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1. 发明授权

US10377904B2 Inorganic hydrophilic coating solution, hydrophilic coating film obtained therefrom, and member using same 有权
公开(公告)号：US10377904B2
公开(公告)日：2019-08-13
申请号：US14116665
申请日：2012-05-31
申请人： Tomohiro Inoue , Manabu Furudate , Yoshitsugu Eguchi , Tadashi Amano
发明人： Tomohiro Inoue , Manabu Furudate , Yoshitsugu Eguchi , Tadashi Amano
IPC分类号： C09D1/00 , B01J37/02 , B01J21/08 , B01J35/00 , C09D5/16 , H01L31/048 , C09D183/02 , H02S40/10 , C09D7/61 , C09D7/40 , B01J21/06 , B01J37/03
摘要： An inorganic hydrophilic coating solution including (a) an aqueous solution containing an amorphous silicate compound obtained by hydrolyzing and condensing a tetrafunctional silicon compound having a purity of 99.0 mass % or greater in an aqueous medium in the presence of a basic compound at a temperature within a range from normal temperature to 170° C., (b) water, and optionally, (c) not more than 30 mass % of an alcohol, a ketone, or a surfactant, where the concentration of the solid fraction derived from the aqueous solution containing the amorphous silicate compound is 0.01 to 2.0 mass % and the pH is 5 to 8; an inorganic hydrophilic coating film formed from a dried and cured product of the inorganic hydrophilic coating solution; a member having a substrate and the inorganic hydrophilic coating film formed on the surface of the substrate; and a cover panel for a solar cell module including the member.

2. 发明授权

US08986580B2 Visible-light-responsive titanium oxide microparticle dispersion, and process for production thereof 有权
标题翻译：可见光响应性氧化钛微粒分散体及其制造方法
公开(公告)号：US08986580B2
公开(公告)日：2015-03-24
申请号：US13503132
申请日：2011-03-11
申请人： Manabu Furudate , Tomohiro Inoue , Yoshitsugu Eguchi , Tadashi Amano
发明人： Manabu Furudate , Tomohiro Inoue , Yoshitsugu Eguchi , Tadashi Amano
IPC分类号： C01G23/053 , C01B15/047 , C01G23/047 , C09C1/36 , B01J37/03 , B01J37/10 , B01J21/06 , B01J23/835 , B01J35/00 , B01J35/08
CPC分类号： C01G23/047 , B01J21/063 , B01J23/835 , B01J35/004 , B01J35/006 , B01J35/08 , B01J37/031 , B01J37/10 , C01P2004/04 , C01P2006/60 , C09C1/3653 , Y10T428/2991
摘要： Disclosed are: a visible-light-responsive titanium oxide microparticle dispersion comprising an aqueous dispersion medium and titanium oxide microparticles dispersed therein, and a peroxotitanium component, an iron component and/or a copper component and a tin component, wherein the content of the peroxotitanium component is 0.1 to 20 mass % relative to the titanium oxide content; and a process for producing a visible-light-responsive titanium oxide microparticle dispersion, comprising (1) producing peroxotitanic acid containing a tin compound from a raw material titanium compound, a tin compound and hydrogen peroxide, (2) heating an aqueous solution of peroxotitanic acid containing the tin compound to 80 to 250° C. under a high pressure to produce a titanium oxide microparticle dispersion containing a peroxotitanium component and a tin component, and (3) adding an iron compound and/or a copper compound to the titanium oxide microparticle dispersion to cause a reaction between the iron compound and/or the copper compound with the dispersion.
摘要翻译：本发明公开了一种包含水分散介质和分散在其中的氧化钛微粒以及过氧钛组分，铁组分和/或铜组分和锡组分的可见光响应的氧化钛微粒分散体，其中过氧钛成分相对于氧化钛含量为0.1〜20质量％以及（1）从原料钛化合物，锡化合物和过氧化氢制备含有锡化合物的过氧钛酸的方法，（2）将过氧钛酸水溶液含有锡化合物的酸在80〜250℃下高压制造含有过氧钛成分和锡成分的氧化钛微粒分散体，（3）将铁化合物和/或铜化合物加入氧化钛微粒分散体引起铁化合物和/或铜化合物与分散体之间的反应。

