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1. 发明授权

US06872324B2 Aqueous dispersion 有权
标题翻译：水分散体
公开(公告)号：US06872324B2
公开(公告)日：2005-03-29
申请号：US10354034
申请日：2003-01-30
申请人： Takashige Maekawa , Minako Shimada , Ryuji Seki , Taiki Hoshino
发明人： Takashige Maekawa , Minako Shimada , Ryuji Seki , Taiki Hoshino
IPC分类号： C08F2/24 , C08F36/04 , C08K5/00 , C09D133/06 , C09D133/16 , C09K3/18 , D06M15/21 , D06M15/256 , D06M15/263 , D06M15/277 , C14C9/00 , C08F136/16 , C08F236/16 , D06M15/347
CPC分类号： D06M15/21 , C08K5/0008 , C09D133/06 , C09D133/16 , C09K3/18 , D06M15/256 , D06M15/263 , D06M15/277 , D06M2200/11 , D06M2200/12 , C08L33/16
摘要： An aqueous dispersion comprising a polymer (a) having a repeating unit (A) which comprises four carbon atoms connected in a linear chain and which has one double bond at the second position and a polyfluoroalkyl group bonded to an arbitrary carbon atom, and a surfactant (B) having a hydrophile-lipophile balance of at least 10, wherein the polymer (a) is dispersed in an aqueous medium by the surfactant (B).
摘要翻译：一种水分散体，其包含具有重复单元（A）的聚合物（a），所述重复单元（A）包含连接在直链上且在第二位置具有一个双键的四个碳原子和与任意碳原子键合的多氟烷基，表面活性剂（B）具有至少10的亲水 - 亲油平衡，其中聚合物（a）通过表面活性剂（B）分散在水性介质中。

2. 发明授权

US06716944B2 Water and oil repellent composition 有权
标题翻译：防水防油组成
公开(公告)号：US06716944B2
公开(公告)日：2004-04-06
申请号：US10317991
申请日：2002-12-13
申请人： Takashige Maekawa , Minako Shimada , Shuichiro Sugimoto , Ryuji Seki
发明人： Takashige Maekawa , Minako Shimada , Shuichiro Sugimoto , Ryuji Seki
IPC分类号： C08F11800
CPC分类号： C09K3/18
摘要： A water and oil repellent composition which can impart an excellent water and oil repellency to an object, even if it is processed at a low temperature, and which can achieve a water and oil repellent treatment providing a soft hand. The water and oil repellent composition which has as an essential component a copolymer consisting essentially of polymerized units of the following monomer (a) and polymerized units of the following monomer (b). monomer (a): an Rf monomer wherein the melting point of fine crystals derived from the Rf groups of the homopolymer does not exist or is at most 50° C. monomer (b): a monomer having no Rf group, wherein the melting point of fine crystals derived from the side chains of the homopolymer is at least 30° C.
摘要翻译：即使在低温下进行处理也能够使物品具有优异的拒水拒油性的斥水斥油剂组合物，能够实现提供软手的拒水拒油处理。具有以下单体（a）的聚合单元和以下单体（b）单体的聚合单元共聚物作为基本组分的斥水斥油剂组合物。单体（a）：R f单体，其中衍生自均聚物的R f基团的细晶体的熔点不存在或至多为50℃。单体（b）：不具有R f基团的单体，其中衍生的细晶体的熔点来自均聚物的侧链为至少30℃

