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1. 发明授权

US4045504A Coupling process 失效
标题翻译：耦合过程
公开(公告)号：US4045504A
公开(公告)日：1977-08-30
申请号：US671388
申请日：1976-03-29
申请人： Maurice E. Brooks , Herbert Riegel , Harvey D. Schindler , Morgan C. Sze
发明人： Maurice E. Brooks , Herbert Riegel , Harvey D. Schindler , Morgan C. Sze
IPC分类号： C07C2/76 , C07C2/82 , C07C3/52 , C07C15/10
CPC分类号： C07C2/82 , C07C2/76 , C07C67/035 , C07C2527/10 , C07C2527/122
摘要： Process for coupling an alkane to either an alkane, alkene, aliphatic carboxylic acid, or aromatic hydrocarbon by effecting contacting thereof and a melt containing a multivalent metal halide in both its higher and lower valance state. In accordance with a preferred embodiment, the contacting is effected in the presence of an oxygen containing gas or the melt is previously contacted with an oxygen containing gas to produce the corresponding oxyhalide of the metal, whereby the reaction may be effected on a continuous basis.
摘要翻译：通过使烷烃与烯烃，烯烃，脂肪族羧酸或芳香族烃的接触和含有多价金属卤化物的熔体在其较高和较低价态下进行偶合来进行。根据优选实施方案，接触在含氧气体的存在下进行，或者熔体预先与含氧气体接触以产生相应的金属卤氧化物，由此可以连续进行反应。

2. 发明授权

US4207268A Oxychlorination of methane 失效
标题翻译：甲烷的氧氯化
公开(公告)号：US4207268A
公开(公告)日：1980-06-10
申请号：US891411
申请日：1978-03-30
申请人： Morgan C. Sze , Herbert Riegel , Harvey D. Schindler
发明人： Morgan C. Sze , Herbert Riegel , Harvey D. Schindler
IPC分类号： C07C17/154 , C07C17/00
CPC分类号： C07C17/154
摘要： Methane is oxychlorinated to one or more chlorinated methanes, without net production of carbon tetrachloride, by contacting methane and chlorine and/or hydrogen chloride with a molten mixture of cuprous chloride, cupric chloride, and copper oxychloride, in the presence of an amount of carbon tetrachloride which inhibits net production thereof.
摘要翻译：通过在一定量的碳存在下，将甲烷和氯和/或氯化氢与氯化亚铜，氯化铜和氯氧化铜的熔融混合物接触，将甲烷氧氯化成一种或多种氯化甲烷，而不产生四氯化碳。四氯化碳抑制其净产量。

3. 发明授权

US3965202A Production of trichloro-ethylene from waste C.sub.2 chlorinated hydrocarbons 失效
标题翻译：从废弃物C（HD 2 {B氯化碳氢化合物）生产三氯乙烯
公开(公告)号：US3965202A
公开(公告)日：1976-06-22
申请号：US371613
申请日：1973-06-20
申请人： Herbert Riegel , Morgan C. Sze , Harvey D. Schindler
发明人： Herbert Riegel , Morgan C. Sze , Harvey D. Schindler
IPC分类号： C07C17/08 , B01J27/00 , C07B61/00 , C07C17/00 , C07C17/10 , C07C17/15 , C07C17/156 , C07C17/158 , C07C17/25 , C07C19/01 , C07C21/067 , C07C21/10 , C07C21/12 , C07C67/00 , C07C21/04
CPC分类号： C07C21/12 , C07C17/158 , C07C21/10 , Y10S260/42
摘要： All or a portion of chlorinated hydrocarbons convertible to trichloroethylene and/or perchloroethylene by chlorination, dehydrochlorination or dehydrogenation and optionally also dechloroination are recovered from a C.sub.2 chlorinated hydrocarbon waste stream and contacted with a molten mixture of, for example, cuprous chloride, cupric chloride and copper oxychloride and hydrogen chloride and/or chlorine, to produce an effluent which contains as reaction product trichloroethylene and/or perchloroethylene. Chlorinated components in the waste stream not contacted with the molten mixture can be burned and the chlorine values used to enrich the chlorine content of the melt.
摘要翻译：通过氯化，脱氯化氢或脱氢以及任选还有脱氯作用将氯代烃全部或部分氯化烃转化为三氯乙烯和/或全氯乙烯从C2氯化烃废物流中回收，并与例如氯化亚铜，氯化铜和氯氧化铜和氯化氢和/或氯，以产生作为反应产物三氯乙烯和/或全氯乙烯含有的流出物。未与熔融混合物接触的废物流中的氯化组分可被燃烧，并且氯值用于富集熔体的氯含量。

