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1. 发明授权

US4499153A Sizes 失效
标题翻译：尺寸
公开(公告)号：US4499153A
公开(公告)日：1985-02-12
申请号：US466708
申请日：1983-02-15
申请人： Wulf von Bonin , Peter Mummenhoff , Ulrich Beck , Heinz Baumgen
发明人： Wulf von Bonin , Peter Mummenhoff , Ulrich Beck , Heinz Baumgen
IPC分类号： D21H17/07 , C08L91/00 , B32B27/06 , D21D3/00
CPC分类号： D21H17/07 , Y10T428/31783
摘要： New products having excellent sizing action, in particular on paper are obtained by reacting .alpha.,.beta.-unsaturated carboxylic acids or their reactive derivatives (such as, for example, esters or anhydrides) with amide-amines of higher carboxylic acids at temperatures above 120.degree. C.The new products are used in size formulations, preferably as aqueous alkaline and, in particular, aqueous ammoniacal, dispersions.
摘要翻译：通过使α，β-不饱和羧酸或其反应性衍生物（例如酯或酸酐）与高于120℃的高羧酸的酰胺 - 胺反应，得到具有优异施胶作用的新产品，特别是在纸上。 C.新产品用于尺寸配方中，优选用作碱性水溶液，特别是氨水分散体。

2. 发明授权

US4381367A Sizing agents for paper and a process for the production thereof 失效
标题翻译：纸张上浆剂及其生产方法
公开(公告)号：US4381367A
公开(公告)日：1983-04-26
申请号：US328009
申请日：1981-12-07
申请人： Wulf von Bonin , Peter Mummenhoff , Heinz Baumgen
发明人： Wulf von Bonin , Peter Mummenhoff , Heinz Baumgen
IPC分类号： C08F220/12 , D21H17/43 , C08F8/32
CPC分类号： D21H17/43 , C08F220/12 , Y10T428/31906
摘要： Paper sizing agents in the form of an aqueous preparation of maleic acid anhydride copolymers of which the anhydride groups had been reacted either with organic or inorganic bases or with primary-tertiary diamines and the reaction products subsequently reacted with epichlorohydrin or with inorganic or organic acids to form salts, the copolymers being made up of polymerised units of(a) from 5 to 75%, by weight, of an aromatic vinyl compound;(b) from 10 to 75%, by weight, of acrylic and/or methacrylic acid C.sub.1 -C.sub.18 alkyl esters;(c) from 5 to 35%, by weight, of maleic acid anhydride;(d) from 0 to 25%, by weight, of other vinyl monomers; and(e) from 0.1 to 10%, by weight, based on the sum of monomers (a) to (d) (which amounts to 100%, by weight), of an unsaturated aldehyde or of an enol ether derived therefrom.The copolymers are produced by radical polymerisation preferably in the absence of solvents.
摘要翻译：以马来酸酐共聚物形式的纸浆施胶剂，其酸酐基已经与有机或无机碱反应或与伯 - 叔二胺反应，反应产物随后与表氯醇或无机或有机酸反应，所述共聚物由（a）5-75重量％的芳族乙烯基化合物的聚合单元组成; （b）10至75重量％的丙烯酸和/或甲基丙烯酸C1-C18烷基酯; （c）5至35重量％的马来酸酐; （d）0-25重量％的其它乙烯基单体; 和（e）基于单体（a）至（d）（其为100重量％））的不饱和醛或由其衍生的烯醇醚的总量的0.1至10重量％。

3. 发明授权

US4568391A Sizing agents 失效
标题翻译：施胶剂
公开(公告)号：US4568391A
公开(公告)日：1986-02-04
申请号：US566644
申请日：1983-12-29
申请人： Wulf von Bonin , Hans-Ulrich Buschhaus , Ulrich Beck , Heinz Baumgen
发明人： Wulf von Bonin , Hans-Ulrich Buschhaus , Ulrich Beck , Heinz Baumgen
IPC分类号： D21H19/10 , C07C68/02 , D21H17/14 , C09K3/00 , C07C68/00
CPC分类号： D21H17/14 , C07C68/02
摘要： The invention provides new sizing agents, in particular for paper, which contain chloroformic acid esters of ester alcohols and/or carboxamide alcohols.The chloroformic acid esters in question preferably have the following idealized structure:(RCOX).sub.n R'(OCOCL).sub.m (I)whereinX=an oxygen atom or an NH radical,R=an aliphatic, araliphatic or cycloaliphatic hydrocarbon radical having 8 to 28 carbon atoms,R'=the radical of an (n+m)-functional alcohol or amino alcohol having 2 to 10 carbon atoms, where the functionality refers to the total number of OH and NH.sub.2 groups,n=an integer from 1 to 4, andm=an integer from 1 to 3.
摘要翻译：本发明提供了新的上浆剂，特别是用于纸，其含有酯醇和/或羧酰胺醇的氯甲酸酯。所讨论的氯甲酸酯优选具有以下理想化结构：（RCOX）nR'（OCOCL）m（I）其中X =氧原子或NH基，R =具有8至28的脂族，芳脂族或脂环族烃基碳原子，R'=具有2至10个碳原子的（n + m） - 官能醇或氨基醇的基团，其中官能度是指OH和NH 2基团的总数，n = 1至4的整数，m = 1〜3的整数。