3. 发明授权

US08609795B2 Water and oil repellent composition 有权
标题翻译：防水防油组成
公开(公告)号：US08609795B2
公开(公告)日：2013-12-17
申请号：US11940577
申请日：2007-11-15
申请人： Shuichiro Sugimoto , Minako Shimada , Toyomichi Shimada , Ryuji Seki , Takashige Maekawa
发明人： Shuichiro Sugimoto , Minako Shimada , Toyomichi Shimada , Ryuji Seki , Takashige Maekawa
IPC分类号： C08F118/00
CPC分类号： D06M15/256 , C08F218/08 , C08F220/18 , C08F220/22 , C08F220/24 , C08F220/34 , C08F220/36 , C08F230/08 , C09K3/18 , D06M15/263 , D06M2200/00 , D06M2200/11 , D06M2200/12 , D06M2200/50
摘要： A water and oil repellent composition having excellent durability, which can impart excellent water and oil repellency to an object, even in a process at low temperatures, and which enables water and oil repellent treatment providing a soft hand. A water and oil repellent composition which comprises, as an essential component, a copolymer containing polymerization units of the following monomer (a) and polymerization units of the following monomer (b): monomer (a): an Rf group-containing monomer which forms a photopolymer having no melting point or a melting point of at most 55° C. attributable to fine crystals derived from the Rf groups and having a glass transition point of at least 20° C. monomer (b): a monomer having no Rf group and having a cross-linkable functional group.
摘要翻译：具有优异的耐久性的防油斥油剂组合物，即使在低温下也能赋予物体优异的拒水拒油性，能够提供柔软的防水防油处理。作为必要成分的防水斥油剂组合物，其含有含有下述单体（a）的聚合单元和下述单体（b）的聚合单元的共聚物：单体（a）：含有Rf基的单体，其形成不含熔点或熔点至多55℃的光聚合物，归因于衍生自Rf基团的微晶，玻璃化转变点至少为20℃。单体（b）：不具有Rf基团的单体并具有可交联的官能团。

4. 发明申请

US20080076862A1 WATER AND OIL REPELLENT COMPOSITION 有权
标题翻译：水和油组合物
公开(公告)号：US20080076862A1
公开(公告)日：2008-03-27
申请号：US11940577
申请日：2007-11-15
申请人： Shuichiro Sugimoto , Minako Shimada , Toyomichi Shimada , Ryuji Seki , Takashige Maekawa
发明人： Shuichiro Sugimoto , Minako Shimada , Toyomichi Shimada , Ryuji Seki , Takashige Maekawa
IPC分类号： C08F18/20
CPC分类号： D06M15/256 , C08F218/08 , C08F220/18 , C08F220/22 , C08F220/24 , C08F220/34 , C08F220/36 , C08F230/08 , C09K3/18 , D06M15/263 , D06M2200/00 , D06M2200/11 , D06M2200/12 , D06M2200/50
摘要： A water and oil repellent composition having excellent durability, which can impart excellent water and oil repellency to an object, even in a process at low temperatures, and which enables water and oil repellent treatment providing a soft hand. A water and oil repellent composition which comprises, as an essential component, a copolymer containing polymerization units of the following monomer (a) and polymerization units of the following monomer (b): monomer (a): an Rf group-containing monomer which forms a photopolymer having no melting point or a melting point of at most 55° C. attributable to fine crystals derived from the Rf groups and having a glass transition point of at least 20° C. monomer (b): a monomer having no Rf group and having a cross-linkable functional group.
摘要翻译：具有优异的耐久性的防油斥油剂组合物，即使在低温下也能赋予物体优异的拒水拒油性，能够提供柔软的防水和防油处理。作为必要成分的防油斥油剂组合物，含有下述单体（a）的聚合单元和下述单体（b）的聚合单元的共聚物：单体（a）：R f 含有基团的单体，其形成不含熔点或熔点至多55℃的光聚合物，归因于衍生自R f F基团的微晶，玻璃化转变点为至少20℃单体（b）：不具有R f F基团且具有可交联官能团的单体。

5. 发明申请

US20050267241A1 Water and oil repellent composition 审中-公开
标题翻译：防水防油组成
公开(公告)号：US20050267241A1
公开(公告)日：2005-12-01
申请号：US11106641
申请日：2005-04-15
申请人： Shuichiro Sugimoto , Minako Shimada , Toyomichi Shimada , Ryuji Seki , Takashige Maekawa
发明人： Shuichiro Sugimoto , Minako Shimada , Toyomichi Shimada , Ryuji Seki , Takashige Maekawa
IPC分类号： C09K3/18 , C08F18/20
CPC分类号： D06M15/256 , C08F218/08 , C08F220/18 , C08F220/22 , C08F220/24 , C08F220/34 , C08F220/36 , C08F230/08 , C09K3/18 , D06M15/263 , D06M2200/00 , D06M2200/11 , D06M2200/12 , D06M2200/50
摘要： A water and oil repellent composition having excellent durability, which can impart excellent water and oil repellency to an object, even in a process at low temperatures, and which enables water and oil repellent treatment providing a soft hand. A water and oil repellent composition which comprises, as an essential component, a copolymer containing polymerization units of the following monomer (a) and polymerization units of the following monomer (b): monomer (a): an Rf group-containing monomer which forms a photopolymer having no melting point or a melting point of at most 55° C. attributable to fine crystals derived from the Rf groups and having a glass transition point of at least 20° C. monomer (b): a monomer having no Rf group and having a cross-linkable functional group.
摘要翻译：具有优异的耐久性的防油斥油剂组合物，即使在低温下也能赋予物体优异的拒水拒油性，能够提供柔软的防水防油处理。作为必要成分的防油斥油剂组合物，含有下述单体（a）的聚合单元和下述单体（b）的聚合单元的共聚物：单体（a）：R f 含有基团的单体，其形成不含熔点或熔点至多55℃的光聚合物，归因于衍生自R f F基团的微晶，玻璃化转变点为至少20℃单体（b）：不具有R f F基团且具有可交联官能团的单体。

