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1. 发明授权

US5466397A Nonlinear optically active pyrazolines and polymeric compositions containing moieties derived therefrom 失效
标题翻译：非线性光学活性吡唑啉和含有衍生自其的部分的聚合物组合物
公开(公告)号：US5466397A
公开(公告)日：1995-11-14
申请号：US159010
申请日：1993-11-29
申请人： Stephen E. Bales , David J. Brennan , Robert J. Gulotty, Jr. , Muthiah N. Inbasekaran , Michael N. Mang , Mark D. Newsham
发明人： Stephen E. Bales , David J. Brennan , Robert J. Gulotty, Jr. , Muthiah N. Inbasekaran , Michael N. Mang , Mark D. Newsham
IPC分类号： C07D231/06 , C07D303/22 , C07D405/14 , C08G59/06 , C08G59/26 , C08G59/62 , C08G64/12 , G02F1/361 , F21V9/00 , C08F2/46
CPC分类号： C07D231/06 , C07D303/22 , C07D405/14 , C08G59/066 , C08G59/26 , C08G59/621 , C08G64/12 , G02F1/3612 , G02F1/3616
摘要： Disclosed are compounds containing substituted pyrazoline which exhibit nonlinear optical activity on orientation and to oriented polymeric compositions comprising moieties derived therefrom in the backbone of the polymer. Also disclosed are the processes for making the oriented polymeric composition of the invention.
摘要翻译：公开了含有取代的吡唑啉的化合物，其在取向上表现出非线性光学活性，并且包含在聚合物的主链中由其衍生的部分的定向聚合物组合物。还公开了制备本发明的取向聚合物组合物的方法。

2. 发明授权

US6051294A Heat-resistant hydroxy-functional polyethers as thermoplastic barrier resins 失效
标题翻译：耐热羟基官能聚醚作为热塑性阻隔树脂
公开(公告)号：US6051294A
公开(公告)日：2000-04-18
申请号：US21058
申请日：1998-02-09
申请人： Jerry E. White , H. Craig Silvis , Stephen E. Bales , Michael N. Mang , Muthiah N. Inbasekaran
发明人： Jerry E. White , H. Craig Silvis , Stephen E. Bales , Michael N. Mang , Muthiah N. Inbasekaran
IPC分类号： C08L71/00 , B65B55/00
CPC分类号： C08L71/00 , Y10T428/1352
摘要： Hydroxy-functional polyethers having a "cardo" diphenylene group in their backbones are prepared by contacting at least one dinucleophilic monomer with at least one dtglycidyl ether of a cardo bisphenol, such as bis(hydroxyphenyl)fluorene, phenolphthalein, or phenolphthalimidine or a substituted cardo bisphenol, such as a substituted bis(hydroxyphenyl)fluorene, a substituted phenolphthalein or a substituted phenolphthalimidine, under conditions sufficient to cause the nucleophillo moieties of the dinucleophilic monomer to react with epoxy moieties to form a polymer backbone containing pendant hydroxy moieties and ether, imino, amino, sulfonamido or ester linkages. These polyethers possess a combination of high barrier to oxygen transmission (i.e., oxygen transmission rate less than 10.0 cm.sup.3 -mil/100 in.sup.2 -atm-day to oxygen) and high heat resistance (i.e., Tg above 120.degree. C.). These polyethers are suitable for use in the manufacture of retort-sterilizable packaging materials exhibiting high barrier to oxygen.
摘要翻译：在其主链中具有“cardo”二亚苯基的羟基官能的聚醚通过使至少一种双亲性单体与双酚（如双（羟基苯基）芴，酚酞或苯酚苯并咪唑或取代的cardo双酚的至少一种dt缩水甘油醚双酚，例如取代的双（羟基苯基）芴，取代的酚酞或取代的苯酚苯酞，在足以使双亲单体的亲核部分与环氧部分反应形成含有侧羟基部分和醚的聚合物主链的条件下，亚氨基，氨基，亚磺酰氨基或酯键。这些聚醚具有高的透氧阻隔性（氧气透过率低于氧气的氧气渗透速度小于10.0立方厘米/ 100英寸/天）和高耐热性（即高于120℃的Tg）。这些聚醚适用于制造显示出高阻隔氧的蒸煮灭菌包装材料。

