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1. 发明申请

US20050287471A1 Novel fluorine-containing polymer having acid-reactive group and chemically amplifying type photoresist composition prepared from same 审中-公开
标题翻译：具有酸反应性基团的新型含氟聚合物和由其制备的化学放大型光致抗蚀剂组合物
公开(公告)号：US20050287471A1
公开(公告)日：2005-12-29
申请号：US11033954
申请日：2005-01-13
申请人： Takayuki Araki , Meiten Koh , Yoshito Tanaka , Takuji Ishikawa , Hirokazu Aoyama , Tetsuo Shimizu
发明人： Takayuki Araki , Meiten Koh , Yoshito Tanaka , Takuji Ishikawa , Hirokazu Aoyama , Tetsuo Shimizu
IPC分类号： G03F7/004 , G03F7/038 , G03F7/039 , G03F7/075 , G03C1/76
CPC分类号： G03F7/039 , G03F7/0045 , G03F7/0046 , G03F7/0382 , G03F7/0392 , G03F7/0395 , G03F7/0397 , G03F7/0758 , Y10S430/106 , Y10S430/108
摘要： There is provided a novel fluorine-containing polymer having an acid-reactive group which has a high transparency against energy rays (radioactive rays) in a vacuum ultraviolet region (157 nm), and further there are provided a material for fluorine-containing base polymer prepared from the polymer and suitable for a photoresist and a chemically amplifying type resist composition obtained therefrom. The polymer has a number average molecular weight of from 1,000 to 1,000,000 and represented by the formula: -(M1)-(M2)-(A)-, wherein M1 is a structural unit having an acid-labile or acid-degradable functional group, M2 is a structural unit of fluorine-containing acryl ester, A is a structural unit derived from other copolymerizable monomer, the percent by mole ratio M1/M2 is 1 to 99/99 to 1 and the polymer comprises from 1 to 99% by mole of the structural unit M1, from 1 to 99% by mole of the structural unit M2 and from 0 to 98% by mole of the structural unit A1. The material for fluorine-containing base polymer comprises a fluorine-containing polymer having an acid-reactive group such as the above-mentioned polymer and is suitable for a photoresist, and the chemically amplifying type resist composition is obtained from those polymer and material.
摘要翻译：提供了一种具有酸反应性基团的新型含氟聚合物，其具有对真空紫外区域（157nm）中的能量射线（放射线）的高透明性，并且还提供了含氟基础聚合物由聚合物制备并适用于由其获得的光致抗蚀剂和化学放大型抗蚀剂组合物。聚合物的数均分子量为1,000〜1,000,000，由下式表示： - （M1） - （M2） - （A） - ，其中M1是具有酸不稳定性或酸可降解官能团的结构单元 M2是含氟丙烯酸酯的结构单元，A是来自其它可共聚单体的结构单元，M1 / M2的摩尔比为1〜99/99〜1，聚合物的含量为1〜99％结构单元M1的摩尔数，结构单元M2的1〜99摩尔％和结构单元A1的0〜98摩尔％。含氟基础聚合物的材料包括具有酸反应性基团的含氟聚合物如上述聚合物，并且适用于光致抗蚀剂，化学放大型抗蚀剂组合物由那些聚合物和材料获得。