6. 发明授权

US06860926B2 Fluorine-containing compound, and water and oil repellent composition 失效
标题翻译：含氟化合物，防水防油组合物
公开(公告)号：US06860926B2
公开(公告)日：2005-03-01
申请号：US09976435
申请日：2001-10-15
申请人： Minako Ishikawa , Takashige Maekawa , Ryuji Seki , Shoji Furuta , Kazuya Oharu
发明人： Minako Ishikawa , Takashige Maekawa , Ryuji Seki , Shoji Furuta , Kazuya Oharu
IPC分类号： C03C17/28 , C03C17/32 , C03C25/24 , C03C25/26 , C07C69/62 , C07C69/63 , C07C311/09 , C09K3/18 , D06M13/236 , D06M15/277 , C07C311/24
CPC分类号： D06M15/277 , C03C17/28 , C03C17/32 , C03C25/25 , C03C25/26 , C07C69/62 , C07C69/63 , C07C311/09 , C09K3/18 , D06M13/236 , D06M2200/10 , D06M2200/11 , D06M2200/12
摘要： The following fluorine-containing compound is presented which is capable of providing dry soil resistance when incorporated to a water and oil repellent.Rf1R2OCOCH2CHR1COOR3Rf2 (wherein each of Rf1 and Rf2 which are independent of each other, is a C3-22 polyfluoroalkyl group, R1 is a hydrogen atom or a C1-10 alkyl group, and each of R2 and R3 which are independent of each other, is a C1-4 alkylene group, etc.).
摘要翻译：提供以下含氟化合物，其在掺入拒水拒油剂时能够提供干性土壤抗性。R 1 R 2 OCOCH 2 CHR 1 COOR 3 R f（其中每个R 彼此独立的和R f2是C3-22多氟烷基，R 1是氢原子或C 1-10烷基，R 2和R 3中的每一个 >彼此独立，是C 1-4亚烷基等）。

