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1. 发明申请

US20060222865A1 Fluorinated compound, water repellent composition and thin film 失效
标题翻译：氟化合物，防水组合物和薄膜
公开(公告)号：US20060222865A1
公开(公告)日：2006-10-05
申请号：US11446200
申请日：2006-06-05
申请人： Taiki Hoshino , Yutaka Furukawa , Takashi Okazoe
发明人： Taiki Hoshino , Yutaka Furukawa , Takashi Okazoe
IPC分类号： C07F7/10 , B32B13/04
CPC分类号： B82Y10/00 , B82Y40/00 , C07F7/1804 , G03F7/0002 , G03F7/0045 , G03F7/0046
摘要： To provide a fluorinated compound, which can readily form a thin film having a hydrophobic/hydrophilic pattern, by employing an ultraviolet light having a relatively low energy. A thin film having a hydrophobic/hydrophilic pattern is formed by irradiating a thin film formed by employing a fluorinated compound represented by the following formula 1 (in the formula 1, each of R1, R2, R3 and R4 which are independent of one another, is a hydrogen atom, a halogen atom or a monovalent organic group, provided that at least one of them is a monovalent organic group having fluorine atoms, and R5 is a hydrogen atom or a monovalent organic group, R6 is a monovalent organic group, and A is a hetero atom) with ultraviolet light.
摘要翻译：为了提供能够容易地形成具有疏水/亲水图案的薄膜的氟化化合物，通过使用具有较低能量的紫外光。通过照射通过使用由下式1表示的氟化化合物形成的薄膜来形成具有疏水/亲水图案的薄膜（在式1中，R 1，R 2， 2个，R 3和R 4彼此独立的是氢原子，卤素原子或一价有机基团，条件是至少其中一个是具有氟原子的一价有机基团，R 5是氢原子或一价有机基团，R 6是一价有机基团，A是一个杂原子）与紫外线。

2. 发明授权

US08338502B2 Polymerizable fluorine-containing compound and treated substrate having a hydrophilic region and a water repellent region 失效
标题翻译：可聚合的含氟化合物和具有亲水区域和拒水区域的处理过的基材
公开(公告)号：US08338502B2
公开(公告)日：2012-12-25
申请号：US12365970
申请日：2009-02-05
申请人： Taiki Hoshino , Yutaka Furukawa
发明人： Taiki Hoshino , Yutaka Furukawa
IPC分类号： C08G18/67 , C08G61/00 , C08F2/46 , B05D3/02 , B41M5/00 , C07C55/36
CPC分类号： C07C69/708 , Y10T428/24802 , Y10T428/265 , Y10T442/2189
摘要： To provide a polymerizable fluorine-containing compound useful for producing a treated substrate having a hydrophilic region and a water repellent region, of which the contrast is high on its surface, without requiring a special apparatus, high energy light, or irradiation with light for a long time.A polymerizable fluorine-containing compound, which is a derivative of a polyhydric alcohol and comprises at least one following structure (A) and at least one following structure (B) in its molecule: structure (A): a structure wherein a compound having a fluoroalkyl group and a carboxyl group is bonded to one hydroxyl group of a polyhydric alcohol by an ester linkage, structure (B): a structure wherein a compound having an ethylenic double bond and a carboxyl group is bonded to one hydroxyl group of a polyhydric alcohol by an ester linkage or a structure wherein a compound having an ethylenic double bond and an isocyanate group is bonded to one hydroxyl group of a polyhydric alcohol by a urethane bond.
摘要翻译：为了提供可用于制备具有亲水区域和防水区域的处理基材的可聚合含氟化合物，其表面上的对比度高，而不需要特殊装置，高能量光或用于光的照射长时间。一种可聚合的含氟化合物，其是多元醇的衍生物，其分子中包含至少一种以下结构（A）和至少一种以下结构（B）：结构（A）：其中具有氟烷基和羧基通过酯键与多元醇的一个羟基键合，结构（B）：其中具有烯键式双键和羧基的化合物与多元醇的一个羟基键合的结构通过酯键或其中具有烯属双键和异氰酸酯基的化合物通过氨基甲酸酯键与多元醇的一个羟基键合的结构。

