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1. 发明授权

US09242911B2 Preparation method for fluorine-containing olefins having organic-group substituents 有权
标题翻译：含有有机基取代基的含氟烯烃的制备方法
公开(公告)号：US09242911B2
公开(公告)日：2016-01-26
申请号：US13985659
申请日：2012-03-08
申请人： Takabumi Nagai , Kenji Adachi , Takashi Shibanuma , Sensuke Ogoshi , Masato Ohashi
发明人： Takabumi Nagai , Kenji Adachi , Takashi Shibanuma , Sensuke Ogoshi , Masato Ohashi
IPC分类号： C07C17/26 , C07C17/263 , C07C45/61 , C07C253/30 , C07F5/04 , C07C45/68 , C07F5/02 , C07C67/343
CPC分类号： C07C17/26 , C07C17/263 , C07C45/61 , C07C45/68 , C07C67/343 , C07C253/30 , C07F5/025 , C07F5/04 , C07C22/08 , C07C255/50 , C07C47/55 , C07C69/76
摘要： An object of the present invention is to provide a method that enables the easy and efficient (high yield, high selectivity, low cost) preparation of a fluorine-containing olefin substituted with an organic group or groups from a fluorine-containing olefin.[Solution]The method for preparing a fluorine-containing olefin substituted with an organic group or groups, the method comprising a step of reacting a fluorine-containing olefin with an organic boron compound in the presence of an organic transition metal catalyst containing at least one transition metal selected from the group consisting of nickel, palladium, platinum, rhodium, ruthenium, and cobalt.
摘要翻译：本发明的目的是提供一种能够容易且有效（高产率，高选择性，低成本）制备由有机基团或含氟烯烃取代的含氟烯烃的方法。 [解决方案]制备含有有机基团的含氟烯烃的方法，该方法包括在含有至少一种有机过渡金属催化剂的有机过渡金属催化剂存在下使含氟烯烃与有机硼化合物反应的步骤选自镍，钯，铂，铑，钌和钴的过渡金属。

2. 发明申请

US20130324757A1 PREPARATION METHOD FOR FLUORINE-CONTAINING OLEFINS HAVING ORGANIC-GROUP SUBSTITUENTS 有权
标题翻译：含有含有有机取代基的烯烃的制备方法
公开(公告)号：US20130324757A1
公开(公告)日：2013-12-05
申请号：US13985659
申请日：2012-03-08
申请人： Takabumi Nagai , Kenji Adachi , Takashi Shibanuma , Sensuke Ogoshi , Masato Ohashi
发明人： Takabumi Nagai , Kenji Adachi , Takashi Shibanuma , Sensuke Ogoshi , Masato Ohashi
IPC分类号： C07C17/26 , C07C253/30 , C07C67/343 , C07F5/04 , C07C45/61
CPC分类号： C07C17/26 , C07C17/263 , C07C45/61 , C07C45/68 , C07C67/343 , C07C253/30 , C07F5/025 , C07F5/04 , C07C22/08 , C07C255/50 , C07C47/55 , C07C69/76
摘要： An object of the present invention is to provide a method that enables the easy and efficient (high yield, high selectivity, low cost) preparation of a fluorine-containing olefin substituted with an organic group or groups from a fluorine-containing olefin.[Solution] The method for preparing a fluorine-containing olefin substituted with an organic group or groups, the method comprising a step of reacting a fluorine-containing olefin with an organic boron compound in the presence of an organic transition metal catalyst containing at least one transition metal selected from the group consisting of nickel, palladium, platinum, rhodium, ruthenium, and cobalt.
摘要翻译：本发明的目的是提供一种能够容易且有效（高产率，高选择性，低成本）制备由有机基团或含氟烯烃取代的含氟烯烃的方法。 [解决方案]制备含有有机基团的含氟烯烃的方法，该方法包括在含有至少一种有机过渡金属催化剂的有机过渡金属催化剂存在下使含氟烯烃与有机硼化合物反应的步骤选自镍，钯，铂，铑，钌和钴的过渡金属。

