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    • 7. 发明专利
    • FORMATION OF METALLIC THIN FILM
    • JPH0465385A
    • 1992-03-02
    • JP17755490
    • 1990-07-06
    • TSUBOCHI KAZUO
    • TSUBOUCHI KAZUOEKI KAZUYA
    • C30B1/02C30B29/02C30B29/52H01L21/3205H01L23/52
    • PURPOSE:To enhance resistance to migration characteristics by forming a non- single-crystal metallic film made of Al or Al alloy in contact with single-crystal metal of the same kind of metal and heat-treating the metallic film to make it single crystal. CONSTITUTION:An insulated film 2 such as SiO2 formed on a semiconductor base body 1 like single crystal Si by a sputtering method. Then an aperture part is formed in the insulated film 2 by reactive ionic etching, etc., and the surface of the base body 1 is exposed. Single crystal Al3 is selectively formed in the aperture part by regulating the surface temp. of the base body at the decomposition temp. of a raw material to 450 deg.C by an Al-CVD method wherein both gaseous alkylaluminum hydride such as dimethylaluminum hydride and gaseous H2 are utilized in this aperture part. Furthermore non-single crystal Al4 is formed on both single crystal Al3 and the insulated film 2 by a CVD method. Thereafter this non-single crystal Al4 is heat-treated by resistance heating, laser beam heating and electron beam heating, etc., at >=550 deg.C in the atmosphere of an individual such as H2 and Ar or of a gaseous mixture and made to single crystal. An insulated film 5 is formed thereon by a CVD method, etc. This method is applicable even to Al alloy in addition to Al.
    • 8. 发明专利
    • REFLECTED ELECTRON BEAM DIFFRACTION APPARATUS
    • JPH02216040A
    • 1990-08-28
    • JP3714189
    • 1989-02-16
    • MIKOSHIBA NOBUOOMI TADAHIROTSUBOCHI KAZUOEKI KAZUYA
    • MIKOSHIBA NOBUOOMI TADAHIROTSUBOUCHI KAZUOEKI KAZUYA
    • G01N23/225G01N23/207
    • PURPOSE:To measure the distribution of individual crystals by arranging a reflected electron beam diffraction electron gun, a photomultiplier and an arithmetic circuit to permits the determination of crystal bearings in faces thereof parallel and vertical to the surface of a sample. CONSTITUTION:Diffraction pattern is formed on a fluorescent screen 6 by a diffraction electron beam 5 resulting from an electron beam 4 emitted from a reflected electron beam diffraction electron gun 1. A signal from a diffraction spot is introduced to photomultipliers 10-12 through optical fibers 7-9 to be amplified and computed with an arithmetic circuit 13. Then, with the circuit 13, intensities of the diffraction spots undergo a multiplication processing by an optional constant and a addition/subtraction processing between the intensities of the diffraction spots subjected to the multiplication processing. A signal 14 as the results of the arithmetic processing is inputted into a CRT 15 as brightness signal. Then, a diffraction intensity image from the surface of a sample is displayed on the CRT 15 by a scan signal synchronizing a scan signal 16 of the electron beam from the electron gun 1. Thus, the fibers 7-9 are disposed under vacuum and a allowed to select optional diffraction spots mechanically.