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1. 发明授权

US07098177B1 Process for producing detergent particles 有权
标题翻译：生产洗涤剂颗粒的方法
公开(公告)号：US07098177B1
公开(公告)日：2006-08-29
申请号：US09581594
申请日：1999-10-14
申请人： Teruo Kubota , Hitoshi Takaya , Hiroyuki Yamashita
发明人： Teruo Kubota , Hitoshi Takaya , Hiroyuki Yamashita
IPC分类号： C11D11/00
CPC分类号： C11D17/06 , C11D11/0082 , C11D17/065
摘要： A process for preparing detergent particles containing step (I): mixing a base particle for supporting a surfactant ((a) component), and a surfactant composition ((b) component), under mixing conditions wherein the (a) component does not substantially undergo breakdown, to give a mixture; wherein the base particle is obtained by spray-drying an aqueous slurry, wherein the mixing operation is carried out by using a mixer containing agitation impellers, and where the mixer further contains disintegration impellers, the mixing operation step (I) is carried out without substantially rotating the disintegration impellers; and step (II): mixing the mixture obtained in step (I) with 5 to 100 parts by weight of fine powder, while substantially maintaining the shape of the (a) component containing (b) component, to give detergent particles, having a degree of particle growth of 1.3 or less, and a bulk density of 500 g/L or more.
摘要翻译：一种制备含有步骤（I）的洗涤剂颗粒的方法：在（a）成分基本上不含有（a）成分的混合条件下混合表面活性剂（（a）成分）和表面活性剂组合物（（b）成分）进行分解，给出混合物; 其特征在于，所述基础颗粒是通过喷雾干燥含水浆料而获得的，其中所述混合操作是通过使用含有搅拌叶轮的混合器进行的，并且其中所述混合器还包含崩解叶轮，所述混合操作步骤（I）旋转分解叶轮; 和步骤（II）：在基本保持含（b）成分的（a）成分的形状的同时，将步骤（I）中获得的混合物与5至100重量份的细粉末混合，得到具有粒子生长度为1.3以下，堆积密度为500g / L以上。

2. 发明授权

US06849590B1 Process for producing granules for supporting surfactant 失效
标题翻译：生产用于支撑表面活性剂的颗粒的方法
公开(公告)号：US06849590B1
公开(公告)日：2005-02-01
申请号：US09869359
申请日：1999-12-28
申请人： Hiroki Yamaboshi , Shuji Takana , Teruo Kubota , Hitoshi Takaya , Hiroyuki Yamashita , Hideichi Nitta
发明人： Hiroki Yamaboshi , Shuji Takana , Teruo Kubota , Hitoshi Takaya , Hiroyuki Yamashita , Hideichi Nitta
IPC分类号： B01J2/00 , C11D11/00 , C11D17/00 , C11D17/06
CPC分类号： B01J2/006 , C11D11/0082 , C11D17/0039 , C11D17/06
摘要： The present invention relates to a process for preparing particles for supporting a surfactant, comprising a step of giving a defect to a coating film containing a water-soluble component, wherein the coating film is formed on surfaces of raw material particles; and a process for preparing detergent particles comprising a step of mixing a surfactant composition and the particles for supporting a surfactant obtained by the above process, under conditions that the surfactant composition shows a liquid state. By using the process of the present invention, there can be obtained particles for supporting a surfactant, in which the supporting ability of the particles is improved, without lowering the detergency. In addition, by using the particles for supporting a surfactant, there can be obtained detergent particles having excellent detergency.
摘要翻译：本发明涉及一种制备用于支撑表面活性剂的颗粒的方法，包括对含有水溶性组分的涂膜产生缺陷的步骤，其中在原料颗粒的表面上形成涂膜; 以及制备洗涤剂颗粒的方法，包括在表面活性剂组合物显示液态的条件下，混合表面活性剂组合物和用于负载由上述方法得到的表面活性剂的颗粒的步骤。通过使用本发明的方法，可以获得支撑表面活性剂的颗粒，其中颗粒的支持能力得到改善，而不降低去污力。另外，通过使用支撑表面活性剂的粒子，可以得到洗涤性优异的洗涤剂粒子。

