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1. 发明授权

US06464950B1 Method for separating and treating exhaust gas of carbon fiber 有权
标题翻译：碳纤维废气分离处理方法
公开(公告)号：US06464950B1
公开(公告)日：2002-10-15
申请号：US09466807
申请日：1999-12-20
申请人： Toshio Morita , Yutaka Suhara , Yoshihisa Sakamoto , Nobuhiro Matsumoto , Kunio Nishimura
发明人： Toshio Morita , Yutaka Suhara , Yoshihisa Sakamoto , Nobuhiro Matsumoto , Kunio Nishimura
IPC分类号： B01D5372
CPC分类号： B82Y30/00 , B01D53/72 , D01F9/127
摘要： A method for producing carbon fiber including the following processes: a process for obtaining fine carbon fiber by thermally decomposing an organic compound in a furnace by use of a catalyst; a process for separating a reaction exhaust gas contained in the carbon fiber; a process for continuously subjecting the carbon fiber to thermal treatment in a non-oxidative atmosphere; and a process for incinerating a thermal treatment exhaust gas generated in the thermal treatment and/or the reaction exhaust gas. The method for separating a reaction exhaust gas from carbon fiber is characterized in that a packed carbon fiber layer is formed, an inert gas is caused to flow through the layer, and the layer is compressed. Combustion of the reaction exhaust gas and combustion of the exhaust gas generated from the subsequent thermal treatment is achieved through employment of a pilot burner holding flame at all times in a vertical incinerator.
摘要翻译：一种生产碳纤维的方法，包括以下方法：通过使用催化剂在炉中热分解有机化合物获得细碳纤维的方法; 用于分离碳纤维中包含的反应废气的方法; 在非氧化性气氛中连续使碳纤维进行热处理的方法; 以及用于焚烧在热处理和/或反应废气中产生的热处理废气的方法。从碳纤维分离反应废气的方法的特征在于，形成填充碳纤维层，使惰性气体流过该层，并且层被压缩。反应废气的燃烧和随后的热处理产生的废气的燃烧是通过使用在垂直焚化炉中始终保持火焰的引燃燃烧器来实现的。

2. 发明申请

US20060257309A1 Carbon fiber, method for producing the same and apparatus therefor 审中-公开
标题翻译：碳纤维，其制造方法及其设备
公开(公告)号：US20060257309A1
公开(公告)日：2006-11-16
申请号：US11487459
申请日：2006-07-17
申请人： Toshio Morita , Yoshihisa Sakamoto , Yutaka Suhara , Kunio Nishimura
发明人： Toshio Morita , Yoshihisa Sakamoto , Yutaka Suhara , Kunio Nishimura
IPC分类号： D01F9/12
CPC分类号： D01D10/02 , D01F9/12
摘要： An object of the present invention is to provide a method and apparatus for heat-treating carbon fiber, in which impairment of a furnace caused by solidification of a transition metal impurity serving as a catalyst raw material is prevented, and the amount of the metal, such as Fe, Co, or Ni, contained in the carbon fiber is reduced. In the present invention, a vaporized metal impurity is contained in an inert gas that is passed through a furnace, and the gas is discharged from a high-temperature section of the furnace. The impurity contained in the gas discharged from the furnace is cooled to solidify, and then recovered. The resultant gas is recycled as an inert gas in the furnace.
摘要翻译：本发明的目的是提供一种用于热处理碳纤维的方法和装置，其中防止了由作为催化剂原料的过渡金属杂质的凝固导致的炉的损伤，并且金属的量，例如包含在碳纤维中的Fe，Co或Ni减少。在本发明中，在通过炉的惰性气体中含有汽化金属杂质，从炉的高温部排出气体。将从炉中排出的气体中所含的杂质冷却固化，然后回收。所得气体在炉中作为惰性气体再循环。