2. 发明授权

US06908724B2 Fluorine-containing polymer having acid-reactive group and chemically amplifying type photoresist composition prepared from same 有权
标题翻译：具有酸反应性基团的含氟聚合物和由其制备的化学放大型光致抗蚀剂组合物
公开(公告)号：US06908724B2
公开(公告)日：2005-06-21
申请号：US10262893
申请日：2002-10-03
申请人： Takayuki Araki , Meiten Koh , Yoshito Tanaka , Takuji Ishikawa , Hirokazu Aoyama , Tetsuo Shimizu
发明人： Takayuki Araki , Meiten Koh , Yoshito Tanaka , Takuji Ishikawa , Hirokazu Aoyama , Tetsuo Shimizu
IPC分类号： G03F7/004 , G03F7/038 , G03F7/039 , G03F7/075
CPC分类号： G03F7/039 , G03F7/0045 , G03F7/0046 , G03F7/0382 , G03F7/0392 , G03F7/0395 , G03F7/0397 , G03F7/0758 , Y10S430/106 , Y10S430/108
摘要： There is provided a novel fluorine-containing polymer having an acid-reactive group which has a high transparency against energy rays (radioactive rays) in a vacuum ultraviolet region (157 nm), and further there are provided a material for fluorine-containing base polymer prepared from the polymer and suitable for a photoresist and a chemically amplifying type resist composition obtained therefrom.The polymer has a number average molecular weight of from 1,000 to 1,000,000 and represented by the formula: —(M1)—(M2)—(A)—, wherein M1 is a structural unit having an acid-labile or acid-degradable functional group, M2 is a structural unit of fluorine-containing acryl ester, A is a structural unit derived from other copolymerizable monomer, the percent by mole ratio M1/M2 is 1 to 99/99 to 1 and the polymer comprises from 1 to 99% by mole of the structural unit M1, from 1 to 99% by mole of the structural unit M2 and from 0 to 98% by mole of the structural unit A1. The material for fluorine-containing base polymer comprises a fluorine-containing polymer having an acid-reactive group such as the above-mentioned polymer and is suitable for a photoresist, and the chemically amplifying type resist composition is obtained from those polymer and material.
摘要翻译：提供了一种具有酸反应性基团的新型含氟聚合物，其具有对真空紫外区域（157nm）中的能量射线（放射线）的高透明性，并且还提供了含氟基础聚合物由聚合物制备并适用于由其获得的光致抗蚀剂和化学放大型抗蚀剂组合物。聚合物的数均分子量为1,000〜1,000,000，由下式表示： - （M1） - （M2） - （A） - ，其中M1是具有酸不稳定性或酸可降解官能团的结构单元 M2是含氟丙烯酸酯的结构单元，A是来自其它可共聚单体的结构单元，M1 / M2的摩尔比为1〜99/99〜1，聚合物的含量为1〜99％结构单元M1的摩尔数，结构单元M2的1〜99摩尔％和结构单元A1的0〜98摩尔％。含氟基础聚合物的材料包括具有酸反应性基团的含氟聚合物如上述聚合物，并且适用于光致抗蚀剂，化学放大型抗蚀剂组合物由那些聚合物和材料获得。

3. 发明授权

US08466227B2 Crosslinked fluorine-containing elastomer fine particles, preparation process of same, and composition 有权
标题翻译：交联的含氟弹性体微粒，其制备方法和组成
公开(公告)号：US08466227B2
公开(公告)日：2013-06-18
申请号：US13289948
申请日：2011-11-04
申请人： Hideto Nakagawa , Haruhiko Mohri , Hirokazu Aoyama , Junpei Terada , Rumi Takeuchi
发明人： Hideto Nakagawa , Haruhiko Mohri , Hirokazu Aoyama , Junpei Terada , Rumi Takeuchi
IPC分类号： B32B5/16 , C08L27/10 , C08L27/12
CPC分类号： C08J3/12 , C08J3/24 , C08J2327/12 , C08L2205/02 , C08L2205/22 , Y10T428/2982 , C08L27/18 , C08L27/16
摘要： There are provided novel crosslinked fluorine-containing elastomer fine particles, a process for preparing crosslinked fluorine-containing elastomer fine particles and a resin composition comprising the same. The crosslinked fluorine-containing elastomer fine particles are crosslinked fluorine-containing elastomer fine particles having a gel fraction of not less than 85% by mass or crosslinked fluorine-containing elastomer fine particles obtained by crosslinking fluorine-containing elastomer particles having at least three iodine atoms per one polymer molecule at an end thereof. The composition is one comprising those fine particles and a synthetic resin. The preparation process is a process for preparing crosslinked fluorine-containing elastomer fine particles, characterized by subjecting peroxide-crosslinkable fluorine-containing elastomer particles to peroxide-crosslinking by heating an aqueous dispersion comprising the fluorine-containing elastomer particles, a peroxide and a polyfunctional unsaturated compound.
摘要翻译：提供了新型交联的含氟弹性体微粒，制备交联的含氟弹性体微粒的方法和包含其的树脂组合物。交联的含氟弹性体微粒是具有不小于85质量％的凝胶分数的交联的含氟弹性体微粒或通过交联含有至少三个碘原子的含氟弹性体颗粒获得的交联的含氟弹性体微粒每一个聚合物分子在其末端。该组合物是包含这些细颗粒和合成树脂的组合物。制备方法是制备交联的含氟弹性体微粒的方法，其特征在于通过加热含氟弹性体颗粒，过氧化物和多官能不饱和的含水弹性体颗粒，使过氧化物交联的含氟弹性体颗粒进行过氧化物交联复合。