3. 发明申请

US20140100105A1 METHOD FOR MANUFACTURING MICROPARTICULATE ANATASE OR RUTILE TITANIUM OXIDE DISPERSION AND COMPONENT HAVING PHOTOCATALYTIC THIN FILM ON SURFACE 有权
标题翻译：用于制造微晶分解或氧化钛分散体的方法和在表面上具有光催化薄膜的组分
公开(公告)号：US20140100105A1
公开(公告)日：2014-04-10
申请号：US14115209
申请日：2012-05-10
申请人： Manabu Furudate , Tomohiro Inoue , Shiro Takahashi , Yoshitsugu Eguchi , Tadashi Amano
发明人： Manabu Furudate , Tomohiro Inoue , Shiro Takahashi , Yoshitsugu Eguchi , Tadashi Amano
IPC分类号： B01J21/08
CPC分类号： B01J21/08 , B01J21/06 , B01J21/063 , B01J23/14 , B01J35/004 , B01J35/023 , B01J37/031 , B01J37/035 , B01J37/08 , C01G23/04 , C01G23/047 , C01G23/053 , C08K2003/2241 , C09D1/00 , C09D5/1618
摘要： A method for manufacturing a microparticulate anatase or rutile titanium oxide dispersion from a peroxotitanic acid solution optionally containing tin, wherein the method for manufacturing an anatase or rutile titanium oxide dispersion is characterized in that the peroxotitanic acid solution is fed continuously to a flow reactor and subjected to hydrothermal treatment at 150 to 250° C. and 0.5 to 10 MPa. The invention makes it possible to provide a method for manufacturing a microparticulate anatase or rutile titanium oxide dispersion having excellent stability in regard to the titanium oxide microparticles and enabling a high-transparency photocatalytic thin film to be produced, and to provide a member having a photocatalytic thin film formed on the surface using this dispersion.
摘要翻译：一种由任选含有锡的过氧钛酸溶液制备微粒锐钛矿或金红石型二氧化钛分散体的方法，其中所述锐钛型或金红石型氧化钛分散体的制造方法的特征在于，将过氧钛酸溶液连续供给流动反应器，在150〜250℃，0.5〜10MPa下进行水热处理。本发明使得可以提供一种在氧化钛微粒上具有优异的稳定性的微粒锐钛矿或金红石型氧化钛分散体的制造方法，能够制造高透光性的光催化薄膜，提供具有光催化剂使用该分散体在表面上形成薄膜。

4. 发明申请

US20120214667A1 VISIBLE-LIGHT-RESPONSIVE TITANIUM OXIDE MICROPARTICLE DISPERSION, AND PROCESS FOR PRODUCTION THEREOF 有权
标题翻译：可见光反应性氧化钛微粒分散体及其生产方法
公开(公告)号：US20120214667A1
公开(公告)日：2012-08-23
申请号：US13503132
申请日：2011-03-11
申请人： Manabu Furudate , Tomohiro Inoue , Yoshitsugu Eguchi , Tadashi Amano
发明人： Manabu Furudate , Tomohiro Inoue , Yoshitsugu Eguchi , Tadashi Amano
IPC分类号： B01J21/06 , B82Y40/00 , B82Y30/00
CPC分类号： C01G23/047 , B01J21/063 , B01J23/835 , B01J35/004 , B01J35/006 , B01J35/08 , B01J37/031 , B01J37/10 , C01P2004/04 , C01P2006/60 , C09C1/3653 , Y10T428/2991
摘要： Disclosed are: a visible-light-responsive titanium oxide microparticle dispersion comprising an aqueous dispersion medium and titanium oxide microparticles dispersed therein, and a peroxotitanium component, an iron component and/or a copper component and a tin component, wherein the content of the peroxotitanium component is 0.1 to 20 mass % relative to the titanium oxide content; and a process for producing a visible-light-responsive titanium oxide microparticle dispersion, comprising (1) producing peroxotitanic acid containing a tin compound from a raw material titanium compound, a tin compound and hydrogen peroxide, (2) heating an aqueous solution of peroxotitanic acid containing the tin compound to 80 to 250° C. under a high pressure to produce a titanium oxide microparticle dispersion containing a peroxotitanium component and a tin component, and (3) adding an iron compound and/or a copper compound to the titanium oxide microparticle dispersion to cause a reaction between the iron compound and/or the copper compound with the dispersion.
摘要翻译：本发明公开了一种包含水分散介质和分散在其中的氧化钛微粒以及过氧钛组分，铁组分和/或铜组分和锡组分的可见光响应的氧化钛微粒分散体，其中过氧钛成分相对于氧化钛含量为0.1〜20质量％以及制造可见光响应性氧化钛微粒分散体的方法，其包括（1）从原料钛化合物，锡化合物和过氧化氢制备含锡化合物的过氧钛酸，（2）加热过氧钛酸水溶液含有锡化合物的酸在80〜250℃下高压制造含有过氧钛成分和锡成分的氧化钛微粒分散体，（3）将铁化合物和/或铜化合物加入氧化钛微粒分散体引起铁化合物和/或铜化合物与分散体之间的反应。

