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1. 发明申请

WO2009075402A1 METHOD OF PREPARING DICHLOROPROPANOL FROM GLYCEROL USING HETEROPOLYACID CATALYSTS 审中-公开
标题翻译：使用异佛尔酮酸催化剂从甘油制备二氯丙醇的方法
公开(公告)号：WO2009075402A1
公开(公告)日：2009-06-18
申请号：PCT/KR2007/006779
申请日：2007-12-24
申请人： SAMSUNG FINE CHEMICALS CO., LTD. , SONG, In-Kyu , LEE, Sang-Hee , WOO, Sung-Yul , SONG, Won-Seob , KWON, Myong-Suk
发明人： SONG, In-Kyu , LEE, Sang-Hee , WOO, Sung-Yul , SONG, Won-Seob , KWON, Myong-Suk
IPC分类号： C07C31/36
CPC分类号： C07D301/24 , C07C29/62 , C07C31/36
摘要： Provided is a method of preparing dichloropropanol from glycerol. According to the method, glycerol is reacted with a chlorinating agent using a heteropolyacid catalyst to prepare dichloropropanol. Accordingly, dichloropropanol can be directly prepared from glycerol by using heteropolyacid catalysts, and conventional problems such as recovery of the catalyst and separation of an azeotropic mixture including the catalyst and the products can be overcome. In addition, since the catalyst can be easily recovered and reused, the manufacturing process can be simplified and expensive dichloropropanol can be produced at high yield from inexpensive glycerol.
摘要翻译：提供从甘油制备二氯丙醇的方法。根据该方法，使用杂多酸催化剂使甘油与氯化剂反应制备二氯丙醇。因此，可以通过使用杂多酸催化剂从甘油直接制备二氯丙醇，并且可以克服常规问题，例如催化剂的回收和包含催化剂和产物的共沸混合物的分离。此外，由于可以容易地回收和重复使用催化剂，因此可以简化制造工艺，并且可以以廉价的甘油高产率生产昂贵的二氯丙醇。

2. 发明申请

WO2009031756A2 CONTINUOUS-FLOW DUAL-BED REACTOR FOR PRODUCTION OF LIQUID-PHASE HYDROCARBON MIXTURE ON FISCHER-TROPSCH CATALYSIS USING SYNTHETIC GAS 审中-公开
标题翻译：连续流动双壁反应器，用于生产液相烃混合物，使用合成气体进行FISCHER-TROPSCH催化
公开(公告)号：WO2009031756A2
公开(公告)日：2009-03-12
申请号：PCT/KR2008004125
申请日：2008-07-14
申请人： KOREA RES INST CHEM TECH , DAELIM IND CO LTD , DOOSAN MECATEC CO LTD , KOREA NAT OIL CORP , HYUNDAI ENGINEERING CO LTD , SK ENERGY CO LTD , JUN KI-WON , SONG IN KYU , CHO KYUNG MIN , PARK SUNYOUNG , BAECK SUNG-HYEON
发明人： JUN KI-WON , SONG IN KYU , CHO KYUNG MIN , PARK SUNYOUNG , BAECK SUNG-HYEON
IPC分类号： B01J8/04 , C07C1/04
CPC分类号： B01J8/0457 , B01J8/0492 , B01J8/0496 , B01J23/75 , B01J23/755 , B01J29/0333 , B01J37/0201 , C10G2/32 , C10G2/332 , C10G47/14 , C10G69/02
摘要： The present invention relates to a process of preparing liquid-phase hydrocarbon mixture, which comprises continuously conducting Fischer-Tropsch synthesis reaction in the upper part and hydrocracking reaction in the lower part by using a continuous-flow dual-bed reactor which comprises two fixed-bed reactors filled with catalysts and continuously placed in upper and lower parts and a hydrogen-supplying pipe between the upper and the lower fixed-bed reactors and continuously supplying hydrogen in the lower fixed-bed reactor, thereby remarkably increasing the yield of C10-C20 liquid-phase hydrocarbon mixture as compared to the conventional Fischer-Tropsch synthesis reaction.
摘要翻译：本发明涉及一种制备液相烃混合物的方法，其包括在上部连续进行费 - 托合成反应和下部的加氢裂化反应，使用连续流动双床反应器，其包括两个固定 - 填充催化剂并连续放置在上部和下部的床反应器和上下固定床反应器之间的氢气供应管，并在下固定床反应器中连续供应氢气，从而显着提高了C10-C20的收率液相烃混合物与常规的费 - 托合成反应相比。

