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1. 发明申请

WO2010085018A1 METHOD OF REGENERATING HETEROPOLYACID CATALYST USED IN THE DIRECT PROCESS OF PREPARING DICHLOROPROPANOL BY REACTING GLYCEROL AND CHLORINATING AGENT, METHOD OF PREPARING DICHLOROPROPANOL COMPRISING THE METHOD OF REGENERATING HETEROPOLYACID CATALYST AND METHOD OF PREPARING EPICHLOROHYDRIN COMPRISING THE METHOD OF PREPARING DICHLOROPROPANOL 审中-公开
标题翻译：在通过反应甘油和氯化剂制备二氯丙醇的直接方法中使用的异戊二酸催化剂的再生方法，包含再生二异氰酸酯催化剂的方法的制备二氯丙醇的方法
公开(公告)号：WO2010085018A1
公开(公告)日：2010-07-29
申请号：PCT/KR2009/000772
申请日：2009-02-18
申请人： SAMSUNG FINE CHEMICALS CO., LTD. , SONG, In Kyu , SONG, Sun Ho , LEE, Sang Hee , PARK, Dong Ryul , WOO, Sung Yul , SONG, Won Seob , KWON, Myong Suk
发明人： SONG, In Kyu , SONG, Sun Ho , LEE, Sang Hee , PARK, Dong Ryul , WOO, Sung Yul , SONG, Won Seob , KWON, Myong Suk
IPC分类号： B01J38/02
CPC分类号： B01J38/68 , B01J27/188 , B01J27/285 , C07C29/62 , Y02P20/584 , C07C31/36
摘要： Provided are a method of regenerating a heteropolyacid catalyst, a method of preparing dichloropropanol including the method of regenerating a heteropolyacid catalyst, and a method of preparing epichlorohydrin including the method of preparing dichloropropanol. The method of regenerating a heteropolyacid catalyst includes: separating a solid heteropolyacid catalyst from a reaction mixture after preparing dichloropropanol by simply evaporating components having a boiling point lower than that of the heteropolyacid catalyst (simple evaporation); and calcining the separated solid heteropolyacid catalyst (calcination). The method of regenerating the heteropolyacid catalyst may further include recrystallizing the calcined heteropolyacid catalyst (recrystallization).
摘要翻译：提供了再生杂多酸催化剂的方法，制备二氯丙醇的方法，包括再生杂多酸催化剂的方法，以及制备表氯醇的方法，包括制备二氯丙醇的方法。再生杂多酸催化剂的方法包括：通过简单地蒸发沸点低于杂多酸催化剂的组分（简单蒸发），在制备二氯丙醇之后，从反应混合物中分离固体杂多酸催化剂; 并煅烧分离的固体杂多酸催化剂（煅烧）。再生杂多酸催化剂的方法还可以包括将煅烧的杂多酸催化剂重结晶（重结晶）。

2. 发明申请

WO2012067470A2 METHOD OF PREPARING DIALKYL LACTAMIDES 审中-公开
标题翻译：制备二烷基内酰胺的方法
公开(公告)号：WO2012067470A2
公开(公告)日：2012-05-24
申请号：PCT/KR2011/008863
申请日：2011-11-21
申请人： SAMSUNG FINE CHEMICALS CO., LTD. , SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , KWON, Myong Suk
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , KWON, Myong Suk
IPC分类号： C07C231/02 , C07C235/06
CPC分类号： C07C231/02 , C07C235/06
摘要： A method of preparing dialyl lactamides. The method of preparing dialkyl lactamides includes preparing ammonium lactate by reacting at least one compound selected from the group consisting of lactic acid and esters thereof with at least one amine compound, preparing dialkyl lactamides by heat-treating the ammonium lactate, and adding at least one of a polymerization inhibitor and an anti-polymerization agent to a reaction mixture of at least one of the preparing of the ammonium lactate and the preparing of the dialkyl lactamides.
摘要翻译：一种制备二酰基内酰胺的方法。制备二烷基内酰胺的方法包括通过使至少一种选自乳酸及其酯的化合物与至少一种胺化合物反应来制备乳酸铵，通过热处理乳酸铵来制备二烷基内酰胺，并添加至少一种的聚合抑制剂和抗聚合剂加入至少一种制备乳酸铵和制备二烷基内酰胺的反应混合物中。