3. 发明授权

US07393515B2 Fluorinated compound, water repellent composition and thin film 失效
标题翻译：氟化合物，防水组合物和薄膜
公开(公告)号：US07393515B2
公开(公告)日：2008-07-01
申请号：US11446200
申请日：2006-06-05
申请人： Taiki Hoshino , Yutaka Furukawa , Takashi Okazoe
发明人： Taiki Hoshino , Yutaka Furukawa , Takashi Okazoe
IPC分类号： B01J3/06 , C07F7/04
CPC分类号： B82Y10/00 , B82Y40/00 , C07F7/1804 , G03F7/0002 , G03F7/0045 , G03F7/0046
摘要： To provide a fluorinated compound, which can readily form a thin film having a hydrophobic/hydrophilic pattern, by employing an ultraviolet light having a relatively low energy.A thin film having a hydrophobic/hydrophilic pattern is formed by irradiating a thin film formed by employing a fluorinated compound represented by the following formula 1 (in the formula 1, each of R1, R2, R3 and R4 which are independent of one another, is a hydrogen atom, a halogen atom or a monovalent organic group, provided that at least one of them is a monovalent organic group having fluorine atoms, and R5 is a hydrogen atom or a monovalent organic group, R6 is a monovalent organic group, and A is a hetero atom) with ultraviolet light
摘要翻译：为了提供能够容易地形成具有疏水/亲水图案的薄膜的氟化化合物，通过使用具有较低能量的紫外光。通过照射通过使用由下式1表示的氟化化合物形成的薄膜来形成具有疏水/亲水图案的薄膜（在式1中，R 1，R 2， 2个，R 3和R 4彼此独立的是氢原子，卤素原子或一价有机基团，条件是至少其中一个是具有氟原子的一价有机基团，R 5是氢原子或一价有机基团，R 6是一价有机基团，A是一个杂原子）与紫外线

4. 发明授权

US08309756B2 Surface treating agent, article and fluorinated ether compound 失效
标题翻译：表面处理剂，制品和氟化醚化合物
公开(公告)号：US08309756B2
公开(公告)日：2012-11-13
申请号：US13278216
申请日：2011-10-21
申请人： Daisuke Shirakawa , Yoshiyuki Gozu , Taiki Hoshino
发明人： Daisuke Shirakawa , Yoshiyuki Gozu , Taiki Hoshino
IPC分类号： C07C69/52 , C07C69/54 , B05D5/08 , B32B27/36
CPC分类号： C09D4/00 , B05D5/083 , C03C17/32 , C08F220/24 , C09D5/1668 , Y10T428/31504 , Y10T428/31507
摘要： To provide a surface treating agent and a composition for surface treatment capable of forming a coating film excellent in the water/oil repellency, the efficiency for removal of oil-and-fat stains, alkali resistance and heat resistance and having a low coefficient of friction; a method for treating the surface of an article by using the surface treating agent or the composition for surface treatment; an article having surface treatment applied; and a novel fluorinated ether compound useful as a surface treating agent. A surface treating agent comprising a compound represented by the following formula (A): RFO(CF2CF2O)aCF2C(O)N(H)b(-Q-OC(O)C(R)═CH2)2-b (A) wherein RF is a C1-20 perfluoro monovalent saturated hydrocarbon group or the like; a is an integer of from 1 to 200; b is 0 or 1; Q is a C1-6 alkylene group or the like; and R is a hydrogen atom or a C1-3 alkyl group.
摘要翻译：为了提供表面处理剂和表面处理组合物，能够形成防水拒油性优异，油脂污渍的除去效率，耐碱性和耐热性，摩擦系数低的涂膜 ; 通过使用表面处理剂或表面处理用组合物处理制品的表面的方法; 应用表面处理的制品; 以及可用作表面处理剂的新型氟化醚化合物。（A）表示的化合物的表面处理剂：RFO（CF 2 CF 2 O）a CF 2 C（O）N（H）b（-Q-OC（O）C（R）= CH 2）2-b 其中RF是C1-20全氟一价饱和烃基等; a为1〜200的整数; b为0或1; Q是C 1-6亚烷基等; 并且R是氢原子或C 1-3烷基。