3. 发明申请

WO2009151175A1 METHOD OF PREPARING DICHLOROPROPANOL FROM GLYCEROL IN THE PRESENCE OF HETEROPOLYACID CATALYST AND/OR ABSORBENT UNDER SOLVENT-FREE CONDITIONS 审中-公开
标题翻译：在无溶剂条件下，在异戊二烯类催化剂和/或吸收剂存在下，从甘油中制备二氯丙醇的方法
公开(公告)号：WO2009151175A1
公开(公告)日：2009-12-17
申请号：PCT/KR2008/003680
申请日：2008-06-26
申请人： SAMSUNG FINE CHEMICALS CO., LTD. , SONG, In-Kyu , LEE, Sang-Hee , SONG, Sun-Ho , PARK, Dong-Ryul , WOO, Sung-Yul , SONG, Won-Seob , KWON, Myong-Suk
发明人： SONG, In-Kyu , LEE, Sang-Hee , SONG, Sun-Ho , PARK, Dong-Ryul , WOO, Sung-Yul , SONG, Won-Seob , KWON, Myong-Suk
IPC分类号： C07C29/62
CPC分类号： C07C29/62 , C07C31/36 , C07C31/42
摘要： Provided is a method of preparing dichloropropanol from glycerol. The method includes reacting glycerol with a chlorinating agent, and the reaction is performed in the presence of a heteropolyacid catalyst and/or an absorbent under solvent-free conditions. Thus, according to the method, dichloropropanol can be directly prepared from glycerol. Since a solvent is not used, a process of removing the solvent is not necessary, and thus the volume of a reactor can be reduced. In addition, conventional problems such as recovery of the catalyst and separation of an azeotropic mixture including the catalyst and products can be overcome. In addition, expensive dichloropropanol can be produced at high yield from inexpensive glycerol.
摘要翻译：提供从甘油制备二氯丙醇的方法。该方法包括使甘油与氯化剂反应，反应在无溶剂条件下在杂多酸催化剂和/或吸收剂存在下进行。因此，根据该方法，可以从甘油直接制备二氯丙醇。由于不使用溶剂，因此不需要除去溶剂的方法，因此能够降低反应器的体积。此外，可以克服常规问题，例如催化剂的回收和包含催化剂和产物的共沸混合物的分离。此外，昂贵的二氯丙醇可以从廉价的甘油以高产率制备。

4. 发明申请

WO2011129531A3 POLARISING PLATE AND A LIQUID-CRYSTAL DISPLAY DEVICE COMPRISING THE SAME 审中-公开
标题翻译：偏振板和包含该液晶显示装置的液晶显示装置
公开(公告)号：WO2011129531A3
公开(公告)日：2012-01-19
申请号：PCT/KR2011001884
申请日：2011-03-18
申请人： DONGWOO FINE CHEM CO LTD , YOO JEONG HO , SONG IN KYU , YOO MIN KEUN
发明人： YOO JEONG HO , SONG IN KYU , YOO MIN KEUN
IPC分类号： G02B5/30 , G02F1/1335
CPC分类号： G02B5/3033
摘要： The present invention relates to a polarising plate and to a liquid-crystal display device comprising the same. More specifically, the present invention relates to a polarising plate which comprises, with respect to 100 parts by weight of a water-soluble polyamide epoxy resin, between 1 and 100 parts by weight (based on solids content) of an acetoacetyl-modified poly(vinyl alcohol) resin, and also comprises an adhesive layer of an adhesive composition having a pH of at least 5, thereby increasing the force of bonding between the functional group of the adhesive composition in the adhesive layer and a protective film (acrylic or propylene based) and a polarizer functional group and hence making it possible to improve durability and reliability by maintaining an adhesive force between the polarizer and the protective film even under high temperature and highly humid conditions. The present invention also relates to a liquid-crystal display device comprising the polarising plate.
摘要翻译：本发明涉及一种偏振片及其制造方法。更具体地说，本发明涉及一种偏振片，其特征在于，相对于100重量份的水溶性聚酰胺环氧树脂，包含1至100重量份（基于固体含量）乙酰乙酰基改性的聚（乙烯醇）树脂，并且还包含具有至少5的pH的粘合剂组合物的粘合剂层，从而增加粘合剂层中的粘合剂组合物的官能团与保护膜（丙烯酸或丙烯基）之间的粘结力）和偏光板官能团，因此即使在高温高湿条件下也能够通过保持偏振片与保护膜之间的粘合力而提高耐久性和可靠性。本发明还涉及包括偏振片的液晶显示装置。