3. 发明授权

US5814373A Heat-resistant hydroxy-functional polyethers as thermoplastic barrier resins 失效
标题翻译：耐热羟基官能聚醚作为热塑性阻隔树脂
公开(公告)号：US5814373A
公开(公告)日：1998-09-29
申请号：US131110
申请日：1993-10-01
申请人： Jerry E. White , H. Craig Silvis , Stephen E. Bales , Michael N. Mang , Muthiah N. Inbasekaran
发明人： Jerry E. White , H. Craig Silvis , Stephen E. Bales , Michael N. Mang , Muthiah N. Inbasekaran
IPC分类号： C08G59/06 , C08G59/62 , C08L71/00 , B65B55/00
CPC分类号： C08G59/066 , C08G59/621 , C08L71/00 , Y10T428/1307 , Y10T428/1341 , Y10T428/1379 , Y10T428/1383
摘要： Hydroxy-functional polyethers having a "cardo" diphenylene group in their backbones are prepared by contacting at least one dinucleophilic monomer with at least one diglycidyl ether of a cardo bisphenol, such as bis(hydroxyphenyl)fluorene, phenolphthalein, or phenolphthalimidine or a substituted cardo bisphenol, such as a substituted bis(hydroxyphenyl)fluorene, a substituted phenolphthalein or a substituted phenolphthalimidine, under conditions sufficient to cause the nucleophilic moieties of the dinucleophilic monomer to react with epoxy moieties to form a polymer backbone containing pendant hydroxy moieties and ether, imino, amino, sulfonamido or ester linkages. These polyethers possess a combination of high barrier to oxygen transmission (i.e., oxygen transmission rate less than 10.0 cm.sup.3 -mil/100 in.sup.2 -atm-day to oxygen) and high heat resistance (i.e., Tg above 120.degree. C.). These polyethers are suitable for use in the manufacture of retort-sterilizable packaging materials exhibiting high barrier to oxygen.
摘要翻译：在其主链中具有“cardo”二亚苯基的羟基官能聚醚通过使至少一种亲核性单体与双酚（如双（羟基苯基）芴，酚酞或苯酚苯并咪唑或取代的cardo双酚的至少一种二缩水甘油醚双酚，例如取代的双（羟基苯基）芴，取代的酚酞或取代的苯酚苯酞，在足以使亲核单体的亲核部分与环氧部分反应形成含有侧羟基部分和醚的聚合物主链的条件下，亚氨基，氨基，亚磺酰氨基或酯键。这些聚醚具有高的透氧阻隔性（氧气透过率低于氧气的氧气渗透速度小于10.0立方厘米/ 100英寸/天）和高耐热性（即高于120℃的Tg）。这些聚醚适用于制造显示出高阻隔氧的蒸煮灭菌包装材料。