4. 发明申请

US20100160503A1 SURFACE-MODIFIED NANOFILLER AND POLYMER COMPOSITE MATERIAL 有权
标题翻译：表面改性纳米复合材料和聚合物复合材料
公开(公告)号：US20100160503A1
公开(公告)日：2010-06-24
申请号：US11993446
申请日：2006-06-22
申请人： Hideto Nakagawa , Haruhiko Mohri , Hirokazu Aoyama
发明人： Hideto Nakagawa , Haruhiko Mohri , Hirokazu Aoyama
IPC分类号： C08K5/3445 , C08K5/02 , C08K5/56 , C08K5/053 , C08K5/50 , C07F5/06 , C07F9/02 , C07D233/64
CPC分类号： C08J5/005 , B82Y30/00 , C08K9/04
摘要： A polymer composite material provides superior heat resistance, mechanical physical properties, substance permeation barrier properties, flame retardant properties, electrical conductivity and the like. Moreover, a novel surface-modified nanofiller utilizes this type of polymer composite material. The polymer composite material contains nanofillers, fluorocompounds and polymers. Fluoruocompounds bond to the surface of the nanofillers. The nanofillers to which fluorocompounds are surface-bonded are mixed with or dispersed in polymers.
摘要翻译：聚合物复合材料提供优异的耐热性，机械物理性能，物质渗透阻挡性能，阻燃性能，导电性等。此外，新型表面改性纳米填料利用这种类型的聚合物复合材料。聚合物复合材料包含纳米填料，氟化合物和聚合物。氟化合物键合到纳米填料的表面。氟化合物表面结合的纳米填料与聚合物混合或分散在聚合物中。

5. 发明授权

US6060628A Manufacturing method for 1,1,1,3,3-pentafluoropropane 失效
标题翻译： 1,1,1,3,3-五氟丙烷的制备方法
公开(公告)号：US6060628A
公开(公告)日：2000-05-09
申请号：US894694
申请日：1997-08-26
申请人： Hirokazu Aoyama , Noriaki Shibata , Akinori Yamamoto
发明人： Hirokazu Aoyama , Noriaki Shibata , Akinori Yamamoto
IPC分类号： B01J23/44 , C07B61/00 , C07C17/23 , C07C17/38 , C07C19/08 , C07F15/00
CPC分类号： C07C19/08 , C07C17/23
摘要： A manufacturing method for 1,1,1,3,3-pentafluoropropane in which the method is composed of:step A wherein 2,3-dichloro-1,1,1,3,3-pentafluoropropane is reduced with hydrogen under the presence of hydrogenation catalyst in gaseous phase;step B wherein all of the products of the said step A are introduced into a cooler condenser, so that either a component of hydrogen and hydrogen chloride as non-condensation component and another compoment of 1,1,1,3,3-pentafluoropropane as condensation components or a component of hydrogen as non-condensation component and another component of hydrogen chloride and 1,1,1,3,3-pentafluoropropane as condensation component are obtained;step C wherein hydrogen is separated from the non-condensation component of the said step B, and it is recycled to the said step A; andstep D wherein 1,1,1,3,3-pentafluoropropane is separated from the condensation component of the said step B.The producing method based on a manufacturing process of 1,1,1,3,3-pentafluoropropane can be provided with good efficiency and economy in industrial scales.
摘要翻译： PCT No.PCT / JP96 / 00273 Sec。 371日期：1997年8月26日 102（e）日期1997年8月26日PCT提交1996年2月8日PCT公布。公开号WO96 / 26914 PCT 日期1996年6月9日1,1,1,3,3-五氟丙烷的制造方法，其中所述方法由以下组成：步骤A，其中2,3-二氯-1,1,1,3,3-五氟丙烷被还原在氢气催化剂存在下用氢气气相; 步骤B，其中将所述步骤A的所有产物引入冷却器冷凝器中，使得氢和氯化氢的组分作为非缩合成分，另一组分为1,1,1,3,3-五氟丙烷作为得到缩合成分或作为非缩合成分的氢的成分和作为缩合成分的氯化氢和1,1,1,3,3-五氟丙烷的其他成分; 步骤C，其中氢与所述步骤B的非缩合组分分离，并将其再循环至所述步骤A; 和步骤D，其中将1,1,1,3,3-五氟丙烷与所述步骤B的缩合组分分离。可以提供基于1,1,1,3,3-五氟丙烷的制备方法的制备方法工业规模效益好，经济效益好。