4. 发明授权

US4614546A Sizes based on ketene dimers 失效
标题翻译：基于烯酮二聚体的尺寸
公开(公告)号：US4614546A
公开(公告)日：1986-09-30
申请号：US738640
申请日：1985-05-29
申请人： Wolf-Dieter Schroer , Ulrich Beck , Peter Mummenhoff , Heinz Baumgen
发明人： Wolf-Dieter Schroer , Ulrich Beck , Peter Mummenhoff , Heinz Baumgen
IPC分类号： D21H17/17 , C08L3/00
CPC分类号： D21H17/17
摘要： New aqueous sizes, in particular paper sizes, are made available which contain(a) ketene dimers of the formula ##STR1## in which R.sub.1 and R.sub.2 can be identical or different and represent hydrocarbon radicals having 6 to 30 carbon atoms,(b) amine-modified starch,(c) hydrophobic compound(s) which contain(s) one or more functional groups which are reactive towards OH groups within a pH range of 2 to 6, and(d) if desired further auxiliaries.
摘要翻译：提供新的水性尺寸，特别是纸张尺寸，其包含（a）式（I）的烯酮二聚体，其中R 1和R 2可以相同或不同，并且表示具有6至30个碳原子的烃基（ b）胺改性的淀粉，（c）含有一个或多个官能团的疏水性化合物，所述官能团在pH范围为2-6范围内对OH基团具有反应性，和（d）如果需要的话还有其他助剂。

5. 发明授权

US4784727A Sizing agent and use thereof 失效
标题翻译：上浆剂及其用途
公开(公告)号：US4784727A
公开(公告)日：1988-11-15
申请号：US459314
申请日：1983-01-20
申请人： Wolf-Dieter Schroer , Joachim Probst , Ingeborg Kolb , Ulrich Beck , Peter Mummenhoff , Heinz Baumgen
发明人： Wolf-Dieter Schroer , Joachim Probst , Ingeborg Kolb , Ulrich Beck , Peter Mummenhoff , Heinz Baumgen
IPC分类号： D21H17/08 , D21H17/15 , D21H17/17 , D21H17/35 , D21H17/36 , D21H17/37 , D21H17/45 , D21H3/02
CPC分类号： D21H17/08 , D21H17/15 , D21H17/17 , D21H17/35 , D21H17/36 , D21H17/37 , D21H17/455
摘要： A sizing agent which contains from 1 to 60 parts, by weight, of a fixing and sizing accelerating agent and from 0 to 80 parts, by weight, of conventional auxiliaries per 10 parts by weight of hydrophobic, cellulose-reactive sizing materials, the fixing and sizing accelerating agent being a polymer composed of linear or branched carbon chains, to which primary, secondary or tertiary amino and/or quaternary ammonium groups are bound directly or by side chains exhibits a thorough and rapid sizing effect, in particular in the better sizing of paper.
摘要翻译：一种施胶剂，其含有1至60重量份的定影和施胶促进剂和0至80重量份的常规助剂，每10重量份疏水性纤维素反应性施胶材料，固定和作为由直链或支链碳链构成的聚合物的定型促进剂，其中伯，仲或叔氨基和/或季铵基团直接或由侧链结合，表现出彻底和快速的施胶效果，特别是在更好的施胶的纸。

