , B01J2219/185
摘要： A polymerization apparatus comprising a cylindrical polymerization vessel having a straight cylindrical section, a cooling means for cooling the contents of the polymerization vessel, and paddle impellers, each fixed to a central shaft positioned along the center line of the vessel and spaced apart at predetermined positions, each impeller having impeller blades for agitating the contents inside the polymerization vessel as the shaft is rotated, wherein the polymerization vessel has an inner capacity of 100 m.sup.3 or more and has a ratio L/D (the length L of the cylindrical section to the inner diameter D of the vessel) of at least 1.5, wherein three or more of the paddle impellers are arranged on and along said shaft in the center of the vessel, and wherein polymerization/inhibitor charge openings are arranged at positions on the interior surface of the wall of the polymerization vessel in such a manner that one charge opening is provided per paddle impeller at a position on the vessel wall which corresponds to the position of a paddle impeller along the shaft.
摘要翻译：一种聚合装置，包括具有直的圆柱形部分的圆柱形聚合容器，用于冷却聚合容器的内容物的冷却装置和桨式叶轮，每个固定在沿着容器的中心线定位的中心轴并且在预定位置间隔开每个叶轮具有用于在轴旋转时搅拌聚合容器内部的内容物的叶轮叶片，其中聚合容器的内容积为100m 3或更大，并且具有L / D比（圆筒部分与容器的内径D）至少为1.5，其中三个或更多个叶片叶轮布置在容器中心的轴上并且沿着轴的中心布置，并且其中聚合/抑制剂装料开口设置在容器的内表面上的位置聚合容器的壁以这样一种方式，即每个桨式叶轮在容器wa上的位置设置一个装料口其对应于桨式叶轮沿轴的位置。

4. 发明授权

US06448372B2 Process for producing vinyl chloride polymer with low residual monomer 失效
标题翻译：生产具有低残留单体的氯乙烯聚合物的方法
公开(公告)号：US06448372B2
公开(公告)日：2002-09-10
申请号：US09764093
申请日：2001-01-19
申请人： Takashi Kobayashi , Ryuichi Saito , Yoshinori Nakahara , Tadashi Amano , Ichiro Hara
发明人： Takashi Kobayashi , Ryuichi Saito , Yoshinori Nakahara , Tadashi Amano , Ichiro Hara
IPC分类号： C08F624
CPC分类号： C08F6/003 , C08F14/06 , C08L27/06 , C08F2/18
摘要： A process for producing a vinyl chloride polymer, including the steps of (a) subjecting a vinyl chloride monomer alone or a monomer mixture containing a vinyl chloride, to suspension polymerization in water; (b) subjecting the resultant vinyl chloride polymer slurry to stripping to remove an unreacted monomer remaining therein; and (c) dehydrating the polymer slurry having been subjected to stripping. In the polymerization step (a), the ratio of water/monomer is set in a weight ratio of from 0.80 to 1.50, and the viscosity at 20° C. of the polymer slurry to be fed to the stripping step is previously kept adjusted to 0.30 Pa·s or lower. In the stripping step (c), the residual unreacted monomer in the polymer slurry can efficiently be removed using steam in a smaller quantity, thus the vinyl chloride polymer can be produced at a high productivity.
摘要翻译：一种制备氯乙烯聚合物的方法，包括以下步骤：（a）使单独的氯乙烯单体或含有氯乙烯的单体混合物在水中悬浮聚合; （b）将得到的氯乙烯聚合物浆料进行汽提以除去其中残留的未反应单体; 和（c）使经过剥离的聚合物浆料脱水。在聚合步骤（a）中，将水/单体的比例设定为0.80至1.50的重量比，并将预先进料到汽提步骤的聚合物浆料的20℃下的粘度预先保持在 0.30 Pa.s以下。在汽提步骤（c）中，聚合物淤浆中残留的未反应单体可以用较少量的蒸汽有效地除去，从而可以高生产率生产氯乙烯聚合物。

