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1. 发明授权

US5210216A Calixarene and oxacalixarene derivatives and use thereof of sequestration metals 失效
标题翻译：杯芳烃和恶唑烷衍生物及其螯合金属的用途
公开(公告)号：US5210216A
公开(公告)日：1993-05-11
申请号：US625573
申请日：1990-12-10
申请人： Stephen J. Harris , John Guthrie , Maureen MacManus , Ciaran McArdle , Michael A. McKervey
发明人： Stephen J. Harris , John Guthrie , Maureen MacManus , Ciaran McArdle , Michael A. McKervey
IPC分类号： C02F1/26 , C02F1/68 , C07C59/70 , C07C205/25 , C07C205/37 , C07C217/24 , C07C235/20 , C07C245/08 , C07C251/38 , C07C251/76 , C07C323/12 , C07C327/44 , C07D213/30 , C07D235/12 , C07D295/185 , C07D313/00 , C07D321/00 , C07D323/00 , C07F7/18 , C08F8/00 , C08G18/32 , C08G18/54 , C08G75/02 , C08G77/38 , C08G85/00 , C08K5/15 , C09J4/00
CPC分类号： C07D213/30 , C02F1/26 , C02F1/683 , C07C205/25 , C07C205/37 , C07C217/24 , C07C235/20 , C07C245/08 , C07C251/38 , C07C251/76 , C07C323/12 , C07C327/44 , C07C59/70 , C07D235/12 , C07D295/185 , C07D313/00 , C07D321/00 , C07D323/00 , C07F7/1836 , C08F8/00 , C08G18/3215 , C08G18/542 , C08G75/02 , C08G77/38 , C08G85/00 , C08K5/15 , C09J4/00 , C07C2103/92
摘要： Calixarene and oxacalixarene derivatives of the formula IV: ##STR1## wherein m'+m"=0-8n=0-8m'.gtoreq.1/2(m'+m")3.ltoreq.m'+m"+n.ltoreq.8if n=0, m'+m".gtoreq.4R.sup.3 is H, halogen, or hydrocarbyl, aryl, hydrocarbylaryl or a substituted derivative thereof and R.sup.3 may be the same or different on each aryl group;R.sup.15 is H or hydrocarbyl, aryl, hydrocarbylaryl or a substituted derivative thereof;X is selected from ##STR2## wherein R.sup.7 and R.sup.8 which may be the same or different are H or hydrocarbyl (including a cycloaliphatic ring formed by R.sup.7 and R.sup.8 together), aryl, hydrocarbylaryl or a substituted derivative thereof; R.sup.9 is --OH, --NH.sub.2, --NHC(O)NH.sub.2 or --NHAr, wherein Ar is aryl or a substituted derivative thereof,n' is 0 or 1.Use of the compounds for sequestration of metals is also described.
摘要翻译：式IV的杯芳烃和恶唑烷衍生物：其中m'+ m“= 0-8 n = 0-8 m'/ = 1/2（m'+ m”）3 = 如果n = 0，m + + m + n，则n'= n，R 3是H，卤素或烃基，芳基，烃基芳基或其取代的衍生物，并且R 3可以相同或每个芳基不同; R 15为H或烃基，芳基，烃基芳基或其取代衍生物; （A）（CH2）n'SR7（B）其中可以相同或不同的R 7和R 8是H或烃基（包括环脂族基）由R 7和R 8一起形成的环），芳基，烃基芳基或其取代的衍生物; R9是-OH，-NH2，-NHC（O）NH2或-NHAr，其中Ar是芳基或其取代衍生物，n'是0或1.还描述了化合物螯合金属的用途。

2. 发明授权

US5216185A Polymerizable calixarene and oxacalixarene derivatives, polymers thereof and use of such derivatives and polymers for sequestration of metals 失效
标题翻译：可聚合的氯仿和氧化二烯衍生物，其聚合物和这些衍生物和聚合物用于金属排序的用途
公开(公告)号：US5216185A
公开(公告)日：1993-06-01
申请号：US625575
申请日：1990-12-10
申请人： Stephen J. Harris , John Guthrie , Maureen MacManus , Michael A. McKervey
发明人： Stephen J. Harris , John Guthrie , Maureen MacManus , Michael A. McKervey
IPC分类号： C07C69/712 , C07C217/18 , C07C323/12 , C07D323/00 , C08F20/26 , C08F20/30 , C08F220/30 , C09K3/00
CPC分类号： C07C69/712 , C07D323/00 , C08F20/30
摘要： Polymerizable calixarene and oxacalixarene derivates wherein at least one aryl group of the macrocyclic ring has a phenolic side chain of the formula VII: ##STR1## wherein Z is a group containing an acrylate or methacrylate functional group. Linear polymers may be formed from these compounds by free radical polymerization at the (meth)acrylate group. Such compounds and their polymers are capable of sequestering metals.