7. 发明申请

US20050004337A1 Process for producing a polyfluoroalkyl (meth) acrylate 审中-公开
标题翻译：（甲基）丙烯酸多氟烷基酯的制造方法
公开(公告)号：US20050004337A1
公开(公告)日：2005-01-06
申请号：US10859213
申请日：2004-06-03
申请人： Shoji Furuta , Taiki Hoshino , Ryuji Seki
发明人： Shoji Furuta , Taiki Hoshino , Ryuji Seki
IPC分类号： B01D3/14 , C07C17/383 , C07C67/10 , C07C67/54 , C07C67/56 , C07C69/003 , C07C69/653 , C08G63/682 , C08G63/78 , C08G63/90 , C08F118/02
CPC分类号： C07C67/10 , C07C17/383 , C07C67/56 , C07C21/18 , C07C69/653
摘要： A process for producing a polyfluoroalkyl (meth)acrylate, which comprises isolating, from a reaction mixture containing a polyfluoroalkyl (meth)acrylate obtained by reacting a polyfluoroalkyl iodide of the formula CnF2n+1(CH2)mI (wherein n is an integer of from 2 to 7, and m is an integer of from 1 to 4) with a metal (meth)acrylate in tert-butanol, said polyfluoroalkyl (meth)acrylate by the following steps (1) to (3): (1) a step of taking out a crude liquid from the reaction mixture by solid-liquid separation; (2) a step of distilling the crude liquid to separate it into compound group A of compounds having a lower boiling point than the polyfluoroalkyl (meth)acrylate and compound group B of the polyfluoroalkyl (meth)acrylate and compounds having a higher boiling point than the polyfluoroalkyl (meth)acrylate; and (3) a step of distilling and purifying the polyfluoroalkyl (meth)acrylate from the compound group B in the presence of a polymerization inhibitor.
摘要翻译：一种制备多氟烷基（甲基）丙烯酸酯的方法，该方法包括从含有通式CnF 2 n + 1（CH 2）m I的多氟烷基碘化物得到的（甲基）丙烯酸多氟烷基酯的反应混合物中分离，其中n为 2〜7，m为1〜4的整数）与叔丁醇中的（甲基）丙烯酸金属化合物，所述（甲基）丙烯酸多氟烷基酯通过以下步骤（1）〜（3）：（1）通过固液分离从反应混合物中取出粗液; （2）蒸馏粗液以将其分解成沸点低于（甲基）丙烯酸多氟烷基酯和（甲基）丙烯酸多氟烷基酯的化合物B的化合物的化合物组A和沸点高于（甲基）丙烯酸多氟烷基酯; 和（3）在聚合抑制剂的存在下，从化合物组B中蒸馏纯化（甲基）丙烯酸多氟烷基酯的步骤。

8. 发明申请

US20090118433A1 PROCESS FOR PRODUCING A POLYFLUOROALKYL (METH)ACRYLATE 有权
标题翻译：制备聚氟代（甲基）丙烯酸酯的方法
公开(公告)号：US20090118433A1
公开(公告)日：2009-05-07
申请号：US12350502
申请日：2009-01-08
申请人： Shoji FURUTA , Taiki Hoshino , Ryuji Seki
发明人： Shoji FURUTA , Taiki Hoshino , Ryuji Seki
IPC分类号： C08L27/22 , C08F114/18
CPC分类号： C07C67/10 , C07C17/383 , C07C67/56 , C07C21/18 , C07C69/653
摘要： A process for producing a polyfluoroalkyl (meth)acrylate, which comprises isolating, from a reaction mixture containing a polyfluoroalkyl (meth)acrylate obtained by reacting a polyfluoroalkyl iodide of the formula CnF2n+1(CH2)mI (wherein n is an integer of from 2 to 7, and m is an integer of from 1 to 4) with a metal (meth)acrylate in tert-butanol, said polyfluoroalkyl (meth)acrylate by the following steps (1) to (3): (1) a step of taking out a crude liquid from the reaction mixture by solid-liquid separation; (2) a step of distilling the crude liquid to separate it into compound group A of compounds having a lower boiling point than the polyfluoroalkyl (meth)acrylate and compound group B of the polyfluoroalkyl (meth)acrylate and compounds having a higher boiling point than the polyfluoroalkyl (meth)acrylate; and (3) a step of distilling and purifying the polyfluoroalkyl (meth)acrylate from the compound group B in the presence of a polymerization inhibitor.
摘要翻译：一种制备多氟烷基（甲基）丙烯酸酯的方法，该方法包括从含有通式CnF 2 n + 1（CH 2）m I的多氟烷基碘化物得到的（甲基）丙烯酸多氟烷基酯的反应混合物中分离，其中n为 2〜7，m为1〜4的整数）与叔丁醇中的（甲基）丙烯酸金属化合物，所述（甲基）丙烯酸多氟烷基酯通过以下步骤（1）〜（3）：（1）通过固液分离从反应混合物中取出粗液; （2）蒸馏粗液以将其分解成沸点低于（甲基）丙烯酸多氟烷基酯和（甲基）丙烯酸多氟烷基酯的化合物B的化合物的化合物组A和沸点高于（甲基）丙烯酸多氟烷基酯; 和（3）在聚合抑制剂的存在下，从化合物组B中蒸馏纯化（甲基）丙烯酸多氟烷基酯的步骤。