5. 发明授权

US07799468B2 Electrolyte material for polymer electrolyte fuel cells, electrolyte membrane and membrane-electrode assembly 有权
标题翻译：用于聚合物电解质燃料电池，电解质膜和膜 - 电极组件的电解质材料
公开(公告)号：US07799468B2
公开(公告)日：2010-09-21
申请号：US11311560
申请日：2005-12-20
申请人： Atsushi Watakabe , Satoru Hommura , Seigo Kotera , Susumu Saito , Koichi Murata , Masanori Sawaguchi , Taiki Hoshino , Junichi Tayanagi , Eiji Endoh
发明人： Atsushi Watakabe , Satoru Hommura , Seigo Kotera , Susumu Saito , Koichi Murata , Masanori Sawaguchi , Taiki Hoshino , Junichi Tayanagi , Eiji Endoh
IPC分类号： H01M6/18
CPC分类号： C07D317/42 , B01D71/82 , C08F8/44 , C08F216/1466 , C08J5/18 , C08J5/225 , C08J2327/12 , H01B1/122 , H01M8/1023 , H01M8/1025 , H01M8/1039 , H01M2300/0082 , H01M2300/0091 , C08F214/262 , C08F216/38
摘要： An electrolyte material for polymer electrolyte fuel cells, which is made of a polymer containing repeating units based on a fluoromonomer having a radical polymerization reactivity, wherein the repeating units contain a 5-membered ring (which may contain 1 or 2 oxygen atoms), of which at least one carbon atom is contained in the main chain of the polymer, and an ionic group such as a sulfonic acid group which is bonded to the 5-membered ring directly or via a perfluoroalkylene group having a linear or branched structure; and the polymer has a softening temperature of at least 120° C.
摘要翻译：一种用于聚合物电解质燃料电池的电解质材料，其由含有具有自由基聚合反应性的含氟单体的重复单元的聚合物制成，其中重复单元包含5元环（可含有1或2个氧原子），该聚合物的主链中含有至少一个碳原子，以及直接或通过具有直链或支链结构的全氟亚烷基与5元环键合的磺酸基等离子性基团; 聚合物的软化温度至少为120℃

6. 发明授权

US07402714B2 Fluoroadamantane derivative 失效
标题翻译：氟金刚烷衍生物
公开(公告)号：US07402714B2
公开(公告)日：2008-07-22
申请号：US11567391
申请日：2006-12-06
申请人： Shu-zhong Wang , Taiki Hoshino , Kimiaki Kashiwagi , Takashi Okazoe , Eisuke Murotani , Masahiro Ito , Kunio Watanabe
发明人： Shu-zhong Wang , Taiki Hoshino , Kimiaki Kashiwagi , Takashi Okazoe , Eisuke Murotani , Masahiro Ito , Kunio Watanabe
IPC分类号： C07C35/37
CPC分类号： C07C69/653 , C07C29/095 , C07C35/52 , C07C67/14 , C07C67/287 , C07C2603/74 , C07C69/708
摘要： Adamantane derivates which can be material compounds of a polymer excellent in etching resistance and having improved transmittance to light having a short wavelength,represented by the formula (2A″) wherein Y1F is a fluorine atom or a hydroxyl group.
摘要翻译：金刚烷衍生物，其可以是耐蚀刻性优异的聚合物的材料化合物，并且具有由式（2A“）表示的具有短波长的光的透射率的改善，其中Y 1F是氟原子或羟基。