3. 发明授权

US06602846B1 Method for producing single nucleus detergent particles 失效
标题翻译：单核洗涤剂颗粒的生产方法
公开(公告)号：US06602846B1
公开(公告)日：2003-08-05
申请号：US09762934
申请日：2001-02-14
申请人： Teruo Kubota , Hitoshi Takaya , Motomitsu Hasumi , Hiroyuki Yamashita
发明人： Teruo Kubota , Hitoshi Takaya , Motomitsu Hasumi , Hiroyuki Yamashita
IPC分类号： C11D1100
CPC分类号： C11D17/065 , C11D11/0082
摘要： The present invention relates to a process for preparing uni-core detergent particles having a degree of particle growth of 1.5 or less and a bulk density of 500 g/L or more, comprising the steps of (A-I) mixing base particles for supporting a surfactant which have an average particle size of from 150 to 500 &mgr;m and a bulk density of 400 g/L or more [Component (a)] with a surfactant composition [Component (c)]; (A-II) mixing a mixture obtained in Step (A-I) with a powdery builder [Component (b)] of which primary average particle size is from 3 to 30 &mgr;m; and (A-III) mixing a mixture obtained in Step (A-II) with a fine powder [Component (d)] of which primary average particle size is smaller than that of Component (b). By using the process of the present invention, the uni-core detergent particles which are excellent in the dissolubility and the flowability properties can be prepared.
摘要翻译：本发明涉及一种制备颗粒生长度为1.5以下，体积密度为500g / L以上的单核洗涤剂粒子的方法，其特征在于，包括（A1）混合用于担载表面活性剂的基础粒子具有表面活性剂组合物[组分（c）]的平均粒度为150至500μm，堆积密度为400g / L或更高[组分（a）]]。（A-II）将步骤（A-I）中获得的混合物与一次平均粒径为3-30μm的粉末助洗剂[组分（b）]混合; 和（A-III）将步骤（A-II）中获得的混合物与一次平均粒径小于组分（b）的细粉末[组分（d）]混合。通过使用本发明的方法，可以制备溶解性和流动性优异的单核洗涤剂颗粒。

4. 发明授权

US06534474B1 Surfactant composition 有权
标题翻译：表面活性剂组成
公开(公告)号：US06534474B1
公开(公告)日：2003-03-18
申请号：US09701781
申请日：2000-12-04
申请人： Kyoko Okada , Teruo Kubota , Hitoshi Takaya , Shu Yamaguchi , Hiroyuki Yamashita
发明人： Kyoko Okada , Teruo Kubota , Hitoshi Takaya , Shu Yamaguchi , Hiroyuki Yamashita
IPC分类号： C11D183
CPC分类号： C11D17/06 , C11D1/83 , C11D3/3707 , C11D10/045
摘要： The surfactant composition of the present invention is a surfactant composition which is capable of being formulated for use in a non-liquid detergent composition, the surfactant composition comprising a) a nonionic surfactant having a melting point of 30° C. or less; b) an anionic surfactant having sulfonate group; and c) an immobilization agent for a) component, wherein b) component is formulated in an amount of from 0 to 300 parts by weight, based on 100 parts by weight of a) component, and wherein c) component is formulated in an amount of from 1 to 100 parts by weight, based on 100 parts by weight of a) component, and wherein the surfactant composition has (1) a temperature range that a viscosity of the composition is 10 Pa·s or less at a temperature equal to or higher than a pour point of the surfactant composition; and (2) a temperature range that a penetrating hardness of the composition is 100 g/cm2 or more in a temperature range between a temperature lower than the pour point of the surfactant composition and a temperature higher than the melting point of a) component.
摘要翻译：本发明的表面活性剂组合物是能够配制用于非液体洗涤剂组合物的表面活性剂组合物，所述表面活性剂组合物包含a）熔点为30℃以下的非离子表面活性剂; b）具有磺酸盐基团的阴离子表面活性剂; 和c）a）组分的固定剂，其中b）组分的配制量为0至300重量份，基于100重量份的a）组分，并且其中c）组分配制成一定量 1至100重量份，基于100重量份的a）组分，并且其中表面活性剂组合物具有（1）组合物的粘度在等于或等于10℃的温度下为10Pa·s以下的温度范围或高于表面活性剂组合物的倾点; 和（2）在比表面活性剂组合物的倾点低的温度和高于a）成分的熔点的温度的温度范围内组合物的穿透硬度为100g / cm 2以上的温度范围。