6. 发明授权

US5919993A Method for preparing halogenated butene and butane 失效
标题翻译：制备卤代丁烯和丁烷的方法
公开(公告)号：US5919993A
公开(公告)日：1999-07-06
申请号：US108576
申请日：1993-09-03
申请人： Tatsuo Nakada , Hirokazu Aoyama , Satoshi Koyama
发明人： Tatsuo Nakada , Hirokazu Aoyama , Satoshi Koyama
IPC分类号： B01J27/12 , C07B61/00 , C07C17/08 , C07C17/20 , C07C17/21 , C07C19/08 , C07C21/18
CPC分类号： C07C17/21
摘要： At least one halogenated compound selected from the group consisting of 1,1,1,4,4,4-hexafluoro-2,3-dichlorobutane, 1,1,1,4,4,4-hexafluoro-2-chloro-2-butene, 1,1,1,2,4,4,4-heptafluoro-2-butene and 1,1,1,2,2,4,4,4-octafluorobutane, is prepared by reacting 1,1,2,3,4,4-hexachloro-1,3-butadiene with hydrogen fluoride in a gas phase in the presence of a fluorinating catalyst. Desired products can be prepared commercially according to the present invention.
摘要翻译： PCT No.PCT / JP93 / 00027 Sec。 371日期1993年9月3日 102（e）1993年9月3日PCT 1993年1月12日PCT PCT。公开号WO93 / 14051 日期：1993年7月22日至少一种选自1,1,1,4,4,4-六氟-2,3-二氯丁烷，1,1,1,4,4,4-六氟-2- 2-氯-2-丁烯，1,1,1,2,4,4,4-七氟-2-丁烯和1,1,1,2,2,4,4,4-八氟丁烷是通过使 1,1,1,2,3,4,4-六氯-1,3-丁二烯与氟化氢在氟化催化剂存在下气相反应。期望的产品可以根据本发明在商业上制备。