7. 发明授权

US08742159B2 Fluorinated compound and fluorinated polymer 有权
标题翻译：氟化合物和氟化聚合物
公开(公告)号：US08742159B2
公开(公告)日：2014-06-03
申请号：US13616024
申请日：2012-09-14
申请人： Taiki Hoshino
发明人： Taiki Hoshino
IPC分类号： C07C69/70
CPC分类号： C07C69/92 , C08F220/24 , C08F220/30
摘要： To provide a fluorinated compound having an RF group with at most 6 carbon atoms, whereby a fluorinated polymer having a highly durable water/oil repellency can be produced, and an environmental load is little, and a fluorinated polymer having a highly durable water/oil repellency and presenting little environmental load, obtainable by polymerizing such a fluorinated compound. A fluorinated compound represented by the following formula (I) and its polymer: CH2═C(M)COOXPhCOO(CH2)mCrF2r+1 (I) (in the formula (I), M is a hydrogen atom, a methyl group or a halogen atom, X is CHR1CH2O or CH2CHR1O, R1 is a C1-4 linear or branched alkyl group or CH2OR2, R2 is a C1-4 linear or branched alkyl group, Ph is a phenylene group, m is an integer of from 1 to 4, and r is an integer of from 1 to 6).
摘要翻译：为了提供具有至多6个碳原子的RF基团的氟化合物，由此可以制备具有高耐用斥水斥油性的氟化聚合物，并且环境负荷小，并且具有高耐久性水/油的氟化聚合物疏水性，并且通过聚合这种氟化化合物可以获得很小的环境负荷。由下式（I）表示的含氟化合物及其聚合物：CH2 = C（M）COOXPhCOO（CH2）mCrF2r + 1（I）（式（I）中，M为氢原子，甲基或卤素原子，X为CHR 1 CH 2 O或CH 2 CHROO，R 1为C 1-4直链或支链烷基或CH 2 OR 2，R 2为C 1-4直链或支链烷基，Ph为亚苯基，m为1〜4的整数，r为1〜6的整数）。

8. 发明授权

US07723439B2 Process for producing a polyfluoroalkyl (meth)acrylate 有权
标题翻译：（甲基）丙烯酸多氟烷基酯的制造方法
公开(公告)号：US07723439B2
公开(公告)日：2010-05-25
申请号：US12350502
申请日：2009-01-08
申请人： Shoji Furuta , Taiki Hoshino , Ryuji Seki
发明人： Shoji Furuta , Taiki Hoshino , Ryuji Seki
IPC分类号： C08L27/22 , C08F114/18
CPC分类号： C07C67/10 , C07C17/383 , C07C67/56 , C07C21/18 , C07C69/653
摘要： A process for producing a polyfluoroalkyl (meth)acrylate, which comprises isolating, from a reaction mixture containing a polyfluoroalkyl (meth)acrylate obtained by reacting a polyfluoroalkyl iodide of the formula CnF2n+1(CH2)mI (wherein n is an integer of from 2 to 7, and m is an integer of from 1 to 4) with a metal (meth)acrylate in tert-butanol, said polyfluoroalkyl (meth)acrylate by the following steps (1) to (3): (1) a step of taking out a crude liquid from the reaction mixture by solid-liquid separation; (2) a step of distilling the crude liquid to separate it into compound group A of compounds having a lower boiling point than the polyfluoroalkyl (meth)acrylate and compound group B of the polyfluoroalkyl (meth)acrylate and compounds having a higher boiling point than the polyfluoroalkyl (meth)acrylate; and (3) a step of distilling and purifying the polyfluoroalkyl (meth)acrylate from the compound group B in the presence of a polymerization inhibitor.
摘要翻译：一种制备多氟烷基（甲基）丙烯酸酯的方法，该方法包括从含有通式CnF 2 n + 1（CH 2）m I的多氟烷基碘化物得到的（甲基）丙烯酸多氟烷基酯的反应混合物中分离，其中n为 2〜7，m为1〜4的整数）与叔丁醇中的（甲基）丙烯酸金属化合物，所述（甲基）丙烯酸多氟烷基酯通过以下步骤（1）〜（3）：（1）通过固液分离从反应混合物中取出粗液; （2）蒸馏粗液以将其分解成沸点低于（甲基）丙烯酸多氟烷基酯和（甲基）丙烯酸多氟烷基酯的化合物B的化合物的化合物组A和沸点高于（甲基）丙烯酸多氟烷基酯; 和（3）在聚合抑制剂的存在下，从化合物组B中蒸馏纯化（甲基）丙烯酸多氟烷基酯的步骤。