5. 发明授权

US06376453B1 Detergent particles 有权
标题翻译：洗涤剂颗粒
公开(公告)号：US06376453B1
公开(公告)日：2002-04-23
申请号：US09355032
申请日：1999-07-22
申请人： Teruo Kubota , Hitoshi Takaya , Shu Yamaguchi , Hiroyuki Yamashita , Shuji Takana
发明人： Teruo Kubota , Hitoshi Takaya , Shu Yamaguchi , Hiroyuki Yamashita , Shuji Takana
IPC分类号： C11D1700
CPC分类号： C11D11/02 , C11D3/0052 , C11D17/065
摘要： To provide detergent particles having high-speed dissolution capable of dissolving quickly in water after supplying the detergent particles in water, and a method for preparing the detergent particles, and a detergent composition comprising the detergent particles. Detergent particles having an average particle size of from 150 to 500 &mgr;m and a bulk density of 500 g/liter or more, wherein the detergent particles comprising a detergent particle being capable of releasing a bubble from an inner portion of the detergent particles in a process of dissolving the detergent particle in water, the bubble having a size of one-tenth or more of a particle size of the detergent particle, and wherein the detergent particles have a dissolution rate as calculated by Equation (1) of 90% or more, under conditions where the detergent particles are supplied in water at 5° C.; stirred for 60 seconds under the test stirring conditions; and filtered with a standard sieve having a sieve-opening of 74 &mgr;m as defined by JIS Z 8801, or wherein the detergent particles have a dissolution rate of 82% or more, the detergent particles stirred for 30 seconds and calculated in the same manner as above.
摘要翻译：提供具有高速溶解性能的洗涤剂颗粒，以及包含洗涤剂颗粒的洗涤剂组合物，其中洗涤剂颗粒在将洗涤剂颗粒供给到水中之后能迅速溶解在水中。平均粒度为150〜500μm，体积密度为500g / l以上的洗涤剂粒子，其中，含有洗涤剂粒子的洗涤剂粒子能够以洗涤剂粒子的内部从内部释放气泡将洗涤剂颗粒溶解在水中，气泡的尺寸为洗涤剂颗粒的粒径的十分之一以上，其中洗涤剂颗粒具有90％以上的等式（1）计算的溶解速率，在洗涤剂颗粒在5℃的水中供应的条件下进行。在试验搅拌条件下搅拌60秒; 用JIS Z 8801定义的筛孔为74μm的筛子进行过滤，或者其中洗涤剂颗粒的溶解率为82％以上，洗涤剂颗粒搅拌30秒，并以与以上。

