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1. 发明授权

US4036897A Production of hexachlorocyclopentadiene 失效
标题翻译：生产六氯环戊二烯
公开(公告)号：US4036897A
公开(公告)日：1977-07-19
申请号：US711632
申请日：1976-08-04
申请人： Vincent A. Strangio , Herbert Riegel , Morgan C. Sze
发明人： Vincent A. Strangio , Herbert Riegel , Morgan C. Sze
IPC分类号： C07C17/10 , C07C23/08
CPC分类号： C07C17/10
摘要： Hexachlorocyclopentadiene is produced by contacting pentane, pentene, cyclopentane or cyclopentene or chlorinated derivatives thereof with a molten salt mixture of cuprous and cupric chloride. Cyclopentadiene can also be employed as an initial feed, in which case the cyclopentadiene is initially chlorinated to effect saturation thereof, followed by contacting of the chloro substituted cyclopentane with a molten salt mixture of cuprous and cupric chloride to produce hexachlorocyclopentadiene.
摘要翻译：六氯环戊二烯通过使戊烷，戊烯，环戊烷或环戊烯或其氯化衍生物与亚铜和氯化铜的熔盐混合物接触来制备。环戊二烯也可以用作初始进料，在这种情况下，环戊二烯最初被氯化以使其饱和，接着氯取代的环戊烷与亚铜和氯化铜的熔融盐混合物接触以产生六氯环戊二烯。

2. 发明授权

US4045504A Coupling process 失效
标题翻译：耦合过程
公开(公告)号：US4045504A
公开(公告)日：1977-08-30
申请号：US671388
申请日：1976-03-29
申请人： Maurice E. Brooks , Herbert Riegel , Harvey D. Schindler , Morgan C. Sze
发明人： Maurice E. Brooks , Herbert Riegel , Harvey D. Schindler , Morgan C. Sze
IPC分类号： C07C2/76 , C07C2/82 , C07C3/52 , C07C15/10
CPC分类号： C07C2/82 , C07C2/76 , C07C67/035 , C07C2527/10 , C07C2527/122
摘要： Process for coupling an alkane to either an alkane, alkene, aliphatic carboxylic acid, or aromatic hydrocarbon by effecting contacting thereof and a melt containing a multivalent metal halide in both its higher and lower valance state. In accordance with a preferred embodiment, the contacting is effected in the presence of an oxygen containing gas or the melt is previously contacted with an oxygen containing gas to produce the corresponding oxyhalide of the metal, whereby the reaction may be effected on a continuous basis.
摘要翻译：通过使烷烃与烯烃，烯烃，脂肪族羧酸或芳香族烃的接触和含有多价金属卤化物的熔体在其较高和较低价态下进行偶合来进行。根据优选实施方案，接触在含氧气体的存在下进行，或者熔体预先与含氧气体接触以产生相应的金属卤氧化物，由此可以连续进行反应。

3. 发明授权

US4329525A Production of chlorinated compounds by use of molten salts 失效
标题翻译：使用熔盐生产氯化合物
公开(公告)号：US4329525A
公开(公告)日：1982-05-11
申请号：US879802
申请日：1978-02-21
申请人： Herbert Riegel , Vincent Strangio , Morgan C. Sze
发明人： Herbert Riegel , Vincent Strangio , Morgan C. Sze
IPC分类号： C07C17/15 , C01B7/01 , C01B7/04 , C01B9/02 , C07C17/00 , C07C67/00
CPC分类号： C07C17/00 , C01B7/04 , Y02P20/22
摘要： A compound is chlorinated with chlorine to produce chlorinated product and hydrogen chloride byproduct. Recovered hydrogen chloride byproduct is contacted with oxygen and a molten salt mixture containing the higher and lower valent chlorides of a multivalent metal, such as cuprous and cupric chloride, to effect recovery of the hydrogen chloride by enriching the molten salt content of the higher valent chloride. The molten salt, enriched in higher valent chloride, is then dechlorinated by use of a stripping gas, preferably hydrogen chloride, to produce a gaseous effluent containing stripped chlorine and the stripping gas, which is then recycled to the chlorination step. The presence of stripping gas, as a diluent, improves the chlorination operation.
摘要翻译：化合物用氯氯化，产生氯化产物和氯化氢副产物。将回收的氯化氢副产物与氧和含有多价金属如亚铜和氯化铜的较高和较低价的氯化物的熔融盐混合物接触，以通过富集高级氯化物的熔融盐含量来回收氯化氢。富含高级氯化物的熔融盐然后通过使用汽提气体，优选氯化氢进行脱氯，以产生含有汽提氯气和汽提气体的气态流出物，然后再循环至氯化步骤。作为稀释剂，汽提气体的存在改善了氯化操作。