5. 发明申请

WO2010085018A1 METHOD OF REGENERATING HETEROPOLYACID CATALYST USED IN THE DIRECT PROCESS OF PREPARING DICHLOROPROPANOL BY REACTING GLYCEROL AND CHLORINATING AGENT, METHOD OF PREPARING DICHLOROPROPANOL COMPRISING THE METHOD OF REGENERATING HETEROPOLYACID CATALYST AND METHOD OF PREPARING EPICHLOROHYDRIN COMPRISING THE METHOD OF PREPARING DICHLOROPROPANOL 审中-公开
标题翻译：在通过反应甘油和氯化剂制备二氯丙醇的直接方法中使用的异戊二酸催化剂的再生方法，包含再生二异氰酸酯催化剂的方法的制备二氯丙醇的方法
公开(公告)号：WO2010085018A1
公开(公告)日：2010-07-29
申请号：PCT/KR2009/000772
申请日：2009-02-18
申请人： SAMSUNG FINE CHEMICALS CO., LTD. , SONG, In Kyu , SONG, Sun Ho , LEE, Sang Hee , PARK, Dong Ryul , WOO, Sung Yul , SONG, Won Seob , KWON, Myong Suk
发明人： SONG, In Kyu , SONG, Sun Ho , LEE, Sang Hee , PARK, Dong Ryul , WOO, Sung Yul , SONG, Won Seob , KWON, Myong Suk
IPC分类号： B01J38/02
CPC分类号： B01J38/68 , B01J27/188 , B01J27/285 , C07C29/62 , Y02P20/584 , C07C31/36
摘要： Provided are a method of regenerating a heteropolyacid catalyst, a method of preparing dichloropropanol including the method of regenerating a heteropolyacid catalyst, and a method of preparing epichlorohydrin including the method of preparing dichloropropanol. The method of regenerating a heteropolyacid catalyst includes: separating a solid heteropolyacid catalyst from a reaction mixture after preparing dichloropropanol by simply evaporating components having a boiling point lower than that of the heteropolyacid catalyst (simple evaporation); and calcining the separated solid heteropolyacid catalyst (calcination). The method of regenerating the heteropolyacid catalyst may further include recrystallizing the calcined heteropolyacid catalyst (recrystallization).
摘要翻译：提供了再生杂多酸催化剂的方法，制备二氯丙醇的方法，包括再生杂多酸催化剂的方法，以及制备表氯醇的方法，包括制备二氯丙醇的方法。再生杂多酸催化剂的方法包括：通过简单地蒸发沸点低于杂多酸催化剂的组分（简单蒸发），在制备二氯丙醇之后，从反应混合物中分离固体杂多酸催化剂; 并煅烧分离的固体杂多酸催化剂（煅烧）。再生杂多酸催化剂的方法还可以包括将煅烧的杂多酸催化剂重结晶（重结晶）。