6. 发明授权

US06864221B1 Granules for carrying surfactant and method for producing the same 失效
标题翻译：用于承载表面活性剂的颗粒及其制备方法
公开(公告)号：US06864221B1
公开(公告)日：2005-03-08
申请号：US09762948
申请日：2000-06-14
申请人： Shuji Takana , Hitoshi Takaya , Hiroki Yamaboshi , Yoichi Sugiyama , Hiroshi Kitagaito , Shu Yamaguchi , Hiroyuki Yamashita
发明人： Shuji Takana , Hitoshi Takaya , Hiroki Yamaboshi , Yoichi Sugiyama , Hiroshi Kitagaito , Shu Yamaguchi , Hiroyuki Yamashita
IPC分类号： C11D3/02 , C11D3/04 , C11D3/10 , C11D3/37 , C11D11/00 , C11D11/02 , C11D17/06
CPC分类号： C11D3/046 , C11D3/10 , C11D3/37 , C11D11/0082 , C11D11/02 , C11D17/065
摘要： The present invention relates to particles for supporting a surfactant and a process for preparing the same. Further, the present invention relates to high-density detergent particles using the particles for supporting a surfactant, and a process for preparing the same. According to the present invention, there can be obtained particles for supporting a surfactant which are excellent in the supporting ability (supporting capacity/supporting strength) for the liquid surfactant composition, and particles for supporting a surfactant which are excellent in the absorption properties (supporting rate) for the liquid surfactant composition, by spray-drying a preparation liquid obtainable by a process comprising the steps of preparing a first preparation liquid comprising a solution or slurry comprising a water-soluble polymer and a water-soluble salt; and subjecting the first preparation liquid to a treatment of increasing a number of water-soluble salt particles, thereby preparing a second preparation liquid having an increased number of water-soluble salt particles, as compared to the number of water-soluble salt particles which are present in the first preparation liquid. Further, since the liquid surfactant composition is supported by the particles for supporting a surfactant, detergent particles which are excellent in detergent performance, quality and the like can be efficiently obtained.
摘要翻译：本发明涉及用于支撑表面活性剂的颗粒及其制备方法。此外，本发明涉及使用用于支撑表面活性剂的颗粒的高密度洗涤剂颗粒及其制备方法。根据本发明，可以获得支撑液体表面活性剂组合物的支持能力（支撑能力/支撑强度）优异的表面活性剂用颗粒和吸收性优异的支撑表面活性剂的颗粒（支撑速率），通过喷雾干燥可通过包括以下步骤的方法获得的制备液：制备包含水溶性聚合物和水溶性盐的溶液或浆液的第一制备液; 并且对第一制备液进行处理以增加数量的水溶性盐颗粒，从而制备具有增加数量的水溶性盐颗粒的第二制备液，与水溶性盐颗粒的数量相比，存在于第一准备液中。此外，由于液体表面活性剂组合物被用于支撑表面活性剂的颗粒负载，所以可以有效地获得洗涤剂性能，质量等方面优异的洗涤剂颗粒。

7. 发明授权

US07067469B2 Solid-shaped detergent 失效
标题翻译：固体洗涤剂
公开(公告)号：US07067469B2
公开(公告)日：2006-06-27
申请号：US10661643
申请日：2003-09-15
申请人： Yuhki Yanagisawa , Nobuyoshi Yamaguchi , Shu Yamaguchi , Hitoshi Takaya , Hiroyuki Yamashita
发明人： Yuhki Yanagisawa , Nobuyoshi Yamaguchi , Shu Yamaguchi , Hitoshi Takaya , Hiroyuki Yamashita
IPC分类号： C11D17/00
CPC分类号： C11D3/0052 , C11D17/0047 , C11D17/065
摘要： A solid-shaped detergent comprising particles for detergent, wherein the particles have a dissolution rate of 90% or more, under conditions where the particles are supplied in water at 5° C.; stirred for 60 seconds under the stirring conditions that 1 g of the particles are supplied to a 1-L beaker having an inner diameter of 105 mm which is charged with 1 L of hard water having 71.2 mg CaCO3/L, wherein a molar ratio of Ca/Mg is 7/3, and stirred with a stirring bar of 35 mm in length and 8 mm in diameter at a rotational speed of 800 rpm; and filtered with a standard sieve having a sieve-opening of 74 μm as defined by JIS Z 8801, wherein the dissolution rate of the particles is calculated by the Equation (1): Dissolution Rate (%)=[1−(T/S)]×100, (1) wherein S is a weight (g) of the particles supplied; and T is a dry weight (g) of insoluble remnants of the particles remaining on the sieve when an aqueous solution prepared under the above stirring conditions is filtered with the sieve.
摘要翻译：一种固体形洗涤剂，其包含用于洗涤剂的颗粒，其中颗粒在5℃的水中供应的条件下，其溶解速率为90％以上。在搅拌条件下搅拌60秒，将1g的颗粒供给到内径为105mm的1L的烧杯中，该烧杯装入1L的具有71.2mg CaCO 3的硬水， / L，其中Ca / Mg的摩尔比为7/3，并以800rpm的转速与长35mm，直径8mm的搅拌棒一起搅拌; 并用JIS Z 8801定义的筛孔为74μm的筛孔进行过滤，其中通过式（1）计算出颗粒的溶解速度：<？in-line-formula description =“In-line 公式“end =”lead“？>溶解速率（％）= [1-（T / S）] x100，（1）<？在线公式描述=”在线公式“end =”tail“？ >其中S是所供应颗粒的重量（g）; 当用筛子过滤在上述搅拌条件下制备的水溶液时，T是残留在筛上的颗粒的不溶性残留物的干重（g）。