9. 发明授权

US07723439B2 Process for producing a polyfluoroalkyl (meth)acrylate 有权
标题翻译：（甲基）丙烯酸多氟烷基酯的制造方法
公开(公告)号：US07723439B2
公开(公告)日：2010-05-25
申请号：US12350502
申请日：2009-01-08
申请人： Shoji Furuta , Taiki Hoshino , Ryuji Seki
发明人： Shoji Furuta , Taiki Hoshino , Ryuji Seki
IPC分类号： C08L27/22 , C08F114/18
CPC分类号： C07C67/10 , C07C17/383 , C07C67/56 , C07C21/18 , C07C69/653
摘要： A process for producing a polyfluoroalkyl (meth)acrylate, which comprises isolating, from a reaction mixture containing a polyfluoroalkyl (meth)acrylate obtained by reacting a polyfluoroalkyl iodide of the formula CnF2n+1(CH2)mI (wherein n is an integer of from 2 to 7, and m is an integer of from 1 to 4) with a metal (meth)acrylate in tert-butanol, said polyfluoroalkyl (meth)acrylate by the following steps (1) to (3): (1) a step of taking out a crude liquid from the reaction mixture by solid-liquid separation; (2) a step of distilling the crude liquid to separate it into compound group A of compounds having a lower boiling point than the polyfluoroalkyl (meth)acrylate and compound group B of the polyfluoroalkyl (meth)acrylate and compounds having a higher boiling point than the polyfluoroalkyl (meth)acrylate; and (3) a step of distilling and purifying the polyfluoroalkyl (meth)acrylate from the compound group B in the presence of a polymerization inhibitor.
摘要翻译：一种制备多氟烷基（甲基）丙烯酸酯的方法，该方法包括从含有通式CnF 2 n + 1（CH 2）m I的多氟烷基碘化物得到的（甲基）丙烯酸多氟烷基酯的反应混合物中分离，其中n为 2〜7，m为1〜4的整数）与叔丁醇中的（甲基）丙烯酸金属化合物，所述（甲基）丙烯酸多氟烷基酯通过以下步骤（1）〜（3）：（1）通过固液分离从反应混合物中取出粗液; （2）蒸馏粗液以将其分解成沸点低于（甲基）丙烯酸多氟烷基酯和（甲基）丙烯酸多氟烷基酯的化合物B的化合物的化合物组A和沸点高于（甲基）丙烯酸多氟烷基酯; 和（3）在聚合抑制剂的存在下，从化合物组B中蒸馏纯化（甲基）丙烯酸多氟烷基酯的步骤。

10. 发明授权

US06720371B2 Water repellent and oil resistant composition 失效
标题翻译：防水防油组合物
公开(公告)号：US06720371B2
公开(公告)日：2004-04-13
申请号：US10164577
申请日：2002-06-10
申请人： Shoji Furuta , Ryuji Seki , Hiroshi Funaki
发明人： Shoji Furuta , Ryuji Seki , Hiroshi Funaki
IPC分类号： C08K506
CPC分类号： D21H17/72 , D21H21/16
摘要： A water repellent and oil resistant composition capable of imparting excellent water repellency and oil resistance to paper even under a condition of drying at a low temperature for a short time, is provided. The composition comprising a fluorocopolymer (A) obtained by polymerizing a polyfluoroalkyl group-containing (meth)acrylate, vinylidene chloride and a compound of the formula [CH2═C(R)COO—CH2—CH(OH)CH2N+(CH3)3·X− (R: a hydrogen atom or a methyl group, and X−: a counter ion)] or the like by means of a lipophilic polymerization initiator (E) having a solubility of less than 3 g in 100 g of water, a non-fluorine surfactant (B), a medium (C) and a water-soluble polymer (D) (a polyacrylamide, a polyvinyl alcohol or starch).
摘要翻译：提供了即使在短时间内在低温下干燥的条件下也能赋予纸的优异的防水性和耐油性的防水防油组合物。包含通过聚合多氟烷基得到的含氟共聚物（A）（甲基）丙烯酸酯，偏二氯乙烯和式[CH 2 = C（R）COO-CH 2 -CH（OH）CH 2 N +（CH 3）3 X“的化合物（R：氢原子或甲基，X - ：抗衡离子）]等，通过在100g水中溶解度小于3g的亲脂性聚合引发剂（E），非氟表面活性剂（ B），中等（C）和水溶性聚合物（D）（聚丙烯酰胺，聚乙烯醇或淀粉）。

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