3. 发明申请

US20120330072A1 METHOD FOR PRODUCING SUBSTITUTED FLUORINE-CONTAINING OLEFIN 有权
标题翻译：生产取代含氟的含烯烃的方法
公开(公告)号：US20120330072A1
公开(公告)日：2012-12-27
申请号：US13581849
申请日：2011-03-03
申请人： Takabumi Nagai , Takashi Shibanuma , Sensuke Ogoshi , Masato Ohashi
发明人： Takabumi Nagai , Takashi Shibanuma , Sensuke Ogoshi , Masato Ohashi
IPC分类号： C07C17/32
CPC分类号： B01J23/892 , B01J31/2295 , B01J31/2404 , B01J31/2409 , B01J2231/4233 , B01J2531/824 , B01J2531/847 , C07C17/2632 , C07C22/08
摘要： This invention relates to a method of reacting fluoroolefin with an organic magnesium compound in the presence of a catalyst comprising nickel or palladium so as to efficiently produce fluoroolefin, such as TFE, in which a fluorine (F) atom or atoms bonded to the sp2 hybridized carbon atom are substituted with an organic group.
摘要翻译：本发明涉及在含有镍或钯的催化剂存在下使氟代烯烃与有机镁化合物反应的方法，以便有效地生产氟（F）原子或结合到sp2上的原子杂原子的TFE等氟烯烃碳原子被有机基团取代。

4. 发明授权

US09067200B2 Method for producing substituted fluorine-containing olefin 有权
标题翻译：取代的含氟烯烃的制备方法
公开(公告)号：US09067200B2
公开(公告)日：2015-06-30
申请号：US13581849
申请日：2011-03-03
申请人： Takabumi Nagai , Takashi Shibanuma , Sensuke Ogoshi , Masato Ohashi
发明人： Takabumi Nagai , Takashi Shibanuma , Sensuke Ogoshi , Masato Ohashi
IPC分类号： C07C17/263 , C07C17/266 , C07C22/08 , B01J23/89
CPC分类号： B01J23/892 , B01J31/2295 , B01J31/2404 , B01J31/2409 , B01J2231/4233 , B01J2531/824 , B01J2531/847 , C07C17/2632 , C07C22/08
摘要： This invention relates to a method of reacting fluoroolefin with an organic magnesium compound in the presence of a catalyst comprising nickel or palladium so as to efficiently produce fluoroolefin, such as TFE, in which a fluorine (F) atom or atoms bonded to the sp2 hybridized carbon atom are substituted with an organic group.
摘要翻译：本发明涉及在含有镍或钯的催化剂存在下使氟代烯烃与有机镁化合物反应的方法，以便有效地生产氟（F）原子或结合到sp2上的原子杂原子的TFE等氟烯烃碳原子被有机基团取代。

5. 发明申请

US20140234198A1 ETCHING METHOD AND METHOD FOR PERFORMING SURFACE PROCESSING ON SOLID MATERIAL FOR SOLAR CELL 审中-公开
标题翻译：用于对太阳能电池进行固体表面处理的蚀刻方法和方法
公开(公告)号：US20140234198A1
公开(公告)日：2014-08-21
申请号：US14237948
申请日：2012-08-10
申请人： Mizuho Morita , Junichi Uchikoshi , Kentaro Tsukamoto , Takabumi Nagai , Kenji Adachi
发明人： Mizuho Morita , Junichi Uchikoshi , Kentaro Tsukamoto , Takabumi Nagai , Kenji Adachi
IPC分类号： H01L31/0236 , H01L31/18
CPC分类号： H01L31/02366 , H01L31/02363 , H01L31/18 , Y02E10/50
摘要： Provided is an etching method including: (1) bringing a material containing at least one organic compound having an N—F bond into contact with the surface of a solid material; and (2) a step of heating the solid material; whereby etching can be performed safely and in a simple manner, at a higher etching rate, without the use of a high-environmental-load gas that causes global warming or highly reactive and toxic fluorine gas or hydrofluoric acid. The etching method may further include: (3) a step of exposing the solid material to light from the side of the material containing at least one organic compound having an N—F bond; and (4) a step of removing the material containing at least one organic compound having an N—F bond together with the residue remained between said material and the solid material. In particular, performing heating at a high temperature and applying light irradiation make it possible to form inverted pyramid-shaped recesses that are suitable for applying light-trapping and/or anti-reflection processing to the surface of the solid material for a solar cell.
摘要翻译：提供一种蚀刻方法，包括：（1）使含有至少一种具有N-F键的有机化合物的材料与固体材料的表面接触; 和（2）加热固体材料的步骤; 从而能够以更高的蚀刻速度安全地且以简单的方式执行蚀刻，而不使用引起全球变暖的高环境负荷气体或高反应性和有毒的氟气或氢氟酸。蚀刻方法可以进一步包括：（3）将固体材料从含有至少一种具有N-F键的有机化合物的材料侧暴露于光的步骤; 和（4）除去含有至少一种具有N-F键的有机化合物的材料与残留物在所述材料和固体材料之间的步骤。特别是，在高温下进行加热并施加光照射使得可以形成适于对太阳能电池的固体材料的表面进行光捕获和/或抗反射处理的倒棱锥形凹部。