8. 发明授权

US06734156B1 Granules for carrying surfactant and method for producing the same 有权
标题翻译：用于承载表面活性剂的颗粒及其制备方法
公开(公告)号：US06734156B1
公开(公告)日：2004-05-11
申请号：US09762948
申请日：2001-02-14
申请人： Shuji Takana , Hitoshi Takaya , Hiroki Yamaboshi , Yoichi Sugiyama , Hiroshi Kitagaito , Shu Yamaguchi , Hiroyuki Yamashita
发明人： Shuji Takana , Hitoshi Takaya , Hiroki Yamaboshi , Yoichi Sugiyama , Hiroshi Kitagaito , Shu Yamaguchi , Hiroyuki Yamashita
IPC分类号： C11D1100
CPC分类号： C11D3/046 , C11D3/10 , C11D3/37 , C11D11/0082 , C11D11/02 , C11D17/065
摘要： The present invention relates to particles for supporting a surfactant and a process for preparing the same. Further, the present invention relates to high-density detergent particles using the particles for supporting a surfactant, and a process for preparing the same. According to the present invention, there can be obtained particles for supporting a surfactant which are excellent in the supporting ability (supporting capacity/supporting strength) for the liquid surfactant composition, and particles for supporting a surfactant which are excellent in the absorption properties (supporting rate) for the liquid surfactant composition, by spray-drying a preparation liquid obtainable by a process comprising the steps of preparing a first preparation liquid comprising a solution or slurry comprising a water-soluble polymer and a water-soluble salt; and subjecting the first preparation liquid to a treatment of increasing a number of water-soluble salt particles, thereby preparing a second preparation liquid having an increased number of water-soluble salt particles, as compared to the number of water-soluble salt particles which are present in the first preparation liquid. Further, since the liquid surfactant composition is supported by the particles for supporting a surfactant, detergent particles which are excellent in detergent performance, quality and the like can be efficiently obtained.
摘要翻译：本发明涉及用于支持表面活性剂的颗粒及其制备方法。此外，本发明涉及使用用于支撑表面活性剂的颗粒的高密度洗涤剂颗粒及其制备方法。根据本发明，可以获得支撑液体表面活性剂组合物的支持能力（支撑能力/支撑强度）优异的表面活性剂用颗粒和吸收性优异的支撑表面活性剂的颗粒（支撑速率），通过喷雾干燥可通过包括以下步骤的方法获得的制备液：制备包含水溶性聚合物和水溶性盐的溶液或浆液的第一制备液; 并且对第一制备液进行处理以增加数量的水溶性盐颗粒，从而制备具有增加数量的水溶性盐颗粒的第二制备液，与水溶性盐颗粒的数量相比，存在于第一准备液中。此外，由于液体表面活性剂组合物被用于支撑表面活性剂的颗粒负载，所以可以有效地获得洗涤剂性能，质量等方面优异的洗涤剂颗粒。