3. 发明授权

US06489025B2 Fine carbon fiber, method for producing the same and electrically conducting material comprising the fine carbon fiber 失效
标题翻译：细碳纤维，其制造方法和包含细碳纤维的导电材料
公开(公告)号：US06489025B2
公开(公告)日：2002-12-03
申请号：US09832792
申请日：2001-04-12
申请人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
发明人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
IPC分类号： D01F600
CPC分类号： B82Y30/00 , D01F9/127 , Y10T428/2913 , Y10T428/2918 , Y10T428/2924 , Y10T428/2929 , Y10T428/30
摘要： A fine carbon fiber having an outer diameter of about 1 to about 80 nm and an aspect ratio of 10 to 30,000, comprising a hollow center portion and a multi-layer sheath structure of a plurality of carbon layers, the layers forming annual rings, wherein the sheath-forming carbon layers form an incomplete sheath, i.e., the carbon layers are partially broken or disrupted in a longitudinal direction, and the outer diameter of the carbon fiber and/or the diameter of the hollow center portion are not uniform in a longitudinal direction. The carbon fiber is obtained by instantaneously reacting a carrier gas at a high temperature and an organic compound gas kept at a temperature below the decomposition temperature of the transition metal compound and has a conductivity equivalent to that of a conventional vapor phase method and is useful as a filler material in resins, rubbers, paints and the like.
摘要翻译：外径约1〜约80nm，纵横比为10〜30,000的细碳纤维，其包含多个碳层的中空中心部分和多层护套结构，所述层形成年轮环，其中，鞘形成碳层形成不完整的护套，即碳层在纵向上部分断裂或破裂，并且碳纤维的外径和/或中空中心部分的直径在纵向上不均匀方向。碳纤维通过使高温下的载气和保持在低于过渡金属化合物的分解温度的温度的有机化合物气体瞬时反应而获得，并且具有与常规气相法相当的导电性，可用作树脂，橡胶，油漆等中的填充材料。

4. 发明申请

US20080226537A1 Fine carbon fiber, method for producing the same and electrically conducting material comprising the fine carbon fiber 审中-公开
标题翻译：细碳纤维，其制造方法和包含细碳纤维的导电材料
公开(公告)号：US20080226537A1
公开(公告)日：2008-09-18
申请号：US12153131
申请日：2008-05-14
申请人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
发明人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , D01F9/127 , Y10T428/2913 , Y10T428/2918 , Y10T428/2924 , Y10T428/2929 , Y10T428/30
摘要： A fine carbon fiber having an outer diameter of about 1 to about 80 nm and an aspect ratio of 10 to 30,000, comprising a hollow center portion and a multi-layer sheath structure of a plurality of carbon layers, the layers forming annual rings, wherein the sheath-forming carbon layers form an incomplete sheath, i.e., the carbon layers are partially broken or disrupted in a longitudinal direction, and the outer diameter of the carbon fiber and/or the diameter of the hollow center portion are not uniform in a longitudinal direction. The carbon fiber is obtained by instantaneously reacting a carrier gas at a high temperature and an organic compound gas kept at a temperature below the decomposition temperature of the transition metal compound and has a conductivity equivalent to that of a conventional vapor phase method and is useful as a filler material in resins, rubbers, paints and the like.
摘要翻译：外径约1〜约80nm，纵横比为10〜30,000的细碳纤维，其包含多个碳层的中空中心部分和多层护套结构，所述层形成年轮，其中，鞘形成碳层形成不完整的护套，即碳层在纵向上部分断裂或破裂，并且碳纤维的外径和/或中空中心部分的直径在纵向上不均匀方向。碳纤维通过使高温下的载气和保持在低于过渡金属化合物的分解温度的温度的有机化合物气体瞬时反应而获得，并且具有与常规气相法相当的导电性，可用作树脂，橡胶，油漆等中的填充材料。

5. 发明申请

US20060083919A1 Fine carbon fiber, method for producing the same and electrically conducting material comprising the fine carbon fiber 审中-公开
公开(公告)号：US20060083919A1
公开(公告)日：2006-04-20
申请号：US11289324
申请日：2005-11-30
申请人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
发明人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
IPC分类号： D02G3/00
CPC分类号： B82Y30/00 , D01F9/127 , Y10T428/2913 , Y10T428/2918 , Y10T428/2924 , Y10T428/2929 , Y10T428/30
摘要： A fine carbon fiber having an outer diameter of about 1 to about 80 nm and an aspect ratio of 10 to 30,000, comprising a hollow center portion and a multi-layer sheath structure of a plurality of carbon layers, the layers forming annual rings, wherein the sheath-forming carbon layers form an incomplete sheath, i.e., the carbon layers are partially broken or disrupted in a longitudinal direction, and the outer diameter of the carbon fiber and/or the diameter of the hollow center portion are not uniform in a longitudinal direction. The carbon fiber is obtained by instantaneously reacting a carrier gas at a high temperature and an organic compound gas kept at a temperature below the decomposition temperature of the transition metal compound and has a conductivity equivalent to that of a conventional vapor phase method and is useful as a filler material in resins, rubbers, paints and the like.