4. 发明授权

US5208299A Nonlinear optical arylhydrazones and nonlinear optical polymers thereof 失效
标题翻译：非线性光学芳基腙及其非线性光学聚合物
公开(公告)号：US5208299A
公开(公告)日：1993-05-04
申请号：US866400
申请日：1992-04-10
申请人： Stephen E. Bales , David J. Brennan , Robert J. Gulotty , Anthony P. Haag , Muthiah N. Inbasekaran
发明人： Stephen E. Bales , David J. Brennan , Robert J. Gulotty , Anthony P. Haag , Muthiah N. Inbasekaran
IPC分类号： G02F1/35 , C07C251/86 , C07C255/66 , C07C317/32 , C07C317/34 , C07C323/48 , C07D277/82 , C08G59/62 , C08G63/68 , C08G63/685 , C08G64/00 , C08G64/08 , C08G64/12 , C08G65/00 , C08G65/40 , C08G73/00 , C08J5/18 , C08L67/02 , C08L69/00 , C08L71/00 , C08L101/00 , D01F6/92 , G02F1/355 , G02F1/361
CPC分类号： C07C317/32 , C07C251/86 , C07C255/66 , C07C317/34 , C07C323/48 , C07D277/82 , C08G59/621 , C08G63/68 , C08G63/685 , C08G64/08 , C08G65/4006 , C08G65/4031 , G02F1/3611 , G02F1/3613 , G02F1/3614 , G02F1/3616
摘要： The present invention relates to nonlinear optical material comprising nonlinear optical dihydroxy arylhydrazones and to nonlinear optical materials comprising compositions containing at least one divalent moiety of nonlinear optical arylhydrazones. The present invention also relates to polyesters, polyestercarbonates, polycarbonates, polyethers, and poly(hydroxy ether) polymers, incorporating the dihydroxy arylhydrazone as recurring divalent moieties in the backbone of the polymer. The polymeric compositions of the present invention have high glass transition temperatures and exhibit stable nonlinear optical activity at high temperatures over a period of time.
摘要翻译：本发明涉及包含非线性光学二羟基芳基腙的非线性光学材料和包含含有非线性光学芳基腙的至少一个二价部分的组合物的非线性光学材料。本发明还涉及在聚合物主链中掺入二羟基芳基腙作为重复的二价部分的聚酯，聚酯碳酸酯，聚碳酸酯，聚醚和聚（羟基醚）聚合物。本发明的聚合物组合物具有高玻璃化转变温度，并且在一段时间内在高温下表现出稳定的非线性光学活性。

5. 发明授权

US5447960A Fungicidal use of phenolic aromatic compounds 失效
标题翻译：杀真菌使用酚类芳香族化合物
公开(公告)号：US5447960A
公开(公告)日：1995-09-05
申请号：US131517
申请日：1993-10-04
申请人： Deirdre M. Sinnott , Hak-Fun Chow , Robert J. Ehr , Steven D. Lubetkin , Stephen E. Bales , Muthiah N. Inbasekaran
发明人： Deirdre M. Sinnott , Hak-Fun Chow , Robert J. Ehr , Steven D. Lubetkin , Stephen E. Bales , Muthiah N. Inbasekaran
IPC分类号： A01N31/08 , A01N35/06 , A01N43/14 , A01N43/40 , A01N45/02 , A01N43/16 , A01N43/42
CPC分类号： A01N43/40 , A01N31/08 , A01N35/06 , A01N43/14 , A01N45/02
摘要： A plant fungicide method comprises applying to the locus of a plant pathogen a fungicidally effective amount of a compound of formula (I) ##STR1## or a salt or a complex thereof, wherein: R.sup.1, R.sup.2, R.sup.3, R.sup.4, R.sup.5, R.sup.6, R.sup.7, and R.sup.8 are independently H, halo, NO.sub.2, (C.sub.1 -C.sub.4) alkyl, or halo(C.sub.1 -C.sub.4) alkyl;R.sup.3', R.sup.4', R.sup.5', R.sup.3", R.sup.4", and R.sup.5" are independently H, halo, OH, or CH.sub.3, provided that at least one is OH;R.sup.6 ' and R.sup.6 " are independently H or OH.
摘要翻译：植物杀真菌剂方法包括向植物病原体的基因座施用杀真菌有效量的式（I）化合物或其盐或其复合物，其中：R1，R2，R3，R4，R5 ，R 6，R 7和R 8独立地为H，卤素，NO 2，（C 1 -C 4）烷基或卤素（C 1 -C 4）烷基; R 3'，R 4'，R 5'，R 3“，R 4”和R 5“独立地为H，卤素，OH或CH 3，条件是至少一个是OH; R6'和R6“独立地为H或OH。