3. 发明申请

WO2011007931A1 METHOD OF PREPARING CHLOROHYDRINS BY REACTING POLYHYDROXY ALIPHATIC HYDROCARBON WITH CHLORINATION AGENT 审中-公开
标题翻译：通过反应具有氯化剂的聚羟基脂肪烃制备氯代醇的方法
公开(公告)号：WO2011007931A1
公开(公告)日：2011-01-20
申请号：PCT/KR2009/005926
申请日：2009-10-15
申请人： SAMSUNG FINE CHEMICALS CO., LTD. , SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , PARK, Sung Jin , KWON, Myong Suk , YU, Ji Hion
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , PARK, Sung Jin , KWON, Myong Suk , YU, Ji Hion
IPC分类号： C07C29/62
CPC分类号： C07C29/62 , C07C31/36
摘要： A method of preparing chlorohydrins from polyhydroxy aliphatic hydrocarbon such as glycerol. The method includes irradiating an ultrasonic wave to a reaction mixture during reaction.
摘要翻译：从多羟基脂肪烃如甘油制备氯代醇的方法。该方法包括在反应期间向反应混合物照射超声波。

4. 发明申请

WO2010076914A1 METHOD OF PREPARING DICHLOROPROPANOL USING GLYCEROL WITH IMPROVED SELECTIVITY FOR DICHLOROPROPANOL 审中-公开
标题翻译：使用甘油的二氯丙醇的制备方法对二氯丙醇具有改进的选择性
公开(公告)号：WO2010076914A1
公开(公告)日：2010-07-08
申请号：PCT/KR2009/000770
申请日：2009-02-18
申请人： SAMSUNG FINE CHEMICALS CO., LTD. , SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , PARK, Sung Jin , SONG, Hong Tae , KWON, Myoung Suk
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , PARK, Sung Jin , SONG, Hong Tae , KWON, Myoung Suk
IPC分类号： C07C29/62
CPC分类号： C07D301/26 , C07C29/62 , C07C31/36
摘要： Provided is a method of preparing dichloropropanol using glycerol. The method includes: chlorination of glycerol including a plurality of chlorination reaction stages using a catalyst; and a water-removing stage performed between the reaction stages, independently of the reaction stages.
摘要翻译：提供使用甘油制备二氯丙醇的方法。该方法包括：使用催化剂氯化甘油包括多个氯化反应阶段; 在反应阶段之间进行脱水阶段，独立于反应阶段。

5. 发明公开

EP2589585A2 METHOD FOR PREPARING CHLOROHYDRINS AND METHOD FOR PREPARING EPICHLOROHYDRIN USING CHLOROHYDRINS PREPARED THEREBY 有权转让
标题翻译：用于生产氯醇及其生产环氧氯丙烷采用这种工艺生产的氯醇
公开(公告)号：EP2589585A2
公开(公告)日：2013-05-08
申请号：EP11801056.0
申请日：2011-06-08
申请人： Samsung Fine Chemicals Co., Ltd.
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , KWON, Myoung Suk
IPC分类号： C07C29/62 , C07C29/80 , C07C31/34 , C07D303/08
CPC分类号： C07C29/62 , C07C29/80 , C07D301/26 , C07D303/08 , C07C31/36
摘要： A method of preparing chlorohydrins and a method of preparing epichlorohydrin using chlorohydrins prepared by using the same method are provided. The method is to prepare chlorohydrins by reacting polyhydroxy aliphatic hydrocarbon with a chlorination agent in the presence of a catalyst, and the method includes at least one combination of a series of unit operations including the following steps in the following stated order: a first reaction step; a water removal step; and a second reaction step, wherein the water removing step is performed by distillation operation based on a boiling point difference between constituents of a reaction mixture. The method of preparing epichlorohydrin includes reacting chlorohydrins prepared by using the method of preparing chlorohydrins with an alkaline agent.
摘要翻译：提供和制备氯醇的方法，制备使用通过使用相同的方法制备氯醇的表氯醇的方法。该方法是通过使多羟基脂肪烃在催化剂的存在下，氯化剂制备氯代醇，并且该方法包括一系列的单元操作包括下列规定顺序的以下步骤中的至少一个组合：第一反应步骤 ; 除水步骤; 和第二反应步骤中，worin水移除步骤是通过蒸馏操作基于反应混合物的成分之间的沸点差异进行。制备表氯醇的方法，包括使通过使用制备氯醇与碱性试剂的方法制备氯醇。