4. 发明授权

US3947489A Coupling process 失效
标题翻译：耦合过程
公开(公告)号：US3947489A
公开(公告)日：1976-03-30
申请号：US769791
申请日：1968-10-23
申请人： Maurice E. Brooks , Herbert Riegel , Harvey D. Schindler , Morgan C. Sze
发明人： Maurice E. Brooks , Herbert Riegel , Harvey D. Schindler , Morgan C. Sze
IPC分类号： C07C1/00 , C07C2/66 , C07C2/76 , C07C2/82 , C07C2/84 , C07C11/12 , C07C15/02 , C07C67/00 , C07C69/15
CPC分类号： C07C2/82 , C07C2/76 , C07C2/84 , C07C67/035 , C07C2527/10 , C07C2527/122
摘要： Process for coupling an alkane to either an alkane, alkene, aliphatic carboxylic acid, or aromatic hydrocarbon by effecting contacting thereof and a melt containing a multivalent metal halide in both its higher and lower valence state. In accordance with a preferred embodiment, the contacting is effected in the presence of an oxygen containing gas or the melt is previously contacted with an oxygen containing gas to produce the corresponding oxyhalide of the metal, whereby the reaction may be effected on a continuous basis.
摘要翻译：通过使烷烃与烯烃，烯烃，脂肪族羧酸或芳族烃的接触和含有多价金属卤化物的熔体在更高和更低价态下进行偶联来进行。根据优选实施方案，接触在含氧气体的存在下进行，或者熔体预先与含氧气体接触以产生相应的金属卤氧化物，由此可以连续进行反应。

5. 发明授权

US4107222A Oxychlorination of methane 失效
标题翻译：甲烷的氧氯化
公开(公告)号：US4107222A
公开(公告)日：1978-08-15
申请号：US631157
申请日：1975-11-11
申请人： Morgan C. Sze , Herbert Riegel , Harvey D. Schindler
发明人： Morgan C. Sze , Herbert Riegel , Harvey D. Schindler
IPC分类号： C07C17/15 , B01J27/00 , B01J27/10 , B01J35/10 , B01J35/12 , C07B61/00 , C07C17/00 , C07C17/154 , C07C67/00
CPC分类号： B01J35/12 , B01J27/10 , C07C17/154
摘要： Methane is oxychlorinated to one or more chlorinated methanes, without net production of carbon tetrachloride, by contacting methane and chlorine and/or hydrogen chloride with a molten mixture of cuprous chloride, cupric chloride, and copper oxychloride, in the presence of an amount of carbon tetrachloride which inhibits net production thereof.
摘要翻译：通过在一定量的碳存在下，将甲烷和氯和/或氯化氢与氯化亚铜，氯化铜和氯氧化铜的熔融混合物接触，将甲烷氧氯化成一种或多种氯化甲烷，而不产生四氯化碳。四氯化碳抑制其净产量。

6. 发明授权

US4227995A Demetallization of hydrocarbon feedstock 失效
标题翻译：烃原料脱金属
公开(公告)号：US4227995A
公开(公告)日：1980-10-14
申请号：US966901
申请日：1978-12-06
申请人： Morgan C. Sze , Harvey D. Schindler
发明人： Morgan C. Sze , Harvey D. Schindler
IPC分类号： C10G25/00 , B01J35/10 , C10G45/02 , C10G49/00 , C10G23/00
CPC分类号： B01J35/108 , B01J35/1009 , C10G2300/107
摘要： A metal containing hydrocarbon feedstock, such as a heavy residue, is contacted with hydrogen and a material characterized by low porosity, less than 0.3 cc/gram; low surface area, less than 5 m.sup.2 /g; high average pore diameter, greater than 1,000 Angstroms; and a high distribution of large pores, at least 40%, and preferably 50 to 80% of pores greater than 10,000 Angstroms. A preferred material is coke.
摘要翻译：含有碳氢化合物原料（例如重残余物）的金属与氢气和特征为低孔隙率小于0.3cc / g的材料接触; 低表面积，小于5m2 / g; 高平均孔径，大于1000埃; 以及大孔的高分布，至少40％，优选50-80％的孔大于10,000埃。优选的材料是焦炭。

7. 发明授权

US4439313A Removal of arsenic impurity from hydrocarbons 失效
标题翻译：从碳氢化合物中去除砷杂质
公开(公告)号：US4439313A
公开(公告)日：1984-03-27
申请号：US332662
申请日：1981-12-21
申请人： Harvey D. Schindler , Morgan C. Sze
发明人： Harvey D. Schindler , Morgan C. Sze
IPC分类号： C10G25/00 , C01G28/00 , C01G28/02 , C10L9/02
CPC分类号： C10G25/003
摘要： Arsenic is removed from a hydrocarbon containing arsenic as an impurity; e.g., shale oil, by contact with hydrogen in the presence of a contact material, such as coke, to deposit the arsenic on the contact material. The arsenic deposited on the contact material is subsequently reacted with an iron compound to produce an iron-arsenic compound suitable for disposal.
摘要翻译：将砷作为杂质从含有砷的烃中除去; 例如页岩油，通过在诸如焦炭的接触材料的存在下与氢接触，以将砷沉积在接触材料上。随后将沉积在接触材料上的砷与铁化合物反应以产生适于处置的铁砷化合物。