3. 发明授权

US5132345A Ion-selective electrodes 失效
标题翻译：离子选择电极
公开(公告)号：US5132345A
公开(公告)日：1992-07-21
申请号：US624623
申请日：1990-12-10
申请人： Stephen J. Harris , Michael A. McKervey , Gyula Svehla , Dermot Diamond
发明人： Stephen J. Harris , Michael A. McKervey , Gyula Svehla , Dermot Diamond
IPC分类号： G01N27/333
CPC分类号： G01N27/333
摘要： An ion-selective polymeric membrane for an electrochemical sensor for use in analytical chemistry, comprisinga) a supporting matrix e.g. of PVC, andb) an ionophore selected from calixarene or oxacalixarene derivatives of the formula IV ##STR1## wherein n+m=3-8;m=0-8;n=0-8;a, which may be the same or different on each aryl group, is 0 or 1;R.sup.2 is alkyl, aryl, alkaryl, alkoxy, alkoxyalkoxy, aryloxy, alkaryloxy, alicyclic, alkylthio, arylthio, alkarylthio, or a substituted derivative thereof;R.sup.3 is --H, alkyl or alkenyl;X is --OH or a group containing an acrylate or methacrylate functional group;provided that when X is --OH, n is at least 1/2(n+m);and provided that when m=0, n=4, a=0 and R.sup.3 is alkyl or allyl, R.sup.2 is not alkoxy having 4 or more carbon atoms in the alkyl group;and provided that when m=0, n=4, a=0 and R.sup.3 is t-butyl, R.sup.2 is not methoxy or ethoxy;or of the formula V ##STR2## wherein R.sup.4 is alkyl; or polymers of those compounds of the formula IV in which X is a group containing an acrylate or methacrylate group.New compounds in which R.sup.2 is --SCH.sub.2 CH.sub.3 are described.Selectivity coefficients and slope measurements are given for the ionophores in PVC electrodes which are selective for sodium, potassium and caesium.
摘要翻译：一种用于分析化学中的用于电化学传感器的离子选择性聚合物膜，包括：a）的PVC，和b）选自式IV的杯芳烃或氧杂七环芳烃衍生物的离子载体，其中n + m = 3-8; m = 0-8; n = 0-8; a在每个芳基上可以相同或不同，为0或1; R2是烷基，芳基，烷芳基，烷氧基，烷氧基烷氧基，芳氧基，烷氧基，脂环族，烷硫基，芳硫基，烷芳硫基或其取代衍生物。 R3是-H，烷基或烯基; X是-OH或含有丙烯酸酯或甲基丙烯酸酯官能团的基团; 条件是当X为-OH时，n为至少1/2（n + m）; 并且条件是当m = 0时，n = 4，a = 0和R3是烷基或烯丙基，R2不是烷基中具有4个或更多个碳原子的烷氧基; 并且条件是当m = 0时，n = 4，a = 0和R3是叔丁基，R 2不是甲氧基或乙氧基; 或其中R 4是烷基的式V V 或其中X为含丙烯酸酯或甲基丙烯酸酯基团的式Ⅳ化合物的聚合物。描述了其中R2是-SCH2CH3的新化合物。对于对钠，钾和铯有选择性的PVC电极中的离子载体，给出了选择性系数和斜率测量。