4. 发明授权

US4207268A Oxychlorination of methane 失效
标题翻译：甲烷的氧氯化
公开(公告)号：US4207268A
公开(公告)日：1980-06-10
申请号：US891411
申请日：1978-03-30
申请人： Morgan C. Sze , Herbert Riegel , Harvey D. Schindler
发明人： Morgan C. Sze , Herbert Riegel , Harvey D. Schindler
IPC分类号： C07C17/154 , C07C17/00
CPC分类号： C07C17/154
摘要： Methane is oxychlorinated to one or more chlorinated methanes, without net production of carbon tetrachloride, by contacting methane and chlorine and/or hydrogen chloride with a molten mixture of cuprous chloride, cupric chloride, and copper oxychloride, in the presence of an amount of carbon tetrachloride which inhibits net production thereof.
摘要翻译：通过在一定量的碳存在下，将甲烷和氯和/或氯化氢与氯化亚铜，氯化铜和氯氧化铜的熔融混合物接触，将甲烷氧氯化成一种或多种氯化甲烷，而不产生四氯化碳。四氯化碳抑制其净产量。

5. 发明授权

US3965202A Production of trichloro-ethylene from waste C.sub.2 chlorinated hydrocarbons 失效
标题翻译：从废弃物C（HD 2 {B氯化碳氢化合物）生产三氯乙烯
公开(公告)号：US3965202A
公开(公告)日：1976-06-22
申请号：US371613
申请日：1973-06-20
申请人： Herbert Riegel , Morgan C. Sze , Harvey D. Schindler
发明人： Herbert Riegel , Morgan C. Sze , Harvey D. Schindler
IPC分类号： C07C17/08 , B01J27/00 , C07B61/00 , C07C17/00 , C07C17/10 , C07C17/15 , C07C17/156 , C07C17/158 , C07C17/25 , C07C19/01 , C07C21/067 , C07C21/10 , C07C21/12 , C07C67/00 , C07C21/04
CPC分类号： C07C21/12 , C07C17/158 , C07C21/10 , Y10S260/42
摘要： All or a portion of chlorinated hydrocarbons convertible to trichloroethylene and/or perchloroethylene by chlorination, dehydrochlorination or dehydrogenation and optionally also dechloroination are recovered from a C.sub.2 chlorinated hydrocarbon waste stream and contacted with a molten mixture of, for example, cuprous chloride, cupric chloride and copper oxychloride and hydrogen chloride and/or chlorine, to produce an effluent which contains as reaction product trichloroethylene and/or perchloroethylene. Chlorinated components in the waste stream not contacted with the molten mixture can be burned and the chlorine values used to enrich the chlorine content of the melt.
摘要翻译：通过氯化，脱氯化氢或脱氢以及任选还有脱氯作用将氯代烃全部或部分氯化烃转化为三氯乙烯和/或全氯乙烯从C2氯化烃废物流中回收，并与例如氯化亚铜，氯化铜和氯氧化铜和氯化氢和/或氯，以产生作为反应产物三氯乙烯和/或全氯乙烯含有的流出物。未与熔融混合物接触的废物流中的氯化组分可被燃烧，并且氯值用于富集熔体的氯含量。