6. 发明申请

WO2009045002A1 METHOD OF PREPARING ZINC FERRITE CATALYSTS USING BUFFER SOLUTION AND METHOD OF PREPARING 1,3-BUTADIENE USING SAID CATALYSTS 审中-公开
标题翻译：使用缓冲溶液制备锌铁氧体催化剂的方法和使用所述催化剂制备1,3-丁二烯的方法
公开(公告)号：WO2009045002A1
公开(公告)日：2009-04-09
申请号：PCT/KR2008/005095
申请日：2008-08-29
申请人： SK ENERGY CO., LTD. , CHUNG, Young Min , KIM, Tae Jin , LEE, Seong Jun , KIM, Yong Seung , OH, Seung Hoon , SONG, In Kyu , KIM, Hee Soo , JUNG, Ji Chul , LEE, Ho Won
发明人： CHUNG, Young Min , KIM, Tae Jin , LEE, Seong Jun , KIM, Yong Seung , OH, Seung Hoon , SONG, In Kyu , KIM, Hee Soo , JUNG, Ji Chul , LEE, Ho Won
IPC分类号： B01J23/80
CPC分类号： B01J23/80 , B01J37/03 , C07C5/48 , C07C2523/80 , C07C11/167
摘要： The present invention relates to a method of preparing a zinc ferrite catalyst using a buffer solution and a method of producing 1,3-butadiene using the zinc ferrite catalyst, and, more particularly, to a method of preparing a zinc ferrite catalyst directly using a buffer solution as a coprecipitation medium without adjusting the pH of a coprecipitation solution by additionally adding acids and bases to the coprecipitation solution, and a method of producing 1,3-butadiene using the zinc ferrite catalyst through the oxidative dehydrogenation reaction of a C4 mixture including n-butene and n-butane.
摘要翻译：本发明涉及使用缓冲溶液制备锌铁氧体催化剂的方法和使用锌铁氧体催化剂制备1,3-丁二烯的方法，更具体地说，涉及直接使用缓冲溶液作为共沉淀介质，而不通过向共沉淀溶液中加入酸和碱调节共沉淀溶液的pH，以及通过C4混合物的氧化脱氢反应使用铁酸锌催化剂生产1,3-丁二烯的方法，包括正丁烯和正丁烷。

7. 发明申请

WO2009031756A3 CONTINUOUS-FLOW DUAL-BED REACTOR FOR PRODUCTION OF LIQUID-PHASE HYDROCARBON MIXTURE ON FISCHER-TROPSCH CATALYSIS USING SYNTHETIC GAS 审中-公开
公开(公告)号：WO2009031756A3
公开(公告)日：2009-03-12
申请号：PCT/KR2008/004125
申请日：2008-07-14
申请人： KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY , DAELIM INDUSTRIAL CO., LTD. , DOOSAN MECATEC CO., LTD. , KOREA NATIONAL OIL CORPORATION , HYUNDAI ENGINEERING CO., LTD. , SK ENERGY CO., LTD. , JUN, Ki-won , SONG, In Kyu , CHO, Kyung min , PARK, Sunyoung , BAECK, Sung-Hyeon
发明人： JUN, Ki-won , SONG, In Kyu , CHO, Kyung min , PARK, Sunyoung , BAECK, Sung-Hyeon
IPC分类号： B01J8/04 , C07C1/04
摘要： The present invention relates to a process of preparing liquid-phase hydrocarbon mixture, which comprises continuously conducting Fischer-Tropsch synthesis reaction in the upper part and hydrocracking reaction in the lower part by using a continuous-flow dual-bed reactor which comprises two fixed-bed reactors filled with catalysts and continuously placed in upper and lower parts and a hydrogen-supplying pipe between the upper and the lower fixed-bed reactors and continuously supplying hydrogen in the lower fixed-bed reactor, thereby remarkably increasing the yield of C 10 -C 20 liquid-phase hydrocarbon mixture as compared to the conventional Fischer-Tropsch synthesis reaction.

