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    • 3. 发明专利
    • PURIFICATION OF CARBON-GRAPHITE MATERIAL
    • JPH02225312A
    • 1990-09-07
    • JP1108889
    • 1989-01-20
    • TOSHIBA CERAMICS CO
    • NISHIMURA MASANORIKATO SHIGEONONAMI HIDEMITSUTAN NOBUYUKI
    • C01B31/04H01L21/208H01L21/22
    • PURPOSE:To unnecessitate to again subject a carbon.graphite material to a degasifying treatment on the use of the carbon.graphite material in a semiconductor production process and enable to improve the luminous characteristics of the compound semiconductor on the employment of the carbon.graphite material in a liquid phase epitaxy by consistently applying an impurity-removing treatment, a hydrogen baking treatment and a vacuum degasification treatment to the carbon.graphite material. CONSTITUTION:A carbon.graphite material is subjected to an impurity-removing treatment using a halogen gas or a gas containing the halogen at a high temperature, to a hydrogen baking treatment at a high temperature and subsequently to a vacuum degasification treatment at a high temperature. Since the impurity- removing treatment, the hydrogen baking treatment and the vacuum degasification treatment are consistently carried out in this order and the hydrogen baking treatment is performed prior to the vacuum degasification treatment, the rate of oxygen compounds in the released gas can be reduced by the treatments at the relatively low temperature and vacuum degree.