6. 发明授权

US3947489A Coupling process 失效
标题翻译：耦合过程
公开(公告)号：US3947489A
公开(公告)日：1976-03-30
申请号：US769791
申请日：1968-10-23
申请人： Maurice E. Brooks , Herbert Riegel , Harvey D. Schindler , Morgan C. Sze
发明人： Maurice E. Brooks , Herbert Riegel , Harvey D. Schindler , Morgan C. Sze
IPC分类号： C07C1/00 , C07C2/66 , C07C2/76 , C07C2/82 , C07C2/84 , C07C11/12 , C07C15/02 , C07C67/00 , C07C69/15
CPC分类号： C07C2/82 , C07C2/76 , C07C2/84 , C07C67/035 , C07C2527/10 , C07C2527/122
摘要： Process for coupling an alkane to either an alkane, alkene, aliphatic carboxylic acid, or aromatic hydrocarbon by effecting contacting thereof and a melt containing a multivalent metal halide in both its higher and lower valence state. In accordance with a preferred embodiment, the contacting is effected in the presence of an oxygen containing gas or the melt is previously contacted with an oxygen containing gas to produce the corresponding oxyhalide of the metal, whereby the reaction may be effected on a continuous basis.
摘要翻译：通过使烷烃与烯烃，烯烃，脂肪族羧酸或芳族烃的接触和含有多价金属卤化物的熔体在更高和更低价态下进行偶联来进行。根据优选实施方案，接触在含氧气体的存在下进行，或者熔体预先与含氧气体接触以产生相应的金属卤氧化物，由此可以连续进行反应。

7. 发明授权

US4107222A Oxychlorination of methane 失效
标题翻译：甲烷的氧氯化
公开(公告)号：US4107222A
公开(公告)日：1978-08-15
申请号：US631157
申请日：1975-11-11
申请人： Morgan C. Sze , Herbert Riegel , Harvey D. Schindler
发明人： Morgan C. Sze , Herbert Riegel , Harvey D. Schindler
IPC分类号： C07C17/15 , B01J27/00 , B01J27/10 , B01J35/10 , B01J35/12 , C07B61/00 , C07C17/00 , C07C17/154 , C07C67/00
CPC分类号： B01J35/12 , B01J27/10 , C07C17/154
摘要： Methane is oxychlorinated to one or more chlorinated methanes, without net production of carbon tetrachloride, by contacting methane and chlorine and/or hydrogen chloride with a molten mixture of cuprous chloride, cupric chloride, and copper oxychloride, in the presence of an amount of carbon tetrachloride which inhibits net production thereof.
摘要翻译：通过在一定量的碳存在下，将甲烷和氯和/或氯化氢与氯化亚铜，氯化铜和氯氧化铜的熔融混合物接触，将甲烷氧氯化成一种或多种氯化甲烷，而不产生四氯化碳。四氯化碳抑制其净产量。

8. 发明授权

US4547284A Coke production 失效
标题翻译：可口可乐生产
公开(公告)号：US4547284A
公开(公告)日：1985-10-15
申请号：US640228
申请日：1984-08-13
申请人： Morgan C. Sze , Thomas M. Bennett , Andre A. Simone , Dennis F. Ogren , Mikio Nakaniwa , Kenji Furukawa
发明人： Morgan C. Sze , Thomas M. Bennett , Andre A. Simone , Dennis F. Ogren , Mikio Nakaniwa , Kenji Furukawa
IPC分类号： C10B55/00 , C10G9/14
CPC分类号： C10B55/00
摘要： In the delayed coking of a coking feedstock wherein the feedstock is continuously heated in a coking heater and introduced into a coke drum, the heater is operated to provide a coke drum temperature of from 415.degree. to 455.degree. C., and, after filling of the drum to the desired level, feedstock introduction is discontinued and the coke drum contents are heated at a temperature of 450.degree. C. to 500.degree. C., and which heating temperature is at least 10.degree. C. greater than the coking temperature, by passing a non-coking vapor through the contents of the drum to reduce the volatile combustible matter content to a value of 4% to 10% by weight and thereby reduce the CTE of the formed coke. The process is applicable to the production of needle coke from various kinds of feedstocks, in particular from a petroleum feedstock wherein the feedstock is initially treated by thermal soaking in the presence of sulfur, followed by thermal cracking to increase the aromaticity. Noncrystalline substances may be removed prior to coking to further improve the process.
摘要翻译：在焦化原料的延迟焦化中，其中原料在焦化加热器中连续加热并引入焦炭鼓中，操作加热器以提供415℃至455℃的焦炭鼓温度，并且在填充将鼓转到所需水平，原料引入停止，并将焦碳鼓内容物在450℃至500℃的温度下加热，并且该加热温度比焦化温度高至少10℃，由使非焦化蒸气通过鼓的内容物，以将易挥发的可燃物含量减少到4重量％至10重量％，从而降低形成的焦炭的CTE。该方法适用于从各种原料，特别是石油原料生产针状焦，其中原料最初通过在硫的存在下进行热浸，然后进行热裂解以增加芳香性。在结焦之前可以除去非结晶物质以进一步改善该方法。