5. 发明授权

US5610245A Polymerization method producing vinyl chloride polymer 失效
标题翻译：生产氯乙烯聚合物的聚合方法
公开(公告)号：US5610245A
公开(公告)日：1997-03-11
申请号：US364461
申请日：1994-12-27
申请人： Yasuhiro Takahashi , Tadashi Amano , Yoshihiro Shirota
发明人： Yasuhiro Takahashi , Tadashi Amano , Yoshihiro Shirota
IPC分类号： B01J19/00 , B01J19/18 , C08F2/18 , C08F14/06
CPC分类号： B01J19/18 , B01J19/0013 , C08F14/06 , B01J2219/00083 , B01J2219/185 , B01J2219/1943
摘要： A polymerization method used, particularly, in suspension polymerization of vinyl chloride, comprising a polymerization vessel (1) having a substantially cylindrical inner space, said inner space of said polymerization vessel being provided with a plurality of baffles (5) comprising vertically extending pipes, and a vertically continuously extending coil (6), and a refrigerant being passed through said baffles and said coil. High-cooling performance can be obtained, a high-speed reaction in a large-sized polymerization vessel becomes possible, and a stable polymerization reaction can be carried out. A high-quality and uniform polymer that has few fish eyes and has a high bulk specific gravity can be obtained.
摘要翻译：一种聚合方法，特别是在氯乙烯的悬浮聚合中使用的聚合方法，包括具有大致圆柱形内部空间的聚合容器（1），所述聚合容器的所述内部空间设置有多个挡板（5），包括垂直延伸的管道，和垂直连续延伸的线圈（6），并且制冷剂通过所述挡板和所述线圈。可以获得高冷却性能，可以在大型聚合容器中进行高速反应，并且可以进行稳定的聚合反应。可以获得鱼眼少且体积比重高的高质量且均匀的聚合物。

6. 发明授权

US5282680A Apparatus for continuous polymerization 失效
标题翻译：连续聚合装置
公开(公告)号：US5282680A
公开(公告)日：1994-02-01
申请号：US63604
申请日：1993-05-19
申请人： Tadashi Amano , Shuji Ohnishi , Minoru Shigemitsu , Yasuhiro Takahashi , Hajime Kitamura
发明人： Tadashi Amano , Shuji Ohnishi , Minoru Shigemitsu , Yasuhiro Takahashi , Hajime Kitamura
IPC分类号： B01F5/16 , B01J19/24 , B01F15/02
CPC分类号： B01F5/16 , B01J19/2415 , B01J19/243 , B01J2219/00094 , B01J2219/00162 , B01J2219/00164 , B01J2219/00182
摘要： An apparatus for continuous polymerization of vinyl chloride or a vinyl chloride-based monomeric mixture, comprising a pre-mixer 1 for preparing an aqueous suspension of the vinyl chloride or vinyl chloride-based monomeric mixture, and a polymer slurry tank 5 connected to the pre-mixer 1 through a polymerization passage comprising a piping 3, wherein a pump comprising a conical hub and an impeller mounted thereon comprised of a single spiral blade is used for drawing out the aqueous suspension from the pre-mixer into the polymerization passage and for discharging a polymer slurry formed in the passage into the slurry tank, and the polymerization passage has a length sufficient for permitting the vinyl chloride or vinyl chloride-based monomeric mixture contained in the aqueous suspension flowing through the passage to be polymerized to a predetermined extent while passing through the passage. The use of the pump having the structure as above ensures a marked suppression of polymer scale deposition in the pump, heat exchanger and pipings, and makes it possible to produce a resin with few fish-eyes. The apparatus is of extremely high industrial value for carrying out continuous polymerization.
摘要翻译：一种用于氯乙烯或氯乙烯基单体混合物的连续聚合的装置，包括用于制备氯乙烯或氯乙烯基单体混合物的水悬浮液的预混合器1和连接到前述聚合物浆料罐5的聚合物浆料罐5。混合器1通过包括管道3的聚合通道，其中包括圆锥形轮毂和安装在其上的叶轮由包括单个螺旋叶片的泵用于将预混合器中的水悬浮液抽出到聚合通道中并用于排出聚合物淤浆形成在通入浆料罐的通道中，并且聚合通道的长度足以允许流过通道的含水悬浮液中所含的氯乙烯或氯乙烯类单体混合物在通过时聚合至预定程度通过通道。具有上述结构的泵的使用确保了泵，热交换器和管道中的聚合物垢沉积的显着抑制，并且使得可以生产几乎没有鱼眼的树脂。该设备具有非常高的工业价值用于进行连续聚合。