4. 发明授权

US5599913A Chromoionophores, optical sensors containing them and a method for determining the presence of alkali metal cations or of a base 失效
标题翻译：含铬荧光体，含有它们的光学传感器和用于测定碱金属阳离子或碱的存在的方法
公开(公告)号：US5599913A
公开(公告)日：1997-02-04
申请号：US381912
申请日：1995-03-28
申请人： Stephen J. Harris , Dermot Diamond , Michael A. McKervey
发明人： Stephen J. Harris , Dermot Diamond , Michael A. McKervey
IPC分类号： C07C205/42 , C07C205/43 , C07C205/45 , C07C245/08 , G01N31/22
CPC分类号： C07C205/43 , C07C205/42 , C07C205/45 , C07C245/08 , C07C2103/92 , Y10S435/808 , Y10T436/11 , Y10T436/173845 , Y10T436/174614
摘要： New chromoionophores of the formula IV ##STR1## wherein a=0-3, b=0 or 1, c =0 or 1, x=0 or 1, y=0 or 1, z=0 or 1,R', which may be the same or different in each aryl group, is H, halogen, hydrocarbyl, aryl, hydrocarbylaryl or a substituted derivative thereof;R, which may be the same or different, is hydrocarbyl, aryl, hydrocarbylaryl, or a substituted derivative thereofare useful in optical sensors or colourmetric reagents for clinical use particularly for lithium, When complexed with lithium, the chromoionophores of the invention and other calixarene derivatives can be used for detecting amines, particularly trimethylamine, as an indicator of fish spoilage.
摘要翻译： PCT No.PCT / IE93 / 00046 Sec。 371日期：1995年3月28日 102（e）1995年3月28日PCT PCT 1993年8月6日PCT公布。公开号WO94 / 04483 日期1994年3月3日公式IV的新的铬离子荧光素其中a = 0-3，b = 0或1，c = 0或1，x = 0或1，y = 0或1，z = 0或1，R'在每个芳基中可以相同或不同，为H，卤素，烃基，芳基，烃基芳基或其取代的衍生物; R可以相同或不同，是烃基，芳基，烃基芳基或其取代的衍生物，可用于特别用于锂的临床用光学传感器或色度试剂中。当与锂络合时，本发明的染色体和其他杯芳烃衍生物可用于检测胺，特别是三甲胺，作为鱼类腐败的指标。

5. 发明授权

US4957960A Encapsulating compositions 失效
标题翻译：封装组合物
公开(公告)号：US4957960A
公开(公告)日：1990-09-18
申请号：US472596
申请日：1990-01-30
申请人： Stephen J. Harris , John G. Woods , John M. Rooney , Marueen G. MacManus , John Guthrie
发明人： Stephen J. Harris , John G. Woods , John M. Rooney , Marueen G. MacManus , John Guthrie
IPC分类号： C08G59/00 , C08K5/00 , C08K5/06 , C08K5/07 , C08K5/15 , C08K5/16 , C08K5/20 , C08K5/5419 , C08K5/549 , C08L63/00 , C08L71/00 , C08L83/04 , C08L101/00 , H01B3/40 , H01L23/29 , H01L23/31
CPC分类号： H01B3/40 , C08K5/0008 , C08K5/06 , C08K5/15 , C08K5/20 , C08K5/549
摘要： An encapsulating composition for electronic devices comprises a curable material such as a silicone resin and an ion scavenger compound selected from certain calixarene or oxacalixarene compounds in which at least half of the phenolic groups have been substituted by specific groups and certain silacrown compounds. Exemplary ion scavenger compounds include ##STR1## the tetraethyl acetate of 7, 13, 19, 25-tetra-tertbutyl-27, 28, 29, 30-tetrahydroxy-2,3-dihomo-3-oxacalix-4-arene and 1,1-dimethasila-17-crown-6.

6. 发明授权

US5043415A Nitrogen-containing oxacalixarene and calixarene derivatives, polymers including groups related to such derivatives, and use of such compounds 失效
标题翻译：含氮氧杂环芳烃和杯芳烃衍生物，包括与这种衍生物有关的基团的聚合物，以及这些化合物的用途
公开(公告)号：US5043415A
公开(公告)日：1991-08-27
申请号：US248874
申请日：1988-09-23
申请人： Stephen J. Harris , Maureen G. MacManus , John Guthrie
发明人： Stephen J. Harris , Maureen G. MacManus , John Guthrie
IPC分类号： C07D313/00 , C07D321/00 , C07D323/00
CPC分类号： C07D321/00 , C07D313/00 , C07D323/00
摘要： The application describes nitrogen-containing an oxacalixarene or calixarene derivative of formula I: ##STR1## wherein m'+m"=0-8n=0-8m'.gtoreq.1/2(m'+M")3.ltoreq.m'+m"+n.ltoreq.8if n=0, m'+m".gtoreq.4R.sup.3 is H, halogen, or hydrocarbyl, aryl, hydrocarbylaryl or a substituted derivative thereof and R.sup.3 may be the same or different on each aryl group;R.sup.1 and R.sup.15 which may be the same or different are H or hydrocarbyl, aryl, hydrocarbylaryl or a substituted derivative thereof;R.sup.2 is selected from:R.sup.4 which is H, or hydrocarbyl, aryl, hydrocarbylaryl or a substituted derivative thereof, ##STR2## wherein R.sup.5 and R.sup.6 which may be the same or different are H, or hydrocarbyl, aryl, hydrocarbylaryl, or a substituted derivative thereof,-OR.sup.1, wherein R.sup.1 is as defined aboveand R.sup.17 which is a residue of a hydrocarbyl, aryl, or hydrocarbylaryl group or of a substituted derivative thereof providing a bond to another oxacalixarene or calixarene derivative of formula I wherein R.sup.2 is R.sup.17.The derivatives may be polymer-bound. Use of the derivatives for sequestration of metals is also described.