6. 发明授权

US4806591A Cationic sizing agents for paper 失效
标题翻译：阳离子上胶剂纸
公开(公告)号：US4806591A
公开(公告)日：1989-02-21
申请号：US921173
申请日：1986-10-20
申请人： Joachim Probst , Heinz Baumgen , Bruno Bomer , Joachim Konig , Renke Mottweiler
发明人： Joachim Probst , Heinz Baumgen , Bruno Bomer , Joachim Konig , Renke Mottweiler
IPC分类号： C08F2/28 , C08F2/24 , C08F257/02 , D21H17/35 , D21H17/37 , D21H17/45 , C08L33/20
CPC分类号： D21H17/455 , C08F2/24 , C08F257/02 , D21H17/35 , D21H17/37
摘要： Cationic sizing agents for paper, obtainable by a process in which a water-soluble cationic terpolymer compound, built up in a chemically uniform manner, of (a) 7 to 40% by weight of N,N-dimethylaminoethyl acrylate and/or methacrylate, (b) 40 to 80% by weight of styrene and (c) 4 to 50% by weight of acrylonitrile, the sum of components (a) to (c) always being 100% by weight and at least 10% of the dimethylamino groups of the terpolymer being quaternized with monoepoxides, with the exception of epihalogenohydrins, and the remainder being protonated, is dissolved in an aqueous medium and, in the presence of 10 to 70% by weight--based on the following monomer mixture--of this emulsifier, (d) 5 to 95% by weight of acrylonitrile, meth-acrylonitrile or styrene or mixtures thereof and (e) 5 to 95% by weight of acrylic acid ester and/or methacrylic acid ester with 1 to 12 C atoms in the alcohol radical--the sum of components (d) and (e) always being 100% by weight--are emulsified and the emulsion thus obtained is subjected to emulsion polymerization, initiated by free radicals, at temperatures of 20.degree. to 150.degree. C.
摘要翻译：可通过以下方法获得的阳离子上胶剂：其中以（a）7〜40重量％的N，N-二甲基氨基乙基丙烯酸酯和/或甲基丙烯酸酯组成的以化学均匀的方式构成的水溶性阳离子三元共聚物，（b）40至80重量％的苯乙烯和（c）4至50重量％的丙烯腈，组分（a）至（c）的总和总是100重量％，并且至少10重量％的二甲基氨基的三元共聚物被单过氧化物季铵化，除了表卤代醇，其余的被质子化，溶解在水性介质中，并且在该乳化剂的基于下列单体混合物的10至70重量％的存在下，（d）5至95重量％的丙烯腈，甲基丙烯腈或苯乙烯或其混合物，和（e）5至95重量％的醇基中具有1至12个C原子的丙烯酸酯和/或甲基丙烯酸酯组分（d）和（e）总是为100重量％的总和被乳化和乳液由此获得的乳液聚合在20℃至150℃的温度下由自由基引发。

7. 发明授权

US4614759A Surface sizing agents for paper 失效
标题翻译：纸表面施胶剂
公开(公告)号：US4614759A
公开(公告)日：1986-09-30
申请号：US762601
申请日：1985-08-05
申请人： Gunter Sackmann , Ulrich Beck , Heinz Baumgen
发明人： Gunter Sackmann , Ulrich Beck , Heinz Baumgen
IPC分类号： D21H17/37 , C08F8/14 , D21H17/43 , C08L35/02
CPC分类号： C08F8/14 , D21H17/43
摘要： Surface sizing agents for paper containing aqueous or aqueous-alcoholic alkali metal, amine or ammonium salt solutions of copolymers of maleic anhydride and diisobutylene and, if appropriate, a vinyl monomer of the formula ##STR1## in which R designates H, --CH.sub.3, --C.sub.2 H.sub.5, --OR.sub.2, --OCOCH.sub.3, ##STR2## or --CH.sub.2 --O--COCH.sub.3, R.sub.1 designates H or --CH.sub.3 andR.sub.2 designates alkyl, the anhydride groups of the copolymers being bis-esterified to the extent of 25-90 mol % with primary aliphatic monoalcohols with 1 to 12 C atoms.
摘要翻译：含有水性或水性醇碱金属的纸的表面施胶剂，马来酸酐和二异丁烯的共聚物的胺或铵盐溶液，以及如果合适的话，其中R表示H，-CH 3， -C2H5，-OR2，-OCOCH3，...或-CH2-O-COCH3，R1表示H或-CH3，R2表示烷基，共聚物的酸酐基被双酯化至25〜90摩尔％具有1至12个C原子的伯脂族一元醇。

8. 发明授权

US5314721A Process for sizing paper 失效
标题翻译：纸张尺寸的过程
公开(公告)号：US5314721A
公开(公告)日：1994-05-24
申请号：US000751
申请日：1993-01-05
申请人： Michael Muller , Joachim Probst , Heinrich Alberts , Joachim Konig , Heinz Baumgen , Fritz Puchner
发明人： Michael Muller , Joachim Probst , Heinrich Alberts , Joachim Konig , Heinz Baumgen , Fritz Puchner
IPC分类号： C08F2/22 , B01F17/52 , C08F2/28 , D21H17/56 , D21H21/16 , D21H27/00 , B05D3/02
CPC分类号： C08F2/28
摘要： The new vinyl polymer dispersions are obtainable by free radical polymerisation of olefinically unsaturated monomers in the presence of a cationic polyamidoamine which has been rendered hydrophobic, and can be used as sizing agents for paper which are distinguished, in particular, by their shear, electrolyte, heat and storage stability.
摘要翻译：新的乙烯基聚合物分散体可以通过烯属不饱和单体的自由基聚合在阳离子聚酰胺胺存在下获得，该阳离子聚酰胺胺已经变得疏水，并且可以用作纸的上浆剂，特别是其剪切，电解质，储热稳定。