7. 发明授权

US09463436B2 Method for manufacturing microparticulate anatase or rutile titanium oxide dispersion and component having photocatalytic thin film on surface 有权
标题翻译：微粒锐钛矿或金红石钛氧化物分散体的制造方法及表面具有光催化薄膜的成分
公开(公告)号：US09463436B2
公开(公告)日：2016-10-11
申请号：US14115209
申请日：2012-05-10
申请人： Manabu Furudate , Tomohiro Inoue , Shiro Takahashi , Yoshitsugu Eguchi , Tadashi Amano
发明人： Manabu Furudate , Tomohiro Inoue , Shiro Takahashi , Yoshitsugu Eguchi , Tadashi Amano
IPC分类号： B01J21/08 , B01J37/03 , B01J37/08 , B01J23/14 , B01J35/00 , C09D1/00 , C09D5/16 , B01J21/06 , C01G23/047 , C01G23/04 , C01G23/053 , B01J35/02 , C08K3/22
CPC分类号： B01J21/08 , B01J21/06 , B01J21/063 , B01J23/14 , B01J35/004 , B01J35/023 , B01J37/031 , B01J37/035 , B01J37/08 , C01G23/04 , C01G23/047 , C01G23/053 , C08K2003/2241 , C09D1/00 , C09D5/1618
摘要： A method for manufacturing a microparticulate anatase or rutile titanium oxide dispersion from a peroxotitanic acid solution optionally containing tin, wherein the method for manufacturing an anatase or rutile titanium oxide dispersion is characterized in that the peroxotitanic acid solution is fed continuously to a flow reactor and subjected to hydrothermal treatment at 150 to 250° C. and 0.5 to 10 MPa. The invention makes it possible to provide a method for manufacturing a microparticulate anatase or rutile titanium oxide dispersion having excellent stability in regard to the titanium oxide microparticles and enabling a high-transparency photocatalytic thin film to be produced, and to provide a member having a photocatalytic thin film formed on the surface using this dispersion.
摘要翻译：一种由任选含有锡的过氧钛酸溶液制备微粒锐钛矿或金红石型二氧化钛分散体的方法，其中所述锐钛型或金红石型氧化钛分散体的制造方法的特征在于，将过氧钛酸溶液连续供给流动反应器，在150〜250℃，0.5〜10MPa下进行水热处理。本发明使得可以提供一种在氧化钛微粒上具有优异的稳定性的微粒锐钛矿或金红石型氧化钛分散体的制造方法，能够制造高透光性的光催化薄膜，提供具有光催化剂使用该分散体在表面上形成薄膜。

8. 发明申请

US20140127514A1 INORGANIC HYDROPHILIC COATING SOLUTION, HYDROPHILIC COATING FILM OBTAINED THEREFROM, AND MEMBER USING SAME 审中-公开
标题翻译：无机水解涂料溶液，由其获得的水性涂料膜，以及使用其的成员
公开(公告)号：US20140127514A1
公开(公告)日：2014-05-08
申请号：US14116665
申请日：2012-05-31
申请人： Tomohiro Inoue , Manabu Furudate , Yoshitsugu Eguchi , Tadashi Amano
发明人： Tomohiro Inoue , Manabu Furudate , Yoshitsugu Eguchi , Tadashi Amano
IPC分类号： C09D1/00
CPC分类号： C09D1/00 , B01J21/063 , B01J21/08 , B01J35/002 , B01J35/004 , B01J37/0219 , B01J37/033 , C09D5/1662 , C09D7/61 , C09D7/67 , C09D183/02 , H01L31/048 , H02S40/10 , Y02E10/50 , Y10T428/31507 , Y10T428/31667
摘要： An inorganic hydrophilic coating solution including (a) an aqueous solution containing an amorphous silicate compound obtained by hydrolyzing and condensing a tetrafunctional silicon compound having a purity of 99.0 mass % or greater in an aqueous medium in the presence of a basic compound at a temperature within a range from normal temperature to 170° C., (b) water, and optionally, (c) not more than 30 mass % of an alcohol, a ketone, or a surfactant, where the concentration of the solid fraction derived from the aqueous solution containing the amorphous silicate compound is 0.01 to 2.0 mass % and the pH is 5 to 8; an inorganic hydrophilic coating film formed from a dried and cured product of the inorganic hydrophilic coating solution; a member having a substrate and the inorganic hydrophilic coating film formed on the surface of the substrate; and a cover panel for a solar cell module including the member.
摘要翻译：一种无机亲水性涂料溶液，其包括（a）含有无定形硅酸盐化合物的水溶液，所述无定形硅酸盐化合物通过在碱性化合物的存在下，在碱性化合物的存在下，在碱性化合物的存在下水解和缩合纯度为99.0质量％以上的四官能硅化合物，（b）水，和（c）不大于30质量％的醇，酮或表面活性剂，其中固体成分的浓度来源于水溶液含有无定形硅酸盐化合物的溶液为0.01〜2.0质量％，pH为5〜8; 由无机亲水性涂布液的干燥固化物形成的无机亲水性涂膜; 具有基材和在所述基材的表面上形成的无机亲水性涂膜的部件; 以及包括该构件的太阳能电池模块用盖板。