6. 发明授权

US07157002B2 Process for the recovery of surfactants 有权
标题翻译：回收表面活性剂的方法
公开(公告)号：US07157002B2
公开(公告)日：2007-01-02
申请号：US10561176
申请日：2004-06-18
申请人： Takabumi Nagai , Kazuhisa Fujii , Hideaki Asai
发明人： Takabumi Nagai , Kazuhisa Fujii , Hideaki Asai
IPC分类号： B01D11/00
CPC分类号： B01D19/0068 , B01D11/0407 , D06F43/08 , G03F7/3092 , H01L21/31133
摘要： The present invention relates to a method for recovering a surfactant from a water-carbon dioxide system comprising at least one type of surfactant, water and carbon dioxide, the method comprising the step of bringing the water-carbon dioxide system into contact with a dehydrating agent to remove water. Furthermore, the present invention relates to a method comprising the steps of installing a device for selectively removing a removal target in a circulation line in which circulated is a mixed system comprising carbon dioxide, a carbon dioxide-compatible surfactant and/or a cosolvent, and a removal target; circulating the mixed system; and selectively removing the removal target that has been incorporated into the surfactant and/or cosolvent.
摘要翻译：本发明涉及从包含至少一种表面活性剂，水和二氧化碳的水 - 二氧化碳体系中回收表面活性剂的方法，该方法包括使水 - 二氧化碳体系与脱水剂接触的步骤去除水。此外，本发明涉及一种方法，包括以下步骤：安装用于选择性地除去循环管线中的除去靶的装置，其中循环是包括二氧化碳，二氧化碳相容的表面活性剂和/或助溶剂的混合系统，以及移除目标; 循环混合系统; 并且选择性地去除已经结合到表面活性剂和/或助溶剂中的去除靶。

7. 发明授权

US07811473B2 Branched surfactant having fluoroalkyl group and hydrocarbon group 有权
标题翻译：具有氟代烷基和烃基的支化表面活性剂
公开(公告)号：US07811473B2
公开(公告)日：2010-10-12
申请号：US11596672
申请日：2005-05-16
申请人： Takabumi Nagai , Kazuhisa Fujii
发明人： Takabumi Nagai , Kazuhisa Fujii
IPC分类号： B01F1/00
CPC分类号： B01F17/0057 , C07C305/06 , C07C307/10 , C07C309/17 , C11D1/004
摘要： The present invention relates to a surfactant represented by Formula (I):[Formula 1] wherein Rf represents a fluoroalkyl group which may have an ether bond; Rh represents an alkyl group; r represents 1 or 0; when r=0, Z1 and Z2 represent (CH2)n1—(X1)p1— and —(X2)q1—, respectively; and when r=1, Z1 and Z2 represent (CH2Y)p2—CH2— and —(CH2Y)q2—, respectively, wherein X1 and X2 may be the same or different and each represents a divalent linking group, p1 represents 0 or 1, q1 represents 0 or 1, n1 represents an integer of 1-10; Y represents O, S or NR, wherein R represents a hydrogen atom, methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, sec-butyl, or t-butyl; p2 and q2 each represent 0 or 1 but are not 0 at the same time; and M represents a hydrogen atom, alkali metal, ½ alkaline earth metal or ammonium.
摘要翻译：本发明涉及由式（I）表示的表面活性剂：[式1]其中Rf表示可具有醚键的氟代烷基; Rh表示烷基; r表示1或0; 当r = 0时，Z1和Z2分别表示（CH2）n1-（X1）p1和 - （X2）q1; 并且当r = 1时，Z 1和Z 2分别表示（CH 2 Y）p2-CH2-和 - （CH2Y）q2-，其中X1和X2可以相同或不同，并且各自表示二价连接基团，p1表示0或1 q1表示0或1，n1表示1〜10的整数， Y表示O，S或NR，其中R表示氢原子，甲基，乙基，正丙基，异丙基，正丁基，异丁基，仲丁基或叔丁基; p2和q2各自表示0或1，但不同时为0; M表示氢原子，碱金属，½碱土金属或铵。

8. 发明申请

US20070175763A1 Electroplating in presence of co2 审中-公开
标题翻译：存在co2时电镀
公开(公告)号：US20070175763A1
公开(公告)日：2007-08-02
申请号：US10589263
申请日：2005-02-14
申请人： Takabumi Nagai , Kazuhisa Fujii , Hideaki Asai
发明人： Takabumi Nagai , Kazuhisa Fujii , Hideaki Asai
IPC分类号： C25D5/00
CPC分类号： C25D3/02 , C25D5/003
摘要： The present invention provides a method for conducting electroplating in the presence of CO2 and a metal salt-containing aqueous solution, wherein the CO2 is in the form of liquid, subcritical or supercritical, the method being characterized in that a nonionic compound having a CO2-affinitive moiety is further added to the system where the aqueous solution and CO2 coexist. The method of the present invention improves the efficiency of the electrochemical reaction process and enables formation of an excellent metal film.
摘要翻译：本发明提供了一种在CO 2 2和含金属盐的水溶液存在下进行电镀的方法，其中CO 2 2是液体，亚临界的形式或超临界的方法，其特征在于，在水溶液和CO 2共存的体系中进一步加入具有CO 2亚烷基部分的非离子化合物。本发明的方法提高了电化学反应过程的效率，并且能够形成优异的金属膜。