9. 发明授权

US4931510A Polymers from ethylenic monomers 失效
标题翻译：乙烯单体的聚合物
公开(公告)号：US4931510A
公开(公告)日：1990-06-05
申请号：US312089
申请日：1989-02-17
申请人： Gunter Sackmann , Joachim Konig , Heinz Baumgen
发明人： Gunter Sackmann , Joachim Konig , Heinz Baumgen
IPC分类号： C08F210/10 , B01F17/52 , C08F2/24 , C08F8/00 , C08F267/10 , D21H17/34 , D21H19/20 , D21H21/16
CPC分类号： D21H21/16 , C08F267/10 , D21H17/34
摘要： Polymers obtainable by subjecting at least one monomer, polymerizable by free radicals, to a free-radical emulsion polymerization in the presence of a polymer of the formulae I and/or II ##STR1## in which M, n, R, R.sup.1, R.sup.2, x and y have the meanings mentioned in the description, the use of the polymers obtained for surface-sizing of paper or paper-like materials and also novel polymers of the formulae I and/or II.
摘要翻译：聚合物可以通过使至少一种可自由基聚合的单体在式I和/或II的聚合物存在下进行自由基乳液聚合，其中M，n，R R1，R2，x和y具有说明书中提到的含义，用于纸或纸状材料表面施胶的聚合物的用途，以及式I和/或II的新型聚合物。

10. 发明授权

US4616061A Aqueous solutions or dispersions of polyisocyanate addition products, a process for the production thereof and the use thereof as coating agents or as sizing agents for paper 失效
标题翻译：多异氰酸酯加成产物的水溶液或分散体，其制备方法及其作为涂布剂或作为纸张施胶剂的用途
公开(公告)号：US4616061A
公开(公告)日：1986-10-07
申请号：US785818
申请日：1985-10-09
申请人： Wolfgang Henning , Walter Meckel , Ulrich Beck , Heinz Baumgen
发明人： Wolfgang Henning , Walter Meckel , Ulrich Beck , Heinz Baumgen
IPC分类号： D06M15/564 , C08G18/00 , C08G18/08 , C08G18/28 , C08G18/38 , C08G18/78 , D21H17/46 , D21H17/57 , D21H19/24 , D21H19/44 , C08L75/04
CPC分类号： C08G18/3823 , C08G18/0819 , C08G18/283 , C08G18/7818 , D21H17/57 , Y10T428/31551 , Y10T428/31558 , Y10T428/31562 , Y10T428/31565 , Y10T428/31569 , Y10T428/31591 , Y10T428/31598 , Y10T428/31601
摘要： The present invention relates to aqueous solutions or dispersions of polyisocyanate addition products, which contain a quantity of incorporated sulphonate and/or carboxylate groups and optionally ethylene oxide units, --CH.sub.2 --CH.sub.2 --O--, incorporated in a polyether chain to guarantee the solubility or dispersibility thereof in water, the content of sulphonate and/or carboxylate groups being about 2 to 300 milliequivalents per 100 g of solids and the content of the aforementioned ethylene oxide units being up to about 25% by weight, based on solids, characterized in that the polyisocyanate addition products have segments incorporated in the polymer chain which correspond to the following general formula: ##STR1## in an amount of about 0.1 to 20% by weight based on the above formulas, but excluding the weight of R.The present invention also relates to a process for the production of the polyisocyanate addition products and to their use as coating agents for flexible or inflexible substrates and as sizing agents for paper or for the production of sizing agents for paper.
摘要翻译：本发明涉及多异氰酸酯加成产物的水溶液或分散体，其含有一定数量的并入的磺酸盐和/或羧酸酯基团和任选的环氧乙烷单元-CH 2 -CH 2 -O-（其掺入聚醚链中以保证溶解度或其在水中的分散性，磺酸盐和/或羧酸盐基团的含量为每100g固体约2至300毫当量，并且上述环氧乙烷单元的含量基于固体高达约25重量％，其特征在于多异氰酸酯加成产物具有引入到聚合物链中的链段，其对应于以下通式：基于上式而为约0.1至20重量％，但不包括R的重量。本发明还涉及用于制备多异氰酸酯加成产物的方法及其作为柔性或不柔性基材的包衣剂的用途作为纸张的上浆剂或用于生产纸张施胶剂。

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