9. 发明申请

US20110294941A1 VINYL CHLORIDE-BASED RESIN COMPOSITION, METHOD OF PRODUCING VINYL CHLORIDE-BASED POLYMER COMPOSITION, AND VINYL CHLORIDE-BASED POLYMER COMPOSITION OBTAINED THEREBY 审中-公开
标题翻译：基于氯乙烯的树脂组合物，基于氯乙烯的聚合物组合物的制备方法和基于氯乙烯的聚合物组合物
公开(公告)号：US20110294941A1
公开(公告)日：2011-12-01
申请号：US13115369
申请日：2011-05-25
申请人： Tatsuya FUJIMOTO , Tadashi Amano , Manabu Furudate , Tomohiro Inoue , Shinji Fujimoto , Ken Yahata
发明人： Tatsuya FUJIMOTO , Tadashi Amano , Manabu Furudate , Tomohiro Inoue , Shinji Fujimoto , Ken Yahata
IPC分类号： C08K3/22 , B82Y30/00
CPC分类号： B82Y30/00
摘要： Provided is a vinyl chloride-based resin composition including a vinyl chloride-based resin and a titanium dioxide having an average particle diameter of 5 to 50 nm, in an amount of 1,000 ppm to 10,000 ppm, by mass, relative to the mass of the vinyl chloride-based resin. By adding a titanium dioxide having an average particle diameter of 5 to 50 nm to a vinyl chloride-based resin in an amount described above, a vinyl chloride-based resin composition of excellent thermal stability can be obtained. In the vinyl chloride-based resin composition, the crystalline form of the titanium dioxide is preferably anatase, rutile, or a combination thereof. Also provided is a method of producing a vinyl chloride-based polymer composition that includes subjecting a vinyl chloride monomer, or a mixture of a vinyl chloride monomer and a monomer that is copolymerizable therewith, to suspension polymerization within an aqueous medium, and also includes adding a titanium dioxide having an average particle diameter of 5 to 50 nm to the raw material prior to commencement of the polymerization, to the reaction mixture during the polymerization, to the reaction product following completion of the polymerization, or to a combination of two or more of the raw material, the reaction mixture and the reaction product. The vinyl chloride-based polymer composition obtained using this method exhibits excellent thermal stability.
摘要翻译：本发明提供一种氯乙烯类树脂组合物，其含有平均粒径为5〜50nm的氯乙烯类树脂和二氧化钛，相对于质量为1000〜10000ppm 氯乙烯类树脂。通过向上述量的氯乙烯类树脂中添加平均粒径为5〜50nm的二氧化钛，可以得到热稳定性优异的氯乙烯系树脂组合物。在氯乙烯系树脂组合物中，二氧化钛的结晶形态优选为锐钛矿型，金红石型，或其组合。还提供了一种生产氯乙烯基聚合物组合物的方法，该组合物包括使氯乙烯单体或氯乙烯单体与其可共聚的单体的混合物在水性介质中进行悬浮聚合，并且还包括加入在聚合开始前与原料平均粒径为5〜50nm的二氧化钛，聚合期间的反应混合物，聚合完成后的反应产物，或两种以上的组合的原料，反应混合物和反应产物。使用该方法获得的基于氯乙烯的聚合物组合物显示出优异的热稳定性。

10. 发明申请

US20080241452A1 FLAME RETARDANT ADHESIVE COMPOSITION, AND ADHESIVE SHEET, COVERLAY FILM AND FLEXIBLE COPPER-CLAD LAMINATE USING SAME 失效
标题翻译：阻燃粘合剂组合物，粘合片，覆盖膜和使用相同的柔性铜箔层压板
公开(公告)号：US20080241452A1
公开(公告)日：2008-10-02
申请号：US11865330
申请日：2007-10-01
申请人： Kazunori KONDO , Shigehiro Hoshida , Tadashi Amano
发明人： Kazunori KONDO , Shigehiro Hoshida , Tadashi Amano
IPC分类号： C08K5/53 , B32B33/00 , C09J7/02 , B32B7/12
CPC分类号： H05K3/386 , B32B7/12 , C08K5/0066 , C08K5/5317 , C09J7/35 , C09J2205/102 , C09J2433/00 , C09J2463/00 , C09J2471/00 , H05K1/0353 , H05K2201/012 , H05K2201/0133 , H05K2201/0769 , Y10T428/14 , Y10T428/266 , Y10T428/2804
摘要： The present invention provides a halogen-free, flame retardant adhesive composition that exhibits excellent anti-migration properties, not only within single layer structures, but also within multilayer structures of much higher density such as copper-clad laminates.The flame retardant adhesive composition according to the present invention comprises: (A) a halogen-free epoxy resin, (B) a carboxyl group-containing acrylic resin and/or a carboxyl group-containing acrylonitrile-butadiene rubber, (C) a curing agent, (E) specific phosphinate and/or diphosphonate compounds, and (F) an ion scavenger and/or a heavy metal deactivator.
摘要翻译：本发明提供了一种无卤阻燃粘合剂组合物，其不仅在单层结构内，而且在诸如覆铜层压板之类的高密度多层结构内表现出优异的抗迁移性能。根据本发明的阻燃粘合剂组合物包括：（A）无卤环氧树脂，（B）含羧基的丙烯酸树脂和/或含羧基的丙烯腈 - 丁二烯橡胶，（C）固化（E）特定的次膦酸盐和/或二膦酸盐化合物，和（F）离子清除剂和/或重金属钝化剂。

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