9. 发明申请

US20050288528A1 Fluorinated adamantane and its derivatives 有权
公开(公告)号：US20050288528A1
公开(公告)日：2005-12-29
申请号：US11153438
申请日：2005-06-16
申请人： Takashi Okazoe , Kunio Watanabe , Masahiro Ito , Eisuke Murotani , Kazuya Oharu , Shu-zhong Wang , Taiki Hoshino , Kimiaki Kashiwagi
发明人： Takashi Okazoe , Kunio Watanabe , Masahiro Ito , Eisuke Murotani , Kazuya Oharu , Shu-zhong Wang , Taiki Hoshino , Kimiaki Kashiwagi
IPC分类号： C07C51/60 , C07C53/38 , C07C67/14 , C07C67/287 , C07C67/307
CPC分类号： C07C51/60 , C07C67/14 , C07C67/287 , C07C67/307 , C07C2603/74 , C07C55/40 , C07C53/50 , C07C69/54 , C07C69/63 , C07C69/708 , C07C69/753 , C07C69/734
摘要： The present invention provides a process A1 for producing a compound (5A), which comprises fluorinating a compound (3A-1) by liquid phase fluorination to a compound (4A-1), followed by a decomposition reaction of an ester bond; a process A2 for producing a compound (5A), which comprises fluorinating a compound (3A-2) by liquid phase fluorination to a compound (4A-2), followed by a decomposition reaction of an ester bond; and a process B for producing a compound (5B), which comprises fluorinating a compound (3B) by liquid phase fluorination to a compound (4B), followed by hydrolysis or alcoholysis. Further, the present invention provides a compound (5A) wherein n is 2 to 4, and a compound (5B) wherein n is 3 or 4. A(-CH2—OCO—R)n (3A-1) Af(-CF2—OCO—Rf)n (4A-1) A(-COOR)n (3A-2) Af(-COORf)n (4A-2) Af(-COF)n (5A) A(-OCO—R)n (3B) Af(-OCO—Rf)n (4B) Af(-OH)n (5B) provided that the carbon atom in adamantane to which —OCO—Rf is bonded, is a tertiary carbon atom, A is a n-valent group having n hydrogen atoms in adamantane converted to connecting bonds, R is a fluorinated monovalent organic group, n is an integer of from 1 to 4, Af is a group having at least one of hydrogen atoms in the group A substituted by a fluorine atom, and Rf is a fluorinated monovalent organic group.

10. 发明授权

US09206113B2 Fluorinated compound and fluorinated polymer 有权
标题翻译：氟化合物和氟化聚合物
公开(公告)号：US09206113B2
公开(公告)日：2015-12-08
申请号：US13412160
申请日：2012-03-05
申请人： Taiki Hoshino
发明人： Taiki Hoshino
IPC分类号： C07C69/70 , C07C69/653 , C07C69/65 , C08F120/22 , C08F220/22
CPC分类号： C07C69/653 , C07C69/65 , C08F120/22 , C08F220/22
摘要： To provide a fluorinated compound having an RF group with at most 6 carbon atoms, whereby a fluorinated polymer having a highly durable water/oil repellency can be produced, and an environmental load is little, and a fluorinated polymer having a highly durable water/oil repellency and presenting little environmental load, obtainable by polymerizing such a fluorinated compound. A fluorinated compound represented by the following formula (I) and its polymer: CH2═C(CH3)COO(CH2)nPhXCrF2r+1 (I) (in the formula (I), n is an integer of from 0 to 2, Ph is a phenylene group, X is a single bond or a C1-4 alkylene group containing an etheric oxygen atom, and r is an integer of from 2 to 6).
摘要翻译：为了提供具有至多6个碳原子的RF基团的氟化合物，由此可以制备具有高耐用斥水斥油性的氟化聚合物，并且环境负荷小，并且具有高耐久性水/油的氟化聚合物疏水性，并且通过聚合这种氟化化合物可以获得很小的环境负荷。由下式（I）表示的含氟化合物及其聚合物：CH2 = C（CH3）COO（CH2）nPhXCrF2r + 1（I）（式（I）中，n为0〜2的整数，Ph 是亚苯基，X是单键或含有醚性氧原子的C1-4亚烷基，r是2〜6的整数）。

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