7. 发明授权

US5659093A Method of producing 1,1,1,3,3-pentafluoropropane, a method of producing 1,1,1,3,3-pentafluoro-2-halogeno-3-chloropropane, and a method of producing 1,1,1,2,3,3-hexachloropropene 失效
标题翻译： 1,1,1,3,3-五氟丙烷的制造方法，1,1,1,3,3-五氟-2-卤代-3-氯丙烷的制造方法以及1,1,1,3,3-五氟丙烷的制造方法， 2,3,3-六氯丙烯
公开(公告)号：US5659093A
公开(公告)日：1997-08-19
申请号：US464834
申请日：1995-06-27
申请人： Seiji Takubo , Hirokazu Aoyama , Tatsuo Nakada
发明人： Seiji Takubo , Hirokazu Aoyama , Tatsuo Nakada
IPC分类号： C07C17/25 , B01J27/08 , C07B61/00 , C07C17/00 , C07C17/04 , C07C17/08 , C07C17/20 , C07C17/21 , C07C17/23 , C07C19/08 , C07C19/10 , C07C19/12 , C07C21/04
CPC分类号： C07C19/12 , B01J27/08 , C07C17/21 , C07C17/23 , C07C17/25 , C07C19/10
摘要： There are provided production methods of 1,1,1,3,3-pentafluoropropane characterized in that 1,1,1,3,3-pentafluoro-2,3-dichloropropane is reacted with hydrogen fluoride in the presence of a noble metal catalyst; of 1,1,1,3,3-pentafluoro-2-halogeno-3-chloropropane characterized in that the halogenated propene indicated as general formula I is fluorinated in the presence of antimony trihalogenide and/or antimony pentahalogenide by hydrogen fluoride of mole ratio of or over five times the said antimony halogenide in a liquid phase; and of 1,1,1,2,3,3-hexaohloropropene characterized in that 1,1,1,2,2,3,3-heptachloropropane is reacted with an aqueous solution of alkali metal hydroxide in the presence of a phase transfer catalyst. Therefore, an industrial manufacturing method which is possible to obtain the objective product easily at low cost and high yield can be provided.
摘要翻译： PCT No.PCT / JP93 / 01887 Sec。 371日期：1995年6月27日 102（e）日期1995年6月27日PCT 1993年12月24日PCT公布。公开号WO94 / 14736 日期：1994年7月7日提供1,1,1,3,3-五氟丙烷的制备方法，其特征在于1,1,1,3,3-五氟-2,3-二氯丙烷与氟化氢反应，的贵金属催化剂; 的1,1,1,3,3-五氟-2-卤代-3-氯丙烷，其特征在于通式I的卤代丙烯在三卤化锑和/或五卤代锑的存在下通过氟化氢的摩尔比氟化所述锑卤化物在液相中为或超过5倍; 和1,1,1,2,3,3-六氯丙烯，其特征在于1,1,1,2,2,3,3-七氯丙烷与碱金属氢氧化物的水溶液在相转移催化剂。因此，可以提供以低成本和高产率容易地获得目标产品的工业制造方法。

8. 发明授权

US5532418A Method of producing 1,1,1,2,3,3,-hexafluoropropane and tetrafluorochloropropene 失效
标题翻译：制备1,1,1,2,3,3 - 六氟丙烷和四氟氯丙烯的方法
公开(公告)号：US5532418A
公开(公告)日：1996-07-02
申请号：US392906
申请日：1995-03-01
申请人： Tatsuo Nakada , Hirokazu Aoyama
发明人： Tatsuo Nakada , Hirokazu Aoyama
IPC分类号： B01J23/26 , B01J23/86 , B01J27/125 , B01J27/132 , C07B61/00 , C07C17/00 , C07C17/20 , C07C17/21 , C07C17/23 , C07C19/08 , C07C21/18 , C09K3/00 , C10M105/52 , C10N40/08 , C11D7/30 , C07C17/08 , C07C17/25
CPC分类号： C07C19/08 , C07C17/00 , C07C17/21 , C07C17/23
摘要： A method of producing 1,1,1,2,3,3-hexafluoropropane in a characteristic process in which tetrafluorochloropropene is first obtained from the dechlorofluorination (removing ClF) of 1,1,1,2,2-pentafluoro-3,3-dichloropropane and/or 1,1,2,2,3-pentafluoro-1,3-dichloropropane by hydrogen in the presence of a metal oxide catalyst and then the product olefin is fluorinated in the presence of a catalyst. By this method, 1,1,1,2,3,3-hexafluoropropane, which is useful as an action fluid and so on and has a property to help preserving the environment, and an intermediate in its synthesis can be easily produced at low cost.
摘要翻译： PCT No.PCT / JP93 / 01117 Sec。 371 1995年3月1日 102（e）1995年3月1日PCT PCT 1993年8月9日PCT公布。 WO94 / 05611 PCT公开号日期：1994年3月17日。一种在特征方法中制备1,1,1,2,3,3-六氟丙烷的方法，其中首先从1,1,1,2的脱氟氟化（去除ClF）获得四氟氯丙烯， 2-五氟-3,3-二氯丙烷和/或1,1,2,2,3-五氟-1,3-二氯丙烷，在金属氧化物催化剂存在下，然后将产物烯烃在催化剂通过该方法，作为动作液等有用并具有助于保持环境的性质的1,1,1,2,3,3-六氟丙烷和其合成中的中间体可以容易地在低成本。

