会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 1. 发明授权
    • Process for producing vinyl chloride polymer with low residual monomer
    • 生产具有低残留单体的氯乙烯聚合物的方法
    • US06448372B2
    • 2002-09-10
    • US09764093
    • 2001-01-19
    • Takashi KobayashiRyuichi SaitoYoshinori NakaharaTadashi AmanoIchiro Hara
    • Takashi KobayashiRyuichi SaitoYoshinori NakaharaTadashi AmanoIchiro Hara
    • C08F624
    • C08F6/003C08F14/06C08L27/06C08F2/18
    • A process for producing a vinyl chloride polymer, including the steps of (a) subjecting a vinyl chloride monomer alone or a monomer mixture containing a vinyl chloride, to suspension polymerization in water; (b) subjecting the resultant vinyl chloride polymer slurry to stripping to remove an unreacted monomer remaining therein; and (c) dehydrating the polymer slurry having been subjected to stripping. In the polymerization step (a), the ratio of water/monomer is set in a weight ratio of from 0.80 to 1.50, and the viscosity at 20° C. of the polymer slurry to be fed to the stripping step is previously kept adjusted to 0.30 Pa·s or lower. In the stripping step (c), the residual unreacted monomer in the polymer slurry can efficiently be removed using steam in a smaller quantity, thus the vinyl chloride polymer can be produced at a high productivity.
    • 一种制备氯乙烯聚合物的方法,包括以下步骤:(a)使单独的氯乙烯单体或含有氯乙烯的单体混合物在水中悬浮聚合; (b)将得到的氯乙烯聚合物浆料进行汽提以除去其中残留的未反应单体; 和(c)使经过剥离的聚合物浆料脱水。 在聚合步骤(a)中,将水/单体的比例设定为0.80至1.50的重量比,并将预先进料到汽提步骤的聚合物浆料的20℃下的粘度预先保持在 0.30 Pa.s以下。 在汽提步骤(c)中,聚合物淤浆中残留的未反应单体可以用较少量的蒸汽有效地除去,从而可以高生产率生产氯乙烯聚合物。
    • 3. 发明授权
    • Method of producing vinyl-based polymer
    • 乙烯基类聚合物的制造方法
    • US06677409B2
    • 2004-01-13
    • US10122304
    • 2002-04-16
    • Ryuichi SaitoTadashi Amano
    • Ryuichi SaitoTadashi Amano
    • C08F240
    • C08F2/40
    • A method of producing a vinyl-based polymer is provided in which the blocking of piping resulting from solidification of a reaction inhibitor does not occur even if the operation of supplying the reaction inhibitor is conducted at a low temperature. This method involves the polymerization of a vinyl monomer via a radical reaction, wherein a reaction inhibitor formed from a compound represented by a general formula (1), shown below, is added to the polymerization system in the form of an aqueous dispersion, either prior to commencement of the polymerization, during the polymerization, or following completion of the polymerization, depending on the effect desired. R represents an alkyl group of 3 to 6 carbon atoms.
    • 提供了一种制备乙烯基类聚合物的方法,其中即使在低温下进行反应抑制剂的操作,也不会发生阻止由反应抑制剂固化产生的管道。 该方法包括通过自由基反应聚合乙烯基单体,其中将由下述通式(1)表示的化合物形成的反应抑制剂以水分散体的形式加入到聚合体系中,先前 根据所需的效果,聚合反应开始,聚合期间或聚合结束后,R表示3〜6个碳原子的烷基。
    • 4. 发明授权
    • Production process for vinyl-based polymer
    • 乙烯基聚合物的生产工艺
    • US06639027B2
    • 2003-10-28
    • US10319550
    • 2002-12-16
    • Ryuichi SaitoTadashi AmanoToshihiko Kawakubo
    • Ryuichi SaitoTadashi AmanoToshihiko Kawakubo
    • C08F242
    • C08F2/40C08F14/06Y10S526/91Y10S526/911C08F2/16
    • A production process for a vinyl-based polymer is provided. The production process comprises a step for polymerizing a vinyl-based monomer by a radical reaction within an aqueous medium in a polymerization vessel, and a step for supplying a reaction inhibitor with a melting point of no more than 40° C. from a reaction inhibitor supply tank to the polymerization vessel via a reaction inhibitor supply pipe. The reaction inhibitor supply tank and the reaction inhibitor supply pipe are heated, and the reaction inhibitor is added to the polymerization vessel in a liquid state with a viscosity of no more than 200 mPa·s. The reaction inhibitor can be added to the polymerization mixture without the use of an organic solvent even at low temperatures, and problems such as the solidification of the reaction inhibitor inside the supply tank or piping, and subsequent blocking of the piping do not occur.