8. 发明申请

WO2008147055A1 A METHOD OF PREPARING MULTICOMPONENT BISMUTH MOLYBDATE CATALYSTS WITH CONTROLLING PH AND A METHOD OF PREPARING 1,3-BUTADIENE USING THEREOF 审中-公开
标题翻译：一种制备具有控制PH的多组分双官能微晶催化剂的方法及其制备1,3-丁二烯的方法
公开(公告)号：WO2008147055A1
公开(公告)日：2008-12-04
申请号：PCT/KR2008/002586
申请日：2008-05-08
申请人： SK ENERGY CO., LTD. , CHUNG, Young Min , LEE, Seong Jun , KIM, Tae Jin , OH, Seung Hoon , KIM, Yong Seung , SONG, In Kyu , KIM, Hee Soo , JUNG, Ji Chul , LEE, Ho Won
发明人： CHUNG, Young Min , LEE, Seong Jun , KIM, Tae Jin , OH, Seung Hoon , KIM, Yong Seung , SONG, In Kyu , KIM, Hee Soo , JUNG, Ji Chul , LEE, Ho Won
IPC分类号： B01J23/31
CPC分类号： H04N21/4126 , B01J23/002 , B01J23/31 , B01J23/8876 , B01J37/031 , B01J2523/00 , C07C5/48 , C07C2523/18 , C07C2523/28 , C07C2523/745 , C07C2523/755 , C07C2523/883 , H04N21/4334 , H04N21/43615 , H04N21/43637 , H04N21/440263 , H04N21/64322 , C07C11/167 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/847
摘要： This invention relates to a method of preparing a multicomponent bismuth molybdate catalyst by changing the pH of a coprecipitation solution upon coprecipitation and a method of preparing 1,3-butadiene using the catalyst. The multicomponent bismuth molybdate catalyst, coprecipitated using a solution having an adjusted pH, the preparation method thereof, and the method of preparing 1,3-butadiene through oxidative dehydrogenation using a C4 mixture including n-butene and n-butane as a reactant are provided. The C4 raffinate, containing many impurities, is directly used as a reactant without an additional process for separating n-butane or extracting n-butene, thus obtaining 1,3-butadiene at high yield. The activity of the multicomponent bismuth molybdate catalyst can be simply increased through precise pH adjustment upon coprecipitation, which is not disclosed in the conventional techniques. This method can be applied to the increase in the activity of multicomponent bismuth molybdate catalysts reported in the art.
摘要翻译：本发明涉及通过在共沉淀时改变共沉淀溶液的pH值和使用该催化剂制备1,3-丁二烯的方法制备多组分钼酸铋催化剂的方法。提供了使用调节pH的溶液共沉淀的多组分钼酸铋催化剂及其制备方法以及使用包含正丁烯和正丁烷作为反应物的C4混合物通过氧化脱氢制备1,3-丁二烯的方法。含有许多杂质的C4萃余液直接用作反应物，而不需要另外的分离正丁烷或提取正丁烯的方法，从而以高产率获得1,3-丁二烯。多组分钼酸铋催化剂的活性可以通过共沉淀下的精确pH调节简单地增加，这在传统技术中没有公开。该方法可以应用于本领域中报道的多组分钼酸铋催化剂的活性的提高。

9. 发明申请

WO2008140213A1 ZINC FERRITE CATALYSTS, METHOD OF PREPARING THEREOF AND METHOD OF PREPARING 1,3-BUTADIENE USING THEREOF 审中-公开
标题翻译：锌铁素体催化剂及其制备方法及其制备1,3-丁二烯的方法
公开(公告)号：WO2008140213A1
公开(公告)日：2008-11-20
申请号：PCT/KR2008/002587
申请日：2008-05-08
申请人： SK ENERGY CO., LTD. , CHUNG, Young Min , LEE, Seong Jun , KIM, Tae Jin , OH, Seung Hoon , KIM, Yong Seung , SONG, In Kyu , KIM, Hee Soo , JUNG, Ji Chul , LEE, Ho Won
发明人： CHUNG, Young Min , LEE, Seong Jun , KIM, Tae Jin , OH, Seung Hoon , KIM, Yong Seung , SONG, In Kyu , KIM, Hee Soo , JUNG, Ji Chul , LEE, Ho Won
IPC分类号： B01J23/80
CPC分类号： B01J23/80 , B01J23/002 , B01J35/002 , B01J37/031 , B01J2523/00 , C07C5/3332 , C07C2523/80 , C07C11/167 , B01J2523/27 , B01J2523/842
摘要： The present invention relates to a zinc ferrite catalyst, a method of producing the same, and a method of preparing 1,3 -butadiene using the same. Specifically, the present invention relates to a zinc ferrite catalyst which is produced in a pH-adjusted solution using a coprecipitation method, a method of producing the same, and a method of preparing 1,3- butadiene using the same, in which the 1,3 -butadiene can be prepared directly using a C4 mixture including n-butene and n-butane through an oxidative dehydrogenation reaction. The present invention is advantageous in that 1,3-butadiene can be obtained at a high yield directly using a C4 fraction without performing an additional process for separating n-butene, as a reactant, from a C4 fraction containing impurities.
摘要翻译：铁酸锌催化剂及其制造方法技术领域本发明涉及铁酸锌催化剂及其制造方法，以及使用该锌铁氧体催化剂的1,3-丁二烯的制造方法。具体而言，本发明涉及使用共沉淀法在pH调节溶液中制造的铁酸锌催化剂及其制造方法，以及使用该锌铁氧体催化剂制备1,3-丁二烯的方法，其中1 可以通过氧化脱氢反应使用包含正丁烯和正丁烷的C4混合物直接制备3-丁二烯。本发明的优点在于，可以直接使用C4馏分以高产率获得1,3-丁二烯，而不进行从含有杂质的C4馏分中分离作为反应物的正丁烯的另外的方法。