9. 发明授权

US5424002A Solvent composition comprising mixture of polyfluoroalkane and lower alcohol 失效
标题翻译：包含多氟烷烃和低级醇的混合物的溶剂组合物
公开(公告)号：US5424002A
公开(公告)日：1995-06-13
申请号：US199190
申请日：1994-02-28
申请人： Yukio Omure , Hirokazu Aoyama , Satoshi Ide , Takahiro Matsuda
发明人： Yukio Omure , Hirokazu Aoyama , Satoshi Ide , Takahiro Matsuda
IPC分类号： C11D7/26 , C11D7/28 , C11D7/50 , C23G5/028 , C11D7/30
CPC分类号： C11D7/261 , C11D7/5018 , C11D7/5081 , C23G5/02803 , C11D7/26 , C11D7/28
摘要： A solvent composition comprising a mixture of at least one polyfluoroalkane and at least one lower alcohol, wherein the polyfluoroalkane is selected among those represented by the general formula (1): (CF.sub.3).sub.2 CF--R wherein R represents a fluorinated ethyl group substituted by 1 to 4 fluorine atoms, and the lower alcohol is selected from the group consisting of methyl, ethyl, n-propyl and isopropyl alcohol.
摘要翻译： PCT No.PCT / JP92 / 01072 Sec。 371日期1994年2月28日 102（e）日期1994年2月28日PCT提交1992年8月26日PCT公布。出版物WO93 / 04160 日本1993年3月4日。一种包含至少一种多氟烷烃和至少一种低级醇的混合物的溶剂组合物，其中所述多氟烷烃选自由通式（1）表示的那些：（CF 3）2 CFF，其中R表示被1〜4个氟原子取代的氟代乙基，低级醇选自甲基，乙基，正丙基和异丙醇。

10. 发明授权

US08236887B2 Fluorine-containing polymer having heteroaromatic ring 有权
标题翻译：具有杂芳环的含氟聚合物
公开(公告)号：US08236887B2
公开(公告)日：2012-08-07
申请号：US12278613
申请日：2007-02-05
申请人： Yuzo Komatsu , Haruhiko Mohri , Hirokazu Aoyama
发明人： Yuzo Komatsu , Haruhiko Mohri , Hirokazu Aoyama
IPC分类号： C08K3/04
CPC分类号： H01G9/038 , C08F8/44 , C08F14/18 , C08F214/26 , C08F214/28 , C08F216/1408 , C08F2800/10 , C08F2810/40 , C08K3/04 , C08L27/12 , C08L2205/02 , H01G11/56 , H01M2/16 , H01M8/1023 , H01M8/1039 , H01M10/0565 , H01M10/0567 , H01M10/0568 , H01M2300/0045 , H01M2300/0082 , H01M2300/0085 , Y02E60/13 , C08L2666/04 , C08F120/06 , C08F112/14 , C08F8/30 , C08F14/22 , C08F114/185
摘要： There is provided a fluorine-containing polymer having an ionic group which has a heteroaromatic ring and is useful as a material comprising various heteroaromatic ring compounds having a stable fluorine-containing heteroaromatic ring, and further a fluorine-containing polymer having a heteroaromatic ring which is useful as a starting material of the above-mentioned polymer or a curing agent. Also, there is provided a fluorine-containing polymer having a heteroaromatic ring such as imidazole in its side chain, a polymer salt thereof, and a polymer composition comprising such a polymer and a polymer salt and a nano filler.
摘要翻译：提供具有离子性基团的含氟聚合物，其具有杂芳环，并且可用作包含具有稳定的含氟杂芳环的各种杂芳环化合物的材料，并且还含有具有杂芳环的含氟聚合物，可用作上述聚合物或固化剂的原料。另外，提供了在其侧链中具有杂芳环如咪唑的含氟聚合物，其聚合物盐和包含这种聚合物和聚合物盐和纳米填料的聚合物组合物。

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