7. 发明授权

US4908399A Encapsulating compositions 失效
标题翻译：封装组合物
公开(公告)号：US4908399A
公开(公告)日：1990-03-13
申请号：US270136
申请日：1988-11-14
申请人： Stephen J. Harris , Maureen G. MacManus , John Guthrie
发明人： Stephen J. Harris , Maureen G. MacManus , John Guthrie
IPC分类号： C08G59/00 , C08K5/00 , C08K5/06 , C08K5/07 , C08K5/15 , C08K5/16 , C08K5/20 , C08K5/5419 , C08K5/549 , C08L63/00 , C08L71/00 , C08L83/04 , C08L101/00 , H01B3/40 , H01L23/29 , H01L23/31
CPC分类号： H01B3/40 , C08K5/0008 , C08K5/06 , C08K5/15 , C08K5/20 , C08K5/549
摘要： An encapsulating composition for electronic devices comprises a curable material such as an epoxy resin and an ion scavenger compound selected from certain calixarene or oxycalixarene compounds in which at least half of the phenolic groups have been substituted by specific groups and certain silacrown compounds. Exemplary ion scavenger compounds include ##STR1## the tetraethyl acetate of 7, 13, 19, 25-tetra-tertbutyl-27, 28, 29, 30-tetrahydroxy-2,3-dihomo-3-oxacalix-4-arene and 1,1-dimethasila-17-crown-6.
摘要翻译：用于电子器件的封装组合物包括可固化材料，例如环氧树脂和选自某些杯芳烃或氧化肟化合物的离子清除剂化合物，其中至少一半的酚基已经被特定基团取代并且某些硅氮烯化合物。示例性的离子清除剂化合物包括7,13,19,25-四叔丁基-27,28,29,30-四羟基-2,3-二氧-3-氧杂环戊烯-4-芳烃的乙酸四乙酯， 1-dimethasila-17-crown-6。

8. 发明申请

US20120301790A1 LITHIUM ION SECONDARY BATTERY ELECTRODE AND METHOD OF FORMING SAME 有权
标题翻译：锂离子二次电池电极及其形成方法
公开(公告)号：US20120301790A1
公开(公告)日：2012-11-29
申请号：US13114458
申请日：2011-05-24
申请人： Xinran Xiao , Adam T. Timmons , Stephen J. Harris
发明人： Xinran Xiao , Adam T. Timmons , Stephen J. Harris
IPC分类号： H01M4/74 , H01M4/26 , B05D5/12
CPC分类号： H01M4/13 , H01M4/0404 , H01M4/139 , H01M4/625 , H01M10/0525 , H01M2220/20 , Y02E60/122 , Y02T10/7011 , Y10S977/742 , Y10S977/762 , Y10S977/948 , Y10T29/49115
摘要： A method of forming an electrode of a lithium ion secondary battery includes combining a binder and active particles to form a mixture, coating a surface with the mixture to form a coated article, translating the article along a first plane, cutting a first plurality of carbon fibers, each having a first average length, to form a second plurality of carbon fibers, each having a longitudinal axis and a second average length that is shorter than the first average length, inserting the second plurality of fibers into the mixture layer so that the longitudinal axis of each of at least a portion of the second plurality of fibers is not parallel to the first plane to form a preform, wherein the second plurality of fibers forms a truss structure disposed in three dimensions within the mixture layer, and heating the preform to form the electrode. An electrode is also disclosed.
摘要翻译：形成锂离子二次电池的电极的方法包括将粘合剂和活性颗粒组合以形成混合物，用混合物涂覆表面以形成涂布制品，沿着第一平面平移物品，切割第一多个碳纤维，每个具有第一平均长度，以形成第二多个碳纤维，每个碳纤维具有比第一平均长度短的纵向轴线和第二平均长度，将第二多个纤维插入混合物层中，使得所述第二多根纤维的至少一部分中的每一个的纵向轴线不平行于所述第一平面以形成预成型件，其中所述第二多根纤维形成三维地设置在所述混合物层内的桁架结构，并且加热所述预制件以形成电极。还公开了一种电极。