10. 发明申请

WO2007119929A1 BISMUTH MOLYBDATE-BASED CATALYSTS, METHOD OF PREPARING THEREOF AND METHOD OF PREPARING 1,3-BUTADIENE USING THEREOF 审中-公开
标题翻译： BISMUTH MOLYBAST基催化剂及其制备方法及其制备1,3-丁二烯的方法
公开(公告)号：WO2007119929A1
公开(公告)日：2007-10-25
申请号：PCT/KR2007/001308
申请日：2007-03-16
申请人： SK ENERGY CO., LTD. , OH, Seung Hoon , LEE, Seong Jun , KIM, Tae Jin , CHOI, Ahn Seop , CHUNG, Young Min , SONG, In Kyu , JUNG, Ji Chul , KIM, Hee Soo
发明人： OH, Seung Hoon , LEE, Seong Jun , KIM, Tae Jin , CHOI, Ahn Seop , CHUNG, Young Min , SONG, In Kyu , JUNG, Ji Chul , KIM, Hee Soo
IPC分类号： B01J23/644
CPC分类号： B01J35/0006 , B01J23/31 , B01J35/002 , B01J37/03 , C07C5/3335 , C07C2523/644 , C07C11/167
摘要： This invention relates to a bismuth molybdate catalyst, a preparation method thereof, and a method of preparing 1,3 -butadiene using the same, and to a bismuth molybdate catalyst, a preparation method thereof, and a method of preparing 1,3 -butadiene using the same, in which 1,3 -butadiene can be prepared through oxidative dehydrogenation directly using a C4 mixture including n-butene and n-butane as a reactant in the presence of a mixed-phase bismuth molybdate catalyst including α-bismuth molybdate (Bi2Mo3On) and γ-bismuth molybdate (Bi2MoO6). According to this invention, the C4 raffinate, containing many impurities, is used as a reactant, without an additional n-butane separation process, thus obtaining 1,3-butadiene at high yield. Unlike complicated multicomponent-based metal oxides, the catalyst of the invention has simple constituents and synthesis routes, and can be easily formed through physical mixing, and thus is very advantageous in assuring reproducibility and can be directly applied to commercial processes.
摘要翻译：本发明涉及钼酸铋催化剂及其制备方法，以及使用其制备1,3-丁二烯的方法，以及钼酸铋催化剂及其制备方法以及制备1,3-丁二烯的方法使用相同的方法，其中可以通过使用包含正丁烯和正丁烷的C4混合物作为反应物在包含钼酸铋的混合钼酸铋催化剂的存在下，通过氧化脱氢制备1,3-丁二烯（ Bi2Mo3On）和钼酸铋（Bi2MoO6）。根据本发明，不含额外的正丁烷分离方法，将含有许多杂质的C4萃余液用作反应物，从而以高产率获得1,3-丁二烯。不同于复合多组分金属氧化物，本发明的催化剂具有简单的组成和合成路线，并且可以通过物理混合容易地形成，因此在确保再现性方面是非常有利的，并且可以直接应用于商业过程。

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