5. 发明授权

US09463436B2 Method for manufacturing microparticulate anatase or rutile titanium oxide dispersion and component having photocatalytic thin film on surface 有权
标题翻译：微粒锐钛矿或金红石钛氧化物分散体的制造方法及表面具有光催化薄膜的成分
公开(公告)号：US09463436B2
公开(公告)日：2016-10-11
申请号：US14115209
申请日：2012-05-10
申请人： Manabu Furudate , Tomohiro Inoue , Shiro Takahashi , Yoshitsugu Eguchi , Tadashi Amano
发明人： Manabu Furudate , Tomohiro Inoue , Shiro Takahashi , Yoshitsugu Eguchi , Tadashi Amano
IPC分类号： B01J21/08 , B01J37/03 , B01J37/08 , B01J23/14 , B01J35/00 , C09D1/00 , C09D5/16 , B01J21/06 , C01G23/047 , C01G23/04 , C01G23/053 , B01J35/02 , C08K3/22
CPC分类号： B01J21/08 , B01J21/06 , B01J21/063 , B01J23/14 , B01J35/004 , B01J35/023 , B01J37/031 , B01J37/035 , B01J37/08 , C01G23/04 , C01G23/047 , C01G23/053 , C08K2003/2241 , C09D1/00 , C09D5/1618
摘要： A method for manufacturing a microparticulate anatase or rutile titanium oxide dispersion from a peroxotitanic acid solution optionally containing tin, wherein the method for manufacturing an anatase or rutile titanium oxide dispersion is characterized in that the peroxotitanic acid solution is fed continuously to a flow reactor and subjected to hydrothermal treatment at 150 to 250° C. and 0.5 to 10 MPa. The invention makes it possible to provide a method for manufacturing a microparticulate anatase or rutile titanium oxide dispersion having excellent stability in regard to the titanium oxide microparticles and enabling a high-transparency photocatalytic thin film to be produced, and to provide a member having a photocatalytic thin film formed on the surface using this dispersion.
摘要翻译：一种由任选含有锡的过氧钛酸溶液制备微粒锐钛矿或金红石型二氧化钛分散体的方法，其中所述锐钛型或金红石型氧化钛分散体的制造方法的特征在于，将过氧钛酸溶液连续供给流动反应器，在150〜250℃，0.5〜10MPa下进行水热处理。本发明使得可以提供一种在氧化钛微粒上具有优异的稳定性的微粒锐钛矿或金红石型氧化钛分散体的制造方法，能够制造高透光性的光催化薄膜，提供具有光催化剂使用该分散体在表面上形成薄膜。

6. 发明申请

US20140127514A1 INORGANIC HYDROPHILIC COATING SOLUTION, HYDROPHILIC COATING FILM OBTAINED THEREFROM, AND MEMBER USING SAME 审中-公开
标题翻译：无机水解涂料溶液，由其获得的水性涂料膜，以及使用其的成员
公开(公告)号：US20140127514A1
公开(公告)日：2014-05-08
申请号：US14116665
申请日：2012-05-31
申请人： Tomohiro Inoue , Manabu Furudate , Yoshitsugu Eguchi , Tadashi Amano
发明人： Tomohiro Inoue , Manabu Furudate , Yoshitsugu Eguchi , Tadashi Amano
IPC分类号： C09D1/00
CPC分类号： C09D1/00 , B01J21/063 , B01J21/08 , B01J35/002 , B01J35/004 , B01J37/0219 , B01J37/033 , C09D5/1662 , C09D7/61 , C09D7/67 , C09D183/02 , H01L31/048 , H02S40/10 , Y02E10/50 , Y10T428/31507 , Y10T428/31667
摘要： An inorganic hydrophilic coating solution including (a) an aqueous solution containing an amorphous silicate compound obtained by hydrolyzing and condensing a tetrafunctional silicon compound having a purity of 99.0 mass % or greater in an aqueous medium in the presence of a basic compound at a temperature within a range from normal temperature to 170° C., (b) water, and optionally, (c) not more than 30 mass % of an alcohol, a ketone, or a surfactant, where the concentration of the solid fraction derived from the aqueous solution containing the amorphous silicate compound is 0.01 to 2.0 mass % and the pH is 5 to 8; an inorganic hydrophilic coating film formed from a dried and cured product of the inorganic hydrophilic coating solution; a member having a substrate and the inorganic hydrophilic coating film formed on the surface of the substrate; and a cover panel for a solar cell module including the member.
摘要翻译：一种无机亲水性涂料溶液，其包括（a）含有无定形硅酸盐化合物的水溶液，所述无定形硅酸盐化合物通过在碱性化合物的存在下，在碱性化合物的存在下，在碱性化合物的存在下水解和缩合纯度为99.0质量％以上的四官能硅化合物，（b）水，和（c）不大于30质量％的醇，酮或表面活性剂，其中固体成分的浓度来源于水溶液含有无定形硅酸盐化合物的溶液为0.01〜2.0质量％，pH为5〜8; 由无机亲水性涂布液的干燥固化物形成的无机亲水性涂膜; 具有基材和在所述基材的表面上形成的无机亲水性涂膜的部件; 以及包括该构件的太阳能电池模块用盖板。