6. 发明授权

US5516877A Crosslinkable carbonate polymers of dihydroxyaryl fluorene 失效
标题翻译：二羟基芳基芴的交联碳酸酯聚合物
公开(公告)号：US5516877A
公开(公告)日：1996-05-14
申请号：US291211
申请日：1994-08-16
申请人： Stephen E. Bales , James P. Godschalx , Philip C. Yang , Matthew T. Bishop , Maurice J. Marks
发明人： Stephen E. Bales , James P. Godschalx , Philip C. Yang , Matthew T. Bishop , Maurice J. Marks
IPC分类号： C08G64/14 , C08G64/00
CPC分类号： C08G64/14
摘要： There are disclosed carbonate polymers of dihydroxyaryl fluorene having crosslinkable moieties. There are also disclosed such polymers in the form of composites. The polymers of this invention are capable of being crosslinked by activation of the crosslinkable moieties. Once crosslinked, these polymers demonstrate an excellent combination of properties including resistance to melting at high temperatures, solvent resistance, optical clarity, impact resistance, and physical strength.
摘要翻译：公开了具有可交联部分的二羟基芳基芴的碳酸酯聚合物。还公开了复合材料形式的这种聚合物。本发明的聚合物能够通过可交联部分的活化而交联。一旦交联，这些聚合物表现出包括耐高温熔融性，耐溶剂性，光学透明度，耐冲击性和物理强度的优异的组合。

7. 发明授权

US5045610A Blend of copolyestercarbonate polymer derived from diaryl dicarboxylic acid 失效
标题翻译：由二芳基二羧酸衍生的共聚酯碳酸酯聚合物的共混物
公开(公告)号：US5045610A
公开(公告)日：1991-09-03
申请号：US401213
申请日：1989-08-31
申请人： Stephen E. Bales , Kenneth A. Burdett , Guo-Shuh J. Lee
发明人： Stephen E. Bales , Kenneth A. Burdett , Guo-Shuh J. Lee
IPC分类号： C08G63/64 , C08L69/00 , C08L101/00
CPC分类号： C08L69/005 , C08G63/64 , C08L101/00
摘要： This invention relates to copolyestercarbonate polymers which are prepared with diaryl dicarboxylic acid compounds, particularly biphenyldicarboxylic acid compounds. Such copolyestercarbonate polymers show good physical properties including high glass transition temperatures and low ultraviolet radiation sensitivity. The thermoplastic copolymestercarbonates can be used to prepare films or molded articles or blended with other thermoplastic resins to give thermoplastic polymer blends for molding purposes.
摘要翻译：本发明涉及用二芳基二羧酸化合物，特别是联苯二羧酸化合物制备的共聚酯碳酸酯聚合物。这种共聚酯碳酸酯聚合物显示出良好的物理性质，包括高玻璃化转变温度和低紫外线辐射敏感性。热塑性共聚酯碳酸酯可用于制备膜或模塑制品或与其它热塑性树脂共混以得到用于模制目的的热塑性聚合物共混物。

8. 发明授权

US4388455A Process for preparing ester carbonate copolymers 失效
标题翻译：制备碳酸酯共聚物的方法
公开(公告)号：US4388455A
公开(公告)日：1983-06-14
申请号：US378693
申请日：1982-05-17
申请人： Stephen E. Bales
发明人： Stephen E. Bales
IPC分类号： C08G63/00 , C08G63/20 , C08G63/64 , C08G64/20
CPC分类号： C08G63/64
摘要： Ordered ester/carbonate copolymers having improved properties at higher solids are provided by (1) contacting a dihydric organic compound such as bisphenol-A with a diacid halide such as terephthaloyl chloride and a carbonate precursor such as phosgene under conditions sufficient to form an ester/carbonate oligomer and (2) contacting the oligomer with additional carbonate precursor to produce the desired ordered ester/carbonate copolymer.
摘要翻译：通过（1）在足以形成酯/酯的条件下使二羟基有机化合物如双酚A与二酰卤如对苯二甲酰氯和碳酸酯前体例如光气接触来提供在较高固体下具有改进性能的有序酯/碳酸酯共聚物，碳酸酯低聚物和（2）使低聚物与另外的碳酸酯前体接触以产生所需的有序酯/碳酸酯共聚物。