    • 提供了一种乙烯基类聚合物的制造方法。 制造方法包括在聚合容器内的水性介质中通过自由基反应聚合乙烯基类单体的步骤,以及从反应抑制剂供给不超过40℃的熔点的反应抑制剂的步骤 通过反应抑制剂供应管向聚合容器供应罐。 反应抑制剂供给槽和反应抑制剂供给管被加热,反应抑制剂以粘度不超过200mPa.s的液态加入到聚合容器中。 反应抑制剂即使在低温下也可以不使用有机溶剂而添加到聚合混合物中,并且不会发生诸如供给罐或管道内的反应抑制剂的固化以及随后的管道堵塞等问题。
    • 5. 发明授权
    • Process for producing vinylidene fluoride resin
    • 偏二氟乙烯树脂的制造方法
    • US5925721A
    • 1999-07-20
    • US25237
    • 1998-02-18
    • Ryuichi SaitoTadashi Amano
    • Ryuichi SaitoTadashi Amano
    • C08F2/44C08F2/00C08F14/22C08F214/22
    • C08F214/22C08F14/22
    • In a process for producing a vinylidene fluoride resin by polymerizing vinylidene fluoride or a mixture of vinylidene fluoride and a vinyl monomer copolymerizable with vinylidene fluoride, a portion of an iodide compound represented by the formula: X-R.sub.f -X wherein R.sub.f is a divalent organic group containing at least two divalent fluoroalkyl ether groups: and X's are independently an iodine atom or a fluorine atom, provided that at least one of the X's is an iodine atom; is added to start the polymerization, and the remainder of the iodide compound is further added dividedly at least twice in the course of the polymerization. This process enables to obtain a vinylidene fluoride resin having a viscosity-average molecular weight of 150,000 or more and also having a superior water repellency. This resin has good mechanical strength and release properties and also can be well processed into films.
    • 在通过聚合偏二氟乙烯或偏二氟乙烯与可与偏二氟乙烯共聚的乙烯基单体的混合物制备偏二氟乙烯树脂的方法中,一部分由下式表示的碘化合物:X-Rf-X其中Rf是二价有机 含有至少两个二价氟烷基醚基团的基团:X独立地为碘原子或氟原子,条件是X中的至少一个为碘原子; 加入以开始聚合,剩余的碘化合物在聚合过程中进一步加入至少两次。 该方法能够得到粘均分子量为15万以上且具有优异的拒水性的偏二氟乙烯树脂。 该树脂具有良好的机械强度和剥离性能,并且可以很好地加工成膜。
    • 7. 发明申请
    • RUTHENIUM FILM-FORMING MATERIAL AND RUTHENIUM FILM-FORMING METHOD
    • 形成薄膜的成膜材料和成膜方法
    • US20120282414A1
    • 2012-11-08
    • US13503899
    • 2010-10-20
    • Ryuichi SaitoKang-go ChungHideki NishimuraTatsuya Sakai
    • Ryuichi SaitoKang-go ChungHideki NishimuraTatsuya Sakai
    • C07F15/00B05D3/02B05D3/06B05D7/24
    • C23C16/18C07C49/92C07F15/0046H01L21/76843H01L28/65
    • Disclosed is a ruthenium film-forming material having a lower melting point and a higher vapor pressure that facilitates supply of the material onto a base and moreover enables a high-quality ruthenium film to be obtained.A ruthenium film-forming material includes a compound represented by general formula (1) below (wherein R1 is independently at each occurrence a hydrogen atom, a halogen atom, a hydrocarbon group having 1 to 4 carbon atoms or a halogenated hydrocarbon group having 1 to 4 carbon atoms; R2 is independently at each occurrence a halogenated hydrocarbon group having 1 to 4 carbon atoms, an alkoxy group having 1 to 4 carbon atoms or a halogenated alkoxy group having 1 to 4 carbon atoms, with the proviso that R1 and R2 are mutually differing groups; R3 is independently at each occurrence a hydrogen atom or a hydrocarbon group having 1 to 4 carbon atoms; and L is an unsaturated hydrocarbon compound having 4 to 10 carbon atoms and having at least two double bonds).
    • 公开了一种具有较低熔点和较高蒸气压的钌膜形成材料,其有助于将材料供应到基底上,并且还能够获得高质量的钌膜。 钌膜形成材料包括由下述通式(1)表示的化合物(其中R 1在每次出现时独立地为氢原子,卤素原子,具有1至4个碳原子的烃基或卤代烃基,其具有1至 4个碳原子; R 2在每次出现时独立地为具有1至4个碳原子的卤代烃基,具有1至4个碳原子的烷氧基或具有1至4个碳原子的卤代烷氧基,条件是R 1和R 2为 相互不同的基团; R 3在每次出现时独立地为氢原子或具有1至4个碳原子的烃基; L为具有4至10个碳原子且具有至少两个双键的不饱和烃化合物)。