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    • 4. 发明专利
    • CRYSTAL FOR SOLID-STATE LASER
    • JPH01241883A
    • 1989-09-26
    • JP6817988
    • 1988-03-24
    • TOSHIBA CORP
    • FUKUDA KATSUYOSHITERAJIMA KAZUTAKA
    • H01S3/16
    • PURPOSE:To provide an excellent crystal for a solid state laser allowing easy formation of the crystal and small variation in its composition by composing the crystal of oxide single crystal of neodymium and boron. CONSTITUTION:Nd2O5 and B2O3 are mixed as materials at 1:3 of molar ratio, and approx. 200g of the mixture is contained in a platinum crucible 3. It is then heated to 1200 deg.C, and sufficiently heated for 10 hours to be melted. Then, melt 7 is set to 1155 deg.C, a seed crystal 9 made of NdB3O6 is brought into contact with the liquid, cooled at a rate of 1 deg.C per one hour, and the crystal is then pulled up. In this case, the crystal 9 is rotated at 100rpm, and the pulling speed is 1mm per one hour. Oxygen gas is introduced from a gas tube 11 into a furnace during this period. NdB3O6 crystal have almost no crack and no variation in the composition, is pale blue green transparent, cut to a rod shape having 3mm of diameter and 3cm of length, and excited by a halogen lamp, thereby providing a laser light having 1.06mum of wavelength.
    • 7. 发明专利
    • APPARATUS FOR PRODUCING SEMICONDUCTOR SINGLE CRYSTAL
    • JPS6472985A
    • 1989-03-17
    • JP22861287
    • 1987-09-14
    • TOSHIBA CORP
    • FUJITA HIROMOTOFUKUDA KATSUYOSHINISHIO JOSHITERAJIMA KAZUTAKA
    • C30B15/00C30B15/10H01L21/208
    • PURPOSE:To prevent the failure, etc., of a crucible during the transportation thereof and to obtain a large-sized single crystal with good workability by fastening the crucible by means of a furnace member enclosing the crucible to integrate the crucible and further, providing holding parts for transportation to the furnace member. CONSTITUTION:The crucible 11 and a supporting base 12 which supports the crucible 11 are fastened and integrated by a reinforcing material 13 and thread working and further, the holding parts for transportation, for example, two holes 13' are provided to the crucible. A raw material is housed into such crucible 11 and the crucible is disposed in a high-pressure vessel 14. After the inside of the vessel is pressurized by gaseous Ar, the crucible 11 is heated by a heater 15 which coaxially encloses the crucible. A raw material 16 is thus obtd. A seed crystal 17 is then lowered and is held in contact with he melt 16; thereafter, the seed crystal 17 is pulled up while the crystal is kept rotated by which the single crystal is obtd. The supporting base 12 which houses the crucible 11 and is assembled with the reinforcing material 13 is taken in this state out of the high-pressure vessel 14 after the end of the production of the single crystal. The content remaining in the crucible 11 is taken out and the reinforcing material 13 is removed. The crucible 11 is taken out of the supporting base 12 and is cleaned.
    • 10. 发明专利
    • HEATER FOR PRODUCTION OF SINGLE CRYSTAL
    • JPS63176391A
    • 1988-07-20
    • JP394787
    • 1987-01-13
    • TOSHIBA CORP
    • NISHIO JOSHIKATSUMATA TORUFUKUDA KATSUYOSHITERAJIMA KAZUTAKA
    • C30B15/14C30B27/02
    • PURPOSE:To enable the production of a single crystal having high uniformity and free from growth stripes, in high yield, preventing the formation of twins and polycrystals, by using a heater having a specific structure, thereby improving the heat-generation uniformity of the heater. CONSTITUTION:The objective heater for the production of a single crystal is composed of a side-wall part 11 coaxially encircling a crucible containing a raw material for single crystal, a base part 12 supporting the side-wall part 11 and an electrode-attaching part 14 supporting the base part 12 and connected to a power source electrode. The above three parts are integrated. Plural slits 15 are applied to the side-wall part 11 in a manner that the wall forms a continuous heater extending from an electrode to the other electrode of the above power source electrodes. The base part 12 is connected to the side-wall part 11 in a plane in which the electrode is connected to the electrode attaching part 14, in a direction having an angle of 45-90 deg. from the line (A-A') connecting the center of an electrode rod and that of the other electrode rod of the above power source electrodes taking the center of axis of the crucible and the side- wall part 11 as the center of the angle and in a plane perpendicular to the above plane.