9. 发明授权

US06645931B1 Solid-shaped detergent 失效
标题翻译：固体洗涤剂
公开(公告)号：US06645931B1
公开(公告)日：2003-11-11
申请号：US09594025
申请日：2000-06-15
申请人： Yuhki Yanagisawa , Nobuyoshi Yamaguchi , Shu Yamaguchi , Hitoshi Takaya , Hiroyuki Yamashita
发明人： Yuhki Yanagisawa , Nobuyoshi Yamaguchi , Shu Yamaguchi , Hitoshi Takaya , Hiroyuki Yamashita
IPC分类号： C11D1700
CPC分类号： C11D3/0052 , C11D17/0047 , C11D17/065
摘要： A solid-shaped detergent comprising particles for detergent, wherein the particles have a dissolution rate of 90% or more, under conditions where the particles are supplied in water at 5° C.; stirred for 60 seconds under the stirring conditions that 1 g of the particles are supplied to a 1-L beaker having an inner diameter of 105 mm which is charged with 1 L of hard, water having 71.2 mg CaCO3/L, wherein a molar ratio of Ca/Mg is 7/3, and stirred with a stirring bar of 35 mm in length and 8 mm in diameter at a rotational speed of 800 rpm; and filtered with a standard sieve having a sieve-opening of 74 &mgr;m as defined by JIS Z 8801, wherein the dissolution rate of the particles is calculated by the Equation (1): Dissolution Rate (%)=[1−(T/S)]×100 (1), wherein S is a weight (g) of the particles supplied; and T is a dry weight (g) of insoluble remnants of the particles remaining on the sieve when an aqueous solution prepared under the above stirring conditions is filtered with the sieve.
摘要翻译：一种固体形洗涤剂，其包含用于洗涤剂的颗粒，其中颗粒在5℃的水中供应的条件下，其溶解速率为90％以上。在搅拌条件下搅拌60秒，将1g的颗粒供给到内径为105mm的1L的烧杯中，该烧杯装入1L的具有71.2mg CaCO 3 / L的硬水，其中摩尔比的Ca / Mg为7/3，并以800rpm的转速与长35mm，直径8mm的搅拌棒一起搅拌，用JIS Z 8801定义的筛孔为74μm的标准筛过滤，其中通过式（1）计算颗粒的溶解速率：溶解速率（％）= [1-（T / S ）]×100（1），其中S是供给的颗粒的重量（g）当用筛子过滤在上述搅拌条件下制备的水溶液时，T是残留在筛上的颗粒的不溶性残留物的干重（g）。

10. 发明申请

US20050256023A1 Detergent particles 有权
标题翻译：洗涤剂颗粒
公开(公告)号：US20050256023A1
公开(公告)日：2005-11-17
申请号：US10523606
申请日：2003-09-02
申请人： Yoshinobu Imaizumi , Hiroyuki Yamashita , Teruo Kubota
发明人： Yoshinobu Imaizumi , Hiroyuki Yamashita , Teruo Kubota
IPC分类号： C11D11/02 , C11D11/04 , C11D17/06 , C11D17/00
CPC分类号： C11D11/04 , C11D11/02 , C11D17/06
摘要： Detergent particles obtained by a process comprising the step of dryneutralizing base particles comprising a water-soluble solid alkali inorganic substance (A) with a liquid acid precursor (B) of a non-soap anionic surfactant, wherein the base particles are obtained by a spray-drying method, and wherein the base particles contain the component (A) in an amount of equal to or greater than 4 times the amount equivalent for neutralizing the component (B) and have an average particle size of from 150 to 400 μm; base particles having an average particle size of from 150 to 400 μm, comprising 20 to 80% by weight of a water-soluble solid alkali inorganic substance; a process for preparing detergent particles comprising the steps of (a) preparing a slurry comprising a water-soluble solid alkali inorganic substance (A) in an amount equal to or greater than 4 times the amount equivalent for neutralizing a liquid acid precursor (B) of a non-soap anionic surfactant to be added in step (c); (b) spray-drying the slurry obtained in step (a) to give base particles; and (c) mixing the liquid acid precursor (B) with the base particles obtained in step (b) and dry-neutralizing the resulting mixture; and a detergent composition comprising the detergent particles as defined above. The detergent particles can be used for laundry detergents, dishwashing detergents and the like.
摘要翻译：通过包括将包含水溶性固体碱性无机物质（A）的基础颗粒与非皂性阴离子表面活性剂的液体酸前体（B）中和的步骤获得的洗涤剂颗粒，其中所述基础颗粒通过喷雾并且其中所述基础颗粒含有等于或大于中和组分（B）的当量的4倍量的组分（A），并且平均粒度为150-400μm; 平均粒径为150〜400μm的碱性粒子，含有20〜80重量％的水溶性固体碱无机物质; 一种制备洗涤剂颗粒的方法，包括以下步骤：（a）制备含有等于或大于中和液体酸性前体（B）的当量的4倍量的水溶性固体碱性无机物质（A）的浆料，的步骤（c）中加入的非皂性阴离子表面活性剂; （b）喷雾干燥步骤（a）中获得的浆料，得到基础颗粒; 和（c）将液体酸前体（B）与步骤（b）中获得的基础颗粒混合并干燥中和所得混合物; 以及包含如上所述的洗涤剂颗粒的洗涤剂组合物。洗涤剂颗粒可用于衣物洗涤剂，餐具洗涤剂等。

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