9. 发明申请

US20060124552A1 Process for the recovery of surfactants 有权
标题翻译：回收表面活性剂的方法
公开(公告)号：US20060124552A1
公开(公告)日：2006-06-15
申请号：US10561176
申请日：2004-06-18
申请人： Takabumi Nagai , Kazuhisa Fujii , Hideaki Asai
发明人： Takabumi Nagai , Kazuhisa Fujii , Hideaki Asai
IPC分类号： C02F1/28
CPC分类号： B01D19/0068 , B01D11/0407 , D06F43/08 , G03F7/3092 , H01L21/31133
摘要： The present invention relates to a method for recovering a surfactant from a water-carbon dioxide system comprising at least one type of surfactant, water and carbon dioxide, the method comprising the step of bringing the water-carbon dioxide system into contact with a dehydrating agent to remove water. Furthermore, the present invention relates to a method comprising the steps of installing a device for selectively removing a removal target in a circulation line in which circulated is a mixed system comprising carbon dioxide, a carbon dioxide-compatible surfactant and/or a cosolvent, and a removal target; circulating the mixed system; and selectively removing the removal target that has been incorporated into the surfactant and/or cosolvent.
摘要翻译：本发明涉及从包含至少一种表面活性剂，水和二氧化碳的水 - 二氧化碳体系中回收表面活性剂的方法，该方法包括使水 - 二氧化碳体系与脱水剂接触的步骤去除水。此外，本发明涉及一种方法，包括以下步骤：安装用于选择性地除去循环管线中的除去靶的装置，其中循环是包括二氧化碳，二氧化碳相容的表面活性剂和/或助溶剂的混合系统，以及移除目标; 循环混合系统; 并且选择性地去除已经结合到表面活性剂和/或助溶剂中的去除靶。

10. 发明授权

US07906042B2 Branched surfactant having fluoroalkyl group and hydrocarbon group 有权
标题翻译：具有氟代烷基和烃基的支化表面活性剂
公开(公告)号：US07906042B2
公开(公告)日：2011-03-15
申请号：US12696694
申请日：2010-01-29
申请人： Takabumi Nagai , Kazuhisa Fujii
发明人： Takabumi Nagai , Kazuhisa Fujii
IPC分类号： B01F1/00
CPC分类号： B01F17/0057 , C07C305/06 , C07C307/10 , C07C309/17 , C11D1/004
摘要： The present invention relates to a surfactant represented by Formula (I): wherein Rf represents a fluoroalkyl group which may have an ether bond; Rh represents an alkyl group; r represents 1 or 0; when r=0, Z1 and Z2 represent (CH2)n1—(X1)p1— and —(X2)q1—, respectively; and when r=1, Z1 and Z2 represent (CH2Y)p2—CH2— and —(CH2Y)q2—, respectively, wherein X1 and X2 may be the same or different and each represents a divalent linking group, p1 represents 0 or 1, q1 represents 0 or 1, n1 represents an integer of 1-10; Y represents O, S or NR, wherein R represents a hydrogen atom, methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, sec-butyl, or t-butyl; p2 and q2 each represent 0 or 1 but are not 0 at the same time; and M represents a hydrogen atom, alkali metal, ½ alkaline earth metal or ammonium.
摘要翻译：本发明涉及由式（I）表示的表面活性剂：其中Rf表示可具有醚键的氟烷基; Rh表示烷基; r表示1或0; 当r = 0时，Z1和Z2分别表示（CH2）n1-（X1）p1和 - （X2）q1; 并且当r = 1时，Z 1和Z 2分别表示（CH 2 Y）p2-CH2-和 - （CH2Y）q2-，其中X1和X2可以相同或不同，并且各自表示二价连接基团，p1表示0或1 q1表示0或1，n1表示1〜10的整数， Y表示O，S或NR，其中R表示氢原子，甲基，乙基，正丙基，异丙基，正丁基，异丁基，仲丁基或叔丁基; p2和q2各自表示0或1，但不同时为0; M表示氢原子，碱金属，½碱土金属或铵。

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