7. 发明申请

US20110294941A1 VINYL CHLORIDE-BASED RESIN COMPOSITION, METHOD OF PRODUCING VINYL CHLORIDE-BASED POLYMER COMPOSITION, AND VINYL CHLORIDE-BASED POLYMER COMPOSITION OBTAINED THEREBY 审中-公开
标题翻译：基于氯乙烯的树脂组合物，基于氯乙烯的聚合物组合物的制备方法和基于氯乙烯的聚合物组合物
公开(公告)号：US20110294941A1
公开(公告)日：2011-12-01
申请号：US13115369
申请日：2011-05-25
申请人： Tatsuya FUJIMOTO , Tadashi Amano , Manabu Furudate , Tomohiro Inoue , Shinji Fujimoto , Ken Yahata
发明人： Tatsuya FUJIMOTO , Tadashi Amano , Manabu Furudate , Tomohiro Inoue , Shinji Fujimoto , Ken Yahata
IPC分类号： C08K3/22 , B82Y30/00
CPC分类号： B82Y30/00
摘要： Provided is a vinyl chloride-based resin composition including a vinyl chloride-based resin and a titanium dioxide having an average particle diameter of 5 to 50 nm, in an amount of 1,000 ppm to 10,000 ppm, by mass, relative to the mass of the vinyl chloride-based resin. By adding a titanium dioxide having an average particle diameter of 5 to 50 nm to a vinyl chloride-based resin in an amount described above, a vinyl chloride-based resin composition of excellent thermal stability can be obtained. In the vinyl chloride-based resin composition, the crystalline form of the titanium dioxide is preferably anatase, rutile, or a combination thereof. Also provided is a method of producing a vinyl chloride-based polymer composition that includes subjecting a vinyl chloride monomer, or a mixture of a vinyl chloride monomer and a monomer that is copolymerizable therewith, to suspension polymerization within an aqueous medium, and also includes adding a titanium dioxide having an average particle diameter of 5 to 50 nm to the raw material prior to commencement of the polymerization, to the reaction mixture during the polymerization, to the reaction product following completion of the polymerization, or to a combination of two or more of the raw material, the reaction mixture and the reaction product. The vinyl chloride-based polymer composition obtained using this method exhibits excellent thermal stability.
摘要翻译：本发明提供一种氯乙烯类树脂组合物，其含有平均粒径为5〜50nm的氯乙烯类树脂和二氧化钛，相对于质量为1000〜10000ppm 氯乙烯类树脂。通过向上述量的氯乙烯类树脂中添加平均粒径为5〜50nm的二氧化钛，可以得到热稳定性优异的氯乙烯系树脂组合物。在氯乙烯系树脂组合物中，二氧化钛的结晶形态优选为锐钛矿型，金红石型，或其组合。还提供了一种生产氯乙烯基聚合物组合物的方法，该组合物包括使氯乙烯单体或氯乙烯单体与其可共聚的单体的混合物在水性介质中进行悬浮聚合，并且还包括加入在聚合开始前与原料平均粒径为5〜50nm的二氧化钛，聚合期间的反应混合物，聚合完成后的反应产物，或两种以上的组合的原料，反应混合物和反应产物。使用该方法获得的基于氯乙烯的聚合物组合物显示出优异的热稳定性。

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