6. 发明公开

EP2594549A2 METHOD FOR PREPARING CHLOROHYDRINS COMPOSITION AND METHOD FOR PREPARING EPICHLOROHYDRIN USING CHLOROHYDRINS COMPOSITION PREPARED THEREBY 有权转让
标题翻译： VERFAHREN ZUR HERSTELLUNG EINER ZUSAMMENSETZUNG AUS CHLORHYDRINEN
公开(公告)号：EP2594549A2
公开(公告)日：2013-05-22
申请号：EP11801058.6
申请日：2011-06-08
申请人： Samsung Fine Chemicals Co., Ltd.
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , KWON, Myoung Suk
IPC分类号： C07C29/62 , C07C29/80 , C07C31/34 , C07D303/08
CPC分类号： C07D301/02 , C07C29/62 , C07C29/80 , C07D303/08 , C07C31/36
摘要： Provided are a method of preparing a chlorohydrin composition and a method of preparing epichlorohydrin by using a chlorohydrin composition prepared by using the method. The method of preparing chlorohydrins in which polyhydroxy aliphatic hydrocarbon is reacted with a chlorination agent in the presence of a catalyst includes performing at least one combination of a series of unit operations comprising a first reaction step, a water removal step, and a second reaction step in this stated order, wherein the method further includes mixing a chlorohydrin concentrate obtained by purifying the reaction mixture discharged from the final reaction step from among the reaction steps and a water-rich layer discharged from the water-removal step and diluting the mixture with water. The method of preparing epichlorohydrin includes contacting the chlorohydrin composition prepared by using the method of preparing a chlorohydrin composition with an alkaline agent
摘要翻译：提供制备氯代醇组合物的方法和通过使用通过使用该方法制备的氯代醇组合物制备表氯醇的方法。制备其中多羟基脂族烃与氯化剂在催化剂存在下反应的氯氢化物的方法包括进行一系列单元操作的至少一种组合，其中包括第一反应步骤，脱水步骤和第二反应步骤按照所述顺序，其中所述方法还包括混合从反应步骤中纯化从最终反应步骤排出的反应混合物和从除水步骤排出的富水层获得的氯代醇浓缩物，并用水稀释混合物。制备表氯醇的方法包括将通过使用氯醇组合物的制备方法制备的氯醇组合物与碱性试剂