6. 发明授权

US06699582B2 Fine carbon fiber, method for producing the same and electrically conducting material comprising the fine carbon fiber 有权
标题翻译：细碳纤维，其制造方法和包含细碳纤维的导电材料
公开(公告)号：US06699582B2
公开(公告)日：2004-03-02
申请号：US10254674
申请日：2002-09-26
申请人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
发明人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
IPC分类号： D01F600
CPC分类号： B82Y30/00 , D01F9/127 , Y10T428/2913 , Y10T428/2918 , Y10T428/2924 , Y10T428/2929 , Y10T428/30
摘要： A fine carbon fiber having an outer diameter of about 1 to about 80 nm and an aspect ratio of 10 to 30,000, comprising a hollow center portion and a multi-layer sheath structure of a plurality of carbon layers, the layers forming annual rings, wherein the sheath-forming carbon layers form an incomplete sheath, i.e., the carbon layers are partially broken or disrupted in a longitudinal direction, and the outer diameter of the carbon fiber and/or the diameter of the hollow center portion are not uniform in a longitudinal direction. The carbon fiber is obtained by instantaneously reacting a carrier gas at a high temperature and an organic compound gas kept at a temperature below the decomposition temperature of the transition metal compound and has a conductivity equivalent to that of a conventional vapor phase method and is useful as a filler material in resins, rubbers, paints and the like.
摘要翻译：外径约1〜约80nm，纵横比为10〜30,000的细碳纤维，其包含多个碳层的中空中心部分和多层护套结构，所述层形成年轮，其中，鞘形成碳层形成不完整的护套，即碳层在纵向上部分断裂或破裂，并且碳纤维的外径和/或中空中心部分的直径在纵向上不均匀方向。碳纤维通过使高温下的载气和保持在低于过渡金属化合物的分解温度的温度的有机化合物气体瞬时反应而获得，并且具有与常规气相法相当的导电性，可用作树脂，橡胶，油漆等中的填充材料。

7. 发明授权

US06998176B2 Fine carbon fiber, method for producing the same and electrically conducting material comprising the fine carbon fiber 有权
公开(公告)号：US06998176B2
公开(公告)日：2006-02-14
申请号：US10699645
申请日：2003-11-04
申请人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
发明人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , D01F9/127 , Y10T428/2913 , Y10T428/2918 , Y10T428/2924 , Y10T428/2929 , Y10T428/30
摘要： A fine carbon fiber having an outer diameter of about 1 to about 80 nm and an aspect ratio of 10 to 30,000, comprising a hollow center portion and a multi-layer sheath structure of a plurality of carbon layers, the layers forming annual rings, wherein the sheath-forming carbon layers form an incomplete sheath, i.e., the carbon layers are partially broken or disrupted in a longitudinal direction, and the outer diameter of the carbon fiber and/or the diameter of the hollow center portion are not uniform in a longitudinal direction. The carbon fiber is obtained by instantaneously reacting a carrier gas at a high temperature and an organic compound gas kept at a temperature below the decomposition temperature of the transition metal compound and has a conductivity equivalent to that of a conventional vapor phase method and is useful as a filler material in resins, rubbers, paints and the like.

8. 发明授权

US06565971B2 Fine carbon fiber and method for producing the same 有权
公开(公告)号：US06565971B2
公开(公告)日：2003-05-20
申请号：US09986438
申请日：2001-11-08
申请人： Toshio Morita , Hitoshi Inoue , Yutaka Suhara
发明人： Toshio Morita , Hitoshi Inoue , Yutaka Suhara
IPC分类号： D01F912
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/34 , C01B2202/36 , D01F9/127 , Y10T428/2419 , Y10T428/24777 , Y10T428/249924 , Y10T428/249927 , Y10T428/249933 , Y10T428/24994 , Y10T428/2916 , Y10T428/2918
摘要： A fine carbon fiber having a multilayer structure having stacked cylindrical carbon sheets and a center axis having a hollow structure. The fine carbon fiber has an outer diameter of 2 to 300 nm and an aspect ratio of 10 to 15,000, and at least one cylindrical carbon sheet layer among the multiple layers is folded at an end part of the carbon fiber and continued to another cylindrical carbon sheet. The folded and continued cylindrical carbon sheets form a cylindrical structure opened at the end part.

9. 发明授权

US06998171B2 Fine carbon fiber and method for producing the same 有权
公开(公告)号：US06998171B2
公开(公告)日：2006-02-14
申请号：US10393983
申请日：2003-03-24
申请人： Toshio Morita , Hitoshi Inoue , Yutaka Suhara
发明人： Toshio Morita , Hitoshi Inoue , Yutaka Suhara
IPC分类号： B32B27/04
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/34 , C01B2202/36 , D01F9/127 , Y10T428/2419 , Y10T428/24777 , Y10T428/249924 , Y10T428/249927 , Y10T428/249933 , Y10T428/24994 , Y10T428/2916 , Y10T428/2918
摘要： A fine carbon fiber having a multilayer structure having stacked cylindrical carbon sheets and a center axis having a hollow structure. The fine carbon fiber has an outer diameter of 2 to 300 nm and an aspect ratio of 10 to 15,000, and at least one cylindrical carbon sheet layer among the multiple layers is folded at an end part of the carbon fiber and continued to another cylindrical carbon sheet. The folded and continued cylindrical carbon sheets form a cylindrical structure opened at the end part.

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