9. 发明授权

US4208191A Production of pipeline gas from coal 失效
标题翻译：从煤炭生产管道煤气
公开(公告)号：US4208191A
公开(公告)日：1980-06-17
申请号：US910823
申请日：1978-05-30
申请人： Morgan C. Sze
发明人： Morgan C. Sze
IPC分类号： C10J3/00 , C10L3/08
CPC分类号： C10J3/00 , C10L3/08 , C10J2300/093 , C10J2300/1662
摘要： Acid gases are removed from a coal gasification gas, followed by contacting the gas with a reduced iron catalyst at conditions selected to primarily produce methane, and some olefins together with carbon dioxide as byproduct. After separation of carbon dioxide byproduct, the gas is contacted with a nickel catalyst under methanation conditions to produce additional methane and convert olefins to alkanes to thereby produce a pipeline gas having an increased heating value.
摘要翻译：从煤气化气体中除去酸性气体，然后在选择主要产生甲烷的条件下将气体与还原铁催化剂接触，一些烯烃和二氧化碳作为副产物。在分离二氧化碳副产物之后，气体在甲烷化条件下与镍催化剂接触以产生额外的甲烷并将烯烃转化为烷烃，从而产生具有增加的热值的管线气体。

10. 发明授权

US4092271A Supported vanadia catalyst for nitrile production and process for preparing the catalyst 失效
标题翻译：用于腈生产的支持的钒氧化物催化剂和用于制备催化剂的方法
公开(公告)号：US4092271A
公开(公告)日：1978-05-30
申请号：US819771
申请日：1977-07-28
申请人： Morgan C. Sze
发明人： Morgan C. Sze
IPC分类号： B01J23/22 , C07D213/84 , B01J21/04 , B01J21/08 , B01J23/04
CPC分类号： C07D213/84 , B01J23/22 , C07C253/28
摘要： Vanadia supported on a silica-alumina or gamma-alumina support in an amount to provide a vanadia to support weight ratio ranging from about 0.3:1 to about 3:1 substantially entirely within the pores of the support, the vanadia having been placed in molten form substantially within the pores of a support having a surface area greater than about 50m.sup.2 gram, a porosity greater than about 0.4 cc/gram which further includes an alkali metal, with the vanadium metal to alkali metal mole ratio being from 2:1 to 30:1. At least a portion of the alkali metal is preferably in the form of alkali metal vanadate. The catalyst is used for the production of nitriles from a compound containing at least one alkyl group.
摘要翻译： Vanadia负载在二氧化硅 - 氧化铝或γ-氧化铝载体上，其用量基本上完全在载体的孔内提供氧化钒至约0.3:1至约3:1的载体重量比，将氧化钒置于熔融基本上在表面积大于约50m 2克，孔隙率大于约0.4cc /克的支撑体的孔内形成，其还包含碱金属，其中钒金属与碱金属的摩尔比为2:1至30 ：1。至少一部分碱金属优选为碱金属钒酸盐的形式。催化剂用于从含有至少一个烷基的化合物制备腈。

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