7. 发明公开

EP2589583A2 METHOD FOR PREPARING CHLOROHYDRINS AND METHOD FOR PREPARING EPICHLOROHYDRIN USING CHLOROHYDRINS PREPARED THEREBY 有权转让
标题翻译：用于生产氯醇及其生产环氧氯丙烷采用这种工艺生产的氯醇
公开(公告)号：EP2589583A2
公开(公告)日：2013-05-08
申请号：EP11801054.5
申请日：2011-06-08
申请人： Samsung Fine Chemicals Co., Ltd.
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , KWON, Myoung Suk
IPC分类号： C07C29/62 , C07C29/80 , C07C31/34 , C07D303/08
CPC分类号： C07C29/62 , C07D301/26 , C07D303/08 , C07C31/36
摘要： A method of preparing chlorohydrins and a method of preparing epichlorohydrin by using chlorohydrins prepared using the method are provided. The method of preparing chlorohydrins by reacting polyhydroxy aliphatic hydrocarbon with a chlorination agent in the presence of a catalyst includes at least one combination of a series of unit operations including a first reaction step, a water removal step, and a second reaction step, in that respective order, and after mixing at least a portion of a reaction mixture discharged from at least one reaction steps from among the plurality of reaction steps with an additional chlorination agent, recirculating the resulting mixture to the reaction step from which the reaction mixture was discharged. The method of preparing epichlorohydrin includes a step of reacting chlorohydrins prepared using the method of preparing chlorohydrins, with an alkaline agent.
摘要翻译：提供和制备氯醇的方法，制备通过使用使用该方法制备氯醇的表氯醇的方法。通过使多羟基脂肪烃在催化剂的存在下，氯化剂制备氯醇的方法，包括：包括第一反应步骤中，除水步骤，和第二反应步骤中，DASS一系列单元操作中的至少一个组合 respectivement顺序，和至少从至少一个反应步骤中排出的反应混合物的一部分从反应步骤的多元性之间与另外的氯化剂将所得的混合物混合，循环至反应步骤之后，从该其排出的反应混合物中。制备表氯醇的方法，包括：使用制备氯醇的方法中，在碱性试剂制备氯醇起反应的步骤，其中。

8. 发明公开

EP2592063A2 METHOD FOR PREPARING CHLOROHYDRINS COMPOSITION AND METHOD FOR PREPARING EPICHLOROHYDRIN USING CHLOROHYDRINS COMPOSITION PREPARED THEREBY 有权转让
标题翻译：用于生产用于生产环氧氯丙烷的氯醇与流程中使用这个过程的合成方法获得由组合物氯代
公开(公告)号：EP2592063A2
公开(公告)日：2013-05-15
申请号：EP11801059.4
申请日：2011-06-08
申请人： Samsung Fine Chemicals Co., Ltd.
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , KWON, Myoung Suk
IPC分类号： C07C29/62 , C07C31/34 , C07D301/24 , C07D303/08
CPC分类号： C07D301/28 , C07C29/62 , C07C29/80 , C07D301/24 , C07D303/08 , C07C31/36 , C07C31/34
摘要： Disclosed are a method for preparing chlorohydrins composition and a method for preparing epichlorohydrin using chlorohydrins prepared thereby. The disclosed method for preparing chlorohydrins composition reacts polyhydroxy aliphatic hydrocarbon with a chlorination agent in the presence of a catalyst, comprises at least one combination of a series of unit operations including a first reaction step, a water removal step, and a second reaction step in the respective order, and additionally comprises a step for reacting the chlorohydrins composition derived from a plurality of reaction mixtures discharged from the plurality of reaction steps with an alkaline chemical, and removing the catalyst included in the chlorohydrins composition in the form of an alkali metal salt. The disclosed method for preparing epichlorohydrin includes a step for contacting the chlorohydrins composition, which was prepared using the method for preparing chlorohydrins composition, with an alkaline chemical.
摘要翻译：公开的是用于制备氯醇的组合物和用于制备使用由其制备氯醇的表氯醇的方法的方法。用于制备氯醇组合物中的盘游离缺失方法发生反应以在催化剂的存在下，氯化剂多羟基脂肪烃，包括一系列单元操作包括第一反应步骤中，除水步骤，和在第二反应步骤中的至少一个组合的respectivement顺序，并另外包括为了进行反应从在碱性化学从反应步骤的多元排出的反应混合物的多元得到的氯醇组合物，和在碱金属的盐的形式除去包含在氯醇组合物中的催化剂的工序，用于制备表氯醇的游离缺失盘方法包括用于接触氯醇组合物，其使用方法为制备氯醇的组合物在碱性化学制备，同的步骤。