9. 发明授权

US5352272A Gas separations utilizing glassy polymer membranes at sub-ambient temperatures 失效
标题翻译：在低于环境温度下使用玻璃状聚合物膜的气体分离
公开(公告)号：US5352272A
公开(公告)日：1994-10-04
申请号：US930059
申请日：1992-08-13
申请人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Stephen E. Bales , Henry N. Beck , Thomas O. Jeanes , Bethanne L. Smith
发明人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Stephen E. Bales , Henry N. Beck , Thomas O. Jeanes , Bethanne L. Smith
IPC分类号： B01D53/22 , B01D53/26 , B01D63/00 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/02 , C01B21/04 , C08G64/10 , C08G75/06 , C08G75/26 , C08L67/00 , C08L67/03 , C08L69/00 , C08L71/12
CPC分类号： B01D71/48 , B01D53/22 , B01D53/228 , B01D53/268 , B01D69/02 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/0251 , C01B21/0444 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12 , C01B2210/0046 , C01B2210/0062 , Y02P20/129
摘要： This invention relates to a method of and apparatus for separating component gases in a gas mixture employing a glassy polymer membrane at temperatures of 5.degree. C. or less so as to achieve superior separation of gas components.
摘要翻译：本发明涉及一种在5℃或更低的温度下使用玻璃状聚合物膜分离气体混合物中的组分气体的方法和装置，以实现气体组分的优异分离。

10. 发明授权

US4840646A Tetrabromo bisphenol based polyestercarbonate membranes and method of using 失效
标题翻译：四溴双酚基聚碳酸酯膜及其使用方法
公开(公告)号：US4840646A
公开(公告)日：1989-06-20
申请号：US221483
申请日：1988-07-19
申请人： Joginder N. Anand , Stephen E. Bales , Darrell C. Feay , Thomas O. Jeanes
发明人： Joginder N. Anand , Stephen E. Bales , Darrell C. Feay , Thomas O. Jeanes
IPC分类号： B01D53/22 , B01D71/48 , B01D71/50 , C08G63/682
CPC分类号： C08G63/682 , B01D53/22 , B01D71/48 , B01D71/50
摘要： The invention is a membrane comprising a dense skin of a polyestercarbonate, wherein the diphenolic residue in the backbone of the polyestercarbonate is a tetrabromo diphenolic residue, wherein the membrane has a separation factor for oxygen and nitrogen of 6.5 or greater at about 24.degree. C. In another aspect, the invention is a method of separating oxygen from a mixture of gases comprising nitrogen and oxygen, wherein the method comprises (a) contacting the gas mixture with a thin, non-porous membrane comprising a polyestercarbonate described hereinbefore under conditions such that the oxygen selectively permeates through the membrane to the other side of the membrane; and (b) removing the permeated oxygen from the other side of the membrane, wherein separation factor for the oxygen and nitrogen is 6.5 or greater at about 24.degree. C. The membranes of this invention demonstrate surprisingly high separation factors for oxygen and nitrogen separations. The membranes of this invention have good mechanical properties and therefore are useful under more extreme conditions, for example temperature and pressure, than many commercially used membranes.
摘要翻译：本发明是一种包含聚酯碳酸酯致密表皮的膜，其中聚酯碳酸酯主链中的二酚残基是四溴二酚残基，其中该膜在约24℃下具有6.5或更高的氧和氮分离因子。在另一方面，本发明是从包含氮和氧的气体混合物中分离氧的方法，其中所述方法包括（a）使气体混合物与包含上述聚酯碳酸酯的薄的非多孔膜接触，条件是使得氧选择性地渗透膜到膜的另一侧; 和（b）从膜的另一侧除去渗透的氧气，其中在约24℃下氧和氮的分离因子为6.5或更大。本发明的膜表现出惊人的高分离因子用于氧气和氮气的分离。本发明的膜具有良好的机械性能，因此在许多商业使用的膜的更极端条件下，例如温度和压力下是有用的。

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