8. 发明授权

US4059503A Stripping ammonia from liquid effluent of a hydrodenitrification process 失效
标题翻译：从加氢脱氮过程的液体流出物中除去氨
公开(公告)号：US4059503A
公开(公告)日：1977-11-22
申请号：US712088
申请日：1976-08-05
申请人： Morgan C. Sze , Harvey D. Schindler , Anthony Fanelli
发明人： Morgan C. Sze , Harvey D. Schindler , Anthony Fanelli
IPC分类号： C10L9/04 , C10G1/00 , C10G65/04 , C10G23/02
CPC分类号： C10G65/04
摘要： A nitrogen containing feedstock is hydrodenitrified by passing the feed through at least two hydrodenitrification zones, with ammonia produced in the hydrodenitrification being purged from the system prior to the last hydrodenitrification zone to maintain a low ammonia partial pressure in the last hydrodenitrification zone. The ammonia is preferably purged by stripping ammonia from the liquid portion of the effluent withdrawn from the next to last hydrodenitrification zone. Improved denitrification is obtained by maintaining a low ammonia partial pressure in the last hydrodenitrification zone.
摘要翻译：通过使进料通过至少两个加氢脱氮区，含氮原料被加氢脱硝，在最后一个加氢脱氮区之前，在加氢脱氮中产生的氨被从系统中清除，以在最后的加氢脱氮区保持低的氨分压。优选通过从从下一个最后一个加氢脱氮区抽出的废液的液体部分中汽提氨来净化氨。通过在最后一个加氢脱氮区保持低的氨分压来获得改进的反硝化作用。

9. 发明授权

US4316792A Hydroliquefaction of coal 失效
标题翻译：煤的水化
公开(公告)号：US4316792A
公开(公告)日：1982-02-23
申请号：US106275
申请日：1979-12-21
申请人： Morgan C. Sze , Harvey D. Schindler
发明人： Morgan C. Sze , Harvey D. Schindler
IPC分类号： C10G1/00 , C10G1/08 , C10G1/06 , B01J8/18 , C10B57/02 , C10G51/06
CPC分类号： C10G1/083
摘要： Coal is catalytically hydroliquefied by passing coal dispersed in a liquefaction solvent and hydrogen upwardly through a plurality of parallel expanded catalyst beds, in a single reactor, in separate streams, each having a cross-sectional flow area of no greater than 255 inches square, with each of the streams through each of the catalyst beds having a length and a liquid and gas superficial velocity to maintain an expanded catalyst bed and provide a Peclet Number of at least 3. If recycle is employed, the ratio of recycle to total feed (coal and liquefaction solvent) is no greater than 2:1, based on volume. Such conditions provide for improved selectivity to liquid product to thereby reduce hydrogen consumption. The plurality of beds are formed by partitions in the reactor.
摘要翻译：通过在单独的反应器中将分散在液化溶剂中的煤和氢向上通过多个平行的膨胀催化剂床，在分开的流中将煤分解成氢气，每个流具有不大于255英寸平方的横截面流动面积，通过每个催化剂床的每个流具有长度和液体和气体空塔速度，以保持膨胀的催化剂床，并提供至少为3的佩佩克数。如果使用再循环，则循环与总进料的比例（煤和液化溶剂）基于体积不大于2:1。这样的条件提供了对液体产物的改进的选择性，从而降低了氢消耗。多个床由反应器中的隔板形成。

10. 发明授权

US4329525A Production of chlorinated compounds by use of molten salts 失效
标题翻译：使用熔盐生产氯化合物
公开(公告)号：US4329525A
公开(公告)日：1982-05-11
申请号：US879802
申请日：1978-02-21
申请人： Herbert Riegel , Vincent Strangio , Morgan C. Sze
发明人： Herbert Riegel , Vincent Strangio , Morgan C. Sze
IPC分类号： C07C17/15 , C01B7/01 , C01B7/04 , C01B9/02 , C07C17/00 , C07C67/00
CPC分类号： C07C17/00 , C01B7/04 , Y02P20/22
摘要： A compound is chlorinated with chlorine to produce chlorinated product and hydrogen chloride byproduct. Recovered hydrogen chloride byproduct is contacted with oxygen and a molten salt mixture containing the higher and lower valent chlorides of a multivalent metal, such as cuprous and cupric chloride, to effect recovery of the hydrogen chloride by enriching the molten salt content of the higher valent chloride. The molten salt, enriched in higher valent chloride, is then dechlorinated by use of a stripping gas, preferably hydrogen chloride, to produce a gaseous effluent containing stripped chlorine and the stripping gas, which is then recycled to the chlorination step. The presence of stripping gas, as a diluent, improves the chlorination operation.
摘要翻译：化合物用氯氯化，产生氯化产物和氯化氢副产物。将回收的氯化氢副产物与氧和含有多价金属如亚铜和氯化铜的较高和较低价的氯化物的熔融盐混合物接触，以通过富集高级氯化物的熔融盐含量来回收氯化氢。富含高级氯化物的熔融盐然后通过使用汽提气体，优选氯化氢进行脱氯，以产生含有汽提氯气和汽提气体的气态流出物，然后再循环至氯化步骤。作为稀释剂，汽提气体的存在改善了氯化操作。

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