9. 发明公开

EP2589586A2 METHOD FOR PREPARING CHLOROHYDRINS COMPOSITION AND METHOD FOR PREPARING EPICHLOROHYDRIN USING CHLOROHYDRINS COMPOSITION PREPARED THEREBY 有权转让
标题翻译：用于生产用于生产环氧氯丙烷的氯醇与流程中使用这个过程的合成方法获得由组合物氯代
公开(公告)号：EP2589586A2
公开(公告)日：2013-05-08
申请号：EP11801057.8
申请日：2011-06-08
申请人： Samsung Fine Chemicals Co., Ltd.
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , KWON, Myoung Suk
IPC分类号： C07C29/62 , C07C29/80 , C07C31/34 , C07D303/08
摘要： A method of preparing a chlorohydrin composition and a method of preparing epichlorohydrin by using a chlorohydrin composition prepared by using the method are provided. The method of preparing a chlorohydrin composition in which a polyhydroxy aliphatic hydrocarbon is reacted with a chlorination agent in the presence of a catalyst includes performing at least one combination of a series of unit operations comprising a first reaction step, a water removal step, and a second reaction step in this stated order, wherein the method further includes mixing a chlorohydrin concentrate obtained by purifying the reaction mixture discharged from the final reaction step from among the plurality of reaction steps and a water-rich layer discharged from the water-removal step. The method of preparing epichlorohydrin includes contacting the chlorohydrin composition prepared by using the method of preparing a chlorohydrin composition with an alkaline agent
摘要翻译：提供了制备氯醇组合物和通过使用由使用该方法制备氯醇组合物制备表氯醇的方法的方法。制备其中的多羟基脂肪烃进行反应在催化剂的存在下，氯化剂氯醇组合物的方法包括：执行至少一个组合的一系列单元操作的，其包括第一反应步骤中，除水步骤，和一个在此所述的顺序第二反应步骤中，worin所述方法还包括混合氯醇浓缩物通过纯化从反应步骤的多元化和从水中除去步骤排出的富水层中的最后反应步骤中排出的反应混合物中获得。制备表氯醇的方法，包括使通过使用在碱性试剂制备具有氯醇组合物的方法制备的氯醇组合物

10. 发明公开

EP2589584A2 METHOD FOR PREPARING CHLOROHYDRINS AND METHOD FOR PREPARING EPICHLOROHYDRIN USING CHLOROHYDRINS PREPARED THEREBY 有权转让
标题翻译：用于生产氯醇及其生产环氧氯丙烷采用这种工艺生产的氯醇
公开(公告)号：EP2589584A2
公开(公告)日：2013-05-08
申请号：EP11801055.2
申请日：2011-06-08
申请人： Samsung Fine Chemicals Co., Ltd.
发明人： SONG, Won Seob , WOO, Sung Yul , SONG, Boo Weon , PARK, Seong Han , KWON, Myoung Suk
IPC分类号： C07C29/62 , C07C29/80 , C07C31/34 , C07D303/08
CPC分类号： C07C29/62 , C07D303/08 , C07C31/36
摘要： A method of preparing chlorohydrins and a method of preparing epichlorohydrin by using chlorohydrins prepared using the method are provided. The method of preparing chlorohydrins by reacting polyhydroxy aliphatic hydrocarbon with a chlorination agent in the presence of a catalyst includes at least one combination of a series of unit operations including a first reaction step, a water removal step, and a second reaction step, in that respective order, wherein the method further includes purifying chlorohydrins from a reaction mixture discharged from a final reaction step of the plurality of reaction steps. The method of preparing epichlorohydrin includes reacting chlorohydrins prepared using the method of preparing chlorohydrins, with an alkaline agent.
摘要翻译：提供和制备氯醇的方法，制备通过使用使用该方法制备氯醇的表氯醇的方法。通过使多羟基脂肪烃在催化剂的存在下，氯化剂制备氯醇的方法，包括：包括第一反应步骤中，除水步骤，和第二反应步骤中，DASS一系列单元操作中的至少一个组合 respectivement顺序，worin该方法包括从来自反应步骤的多个最终反应步骤排出的反应混合物中纯化。此外氯醇。制备表氯醇的方法，包括使氯醇使用制备氯醇的方法中，在碱性试剂制备，。

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