9. 发明授权

US5262645A Sensor for measuring alcohol content of alcohol gasoline fuel mixtures 失效
标题翻译：用于测量酒精汽油燃料混合物的酒精含量的传感器
公开(公告)号：US5262645A
公开(公告)日：1993-11-16
申请号：US754475
申请日：1991-09-03
申请人： David K. Lambert , Stephen J. Harris , Stephen J. Swarin
发明人： David K. Lambert , Stephen J. Harris , Stephen J. Swarin
IPC分类号： G01N21/31 , G01N21/35 , G01N33/28
CPC分类号： G01N21/314 , G01N21/3504 , G01N21/3577 , G01N21/359 , G01N33/2852
摘要： An alcohol sensing device is provided for determining the alcohol content within an alcohol/gasoline fuel mixture provided to an internal combustion engine. The sensing device uses infrared spectrometry measuring techniques. The infrared sensing device determines the ratio of light absorption by the alcohol/gasoline mixture at two discrete wavelengths within the near-infrared spectrum. The two particular wavelengths of interest are preferably chosen so that at one of the infrared wavelengths, alcohol is strongly absorbing while the gasoline exhibits very little absorption, and at the second wavelength both the alcohol and the gasoline exhibit are essentially non-absorbing. A light beam is transmitted through the alcohol/gasoline fuel mixture such that the two discrete wavelengths traverse the same optical path. A first and second detector are adjacently disposed so as to receive the emitted light from each wavelength after their transmission through the alcohol/gasoline fuel mixture. A third and fourth detector are adjacently disposed in proximity to the first and second detectors for sensing the drift in ambient temperatures corresponding to the first and second detectors. Once the signals corresponding to the two wavelengths are obtained and the signals corresponding to the ambient temperatures are factored out, the ratio of the absorbances by the fuel mixture at both wavelengths is computed. From this ratio and the fuel temperature the concentration of alcohol in the fuel is determined.
摘要翻译：提供了一种酒精感测装置，用于确定提供给内燃机的醇/汽油燃料混合物中的醇含量。感测装置使用红外光谱测量技术。红外感测装置确定近红外光谱中两个离散波长下的醇/汽油混合物的光吸收率。优选选择感兴趣的两个特定波长，使得在红外波长的一个处，醇是强吸收的，而汽油表现出非常少的吸收，而在第二波长下，醇和汽油表现出基本上不吸收。光束通过酒精/汽油燃料混合物传播，使得两个离散的波长穿过相同的光路。相邻地设置第一和第二检测器，以便在透过酒精/汽油燃料混合物之后接收来自每个波长的发射光。第三和第四检测器相邻设置在第一和第二检测器附近，用于感测对应于第一和第二检测器的环境温度的漂移。一旦获得对应于两个波长的信号，并且将与环境温度相对应的信号进行分解，则计算两个波长处的燃料混合物的吸光度比。从该比率和燃料温度确定燃料中的醇的浓度。

10. 发明授权

US4992509A Polyvinyl acetal resin, use thereof as an adhesion promoting additive, method of producing same, and adhesive composition comprising same 失效
标题翻译：聚乙烯醇缩醛树脂，其作为粘合促进添加剂的用途，其制造方法以及包含其的粘合剂组合物
公开(公告)号：US4992509A
公开(公告)日：1991-02-12
申请号：US252831
申请日：1988-10-03
申请人： Stephen J. Harris
发明人： Stephen J. Harris
IPC分类号： C08F8/28 , C08F8/14
CPC分类号： C08F8/14 , C08F2810/30
摘要： Polyvinyl acetal resin, use thereof as an adhesion promoting additive, method of producing same, and adhesive composition comprising sameAn acrylate- or methacrylate-substituted polyvinyl acetal resin of formula I: ##STR1## wherein the weight percentages of the X, Y and Z groups are variable, R is a hydrogen atom or an alkyl group, andR.sub.1 is hydrogen atom or a methyl group, is described.The resin of formula I is produced by acrylating or methacrylating a polyvinyl acetal resin of formula II: ##STR2## in which the weight percentages of the X', Y' and Z' groups are variable, particularly in the range 68 to 88% X, 6 to 19% Y' and 1 to 26% Z.The compounds of formula I are used to promote adhesion of acrylate or methacrylate ester based adhesive compositions to polyester plastic substrates.

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