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1. 发明授权

US5734098A Method to monitor and control chemical treatment of petroleum, petrochemical and processes with on-line quartz crystal microbalance sensors 失效
标题翻译：使用在线石英晶体微量天平传感器监测和控制石油，石化和工艺化学处理的方法
公开(公告)号：US5734098A
公开(公告)日：1998-03-31
申请号：US621402
申请日：1996-03-25
申请人： Paul R. Kraus , Robert D. McClain , Michael K. Poindexter
发明人： Paul R. Kraus , Robert D. McClain , Michael K. Poindexter
IPC分类号： C02F1/00 , C07B61/00 , C07C7/00 , C07C11/02 , C07C253/34 , C07C255/08 , C10G15/00 , G01N5/02 , G01N9/00 , G01N9/36 , G01N11/10 , G01N11/16 , G01N27/00 , G01N29/02 , G01N29/036 , G01N33/00 , G01N33/18 , G01N33/28 , G05D21/00
CPC分类号： G01N29/022 , G01N17/008 , G01N29/036 , G01N11/10 , G01N2291/0256 , G01N2291/02818 , G01N2291/0422 , G01N2291/0426 , G01N9/002
摘要： Thickness-shear mode resonators which simultaneously measure mass deposition and fluid properties can be utilized to monitor petroleum processing, petrochemical and water treatment systems. Specialty chemical additive materials can be accurately and instantaneously added to control conditions detected by the thickness-shear mode resonators. The thickness-shear mode resonators are piezoelectric crystals used in conjunction with oscillator circuitry that can determine mass as well as viscosity and/or density of a fluid in contact with the piezoelectric surface.
摘要翻译：同时测量质量沉积和流体性质的厚度剪切模式谐振器可用于监测石油加工，石化和水处理系统。专门的化学添加剂材料可以精确和即时添加，以控制由厚度 - 剪切模式谐振器检测到的条件。厚度 - 剪切模式谐振器是与振荡器电路结合使用的压电晶体，其可以确定与压电表面接触的流体的质量以及粘度和/或密度。

2. 发明授权

US5879534A Non-enolizable oxygenates as anti foulants in ethylene dichloride manufacture 失效
标题翻译：不可烯化的含氧化合物作为二氯乙烷中的防污剂制造
公开(公告)号：US5879534A
公开(公告)日：1999-03-09
申请号：US102483
申请日：1998-06-22
申请人： Vincent E. Lewis , Robert D. McClain , Michael K. Poindexter
发明人： Vincent E. Lewis , Robert D. McClain , Michael K. Poindexter
IPC分类号： C07C17/42 , C10G19/02 , C10G75/04 , C10G9/16
CPC分类号： C07C17/42 , C10G19/02 , C10G75/04 , Y10S585/95
摘要： A method of inhibiting the formation of fouling deposits occurring in spent caustic wash systems used for ethylene dichloride (EDC) manufacturing processes. Fouling occurs in these systems when they are in contact with EDC processing streams contaminated with oxygen-containing compounds, such as aldehydes. These deposits are formed in EDC processing streams contaminated with oxygen-containing compounds while in contact with a caustic solution having a pH>7. The invention comprises adding an effective deposit-inhibiting amount of a non-enolizable carbonyl compound to the caustic solution. Preferred non-enolizable carbonyl compounds are formaldehyde, glyoxal, benzaldehyde, p-anisaldehyde, formic acid, glyoxalic acid and paraformaldehyde.
摘要翻译：一种抑制在用于二氯乙烷（EDC）制造过程的废碱洗涤系统中发生的结垢沉积物形成的方法。当这些系统与含氧化合物（如醛）污染的EDC处理流接触时，会在这些系统中发生结垢。这些沉积物在与含氧化合物污染的EDC处理流中形成，同时与pH> 7的苛性碱溶液接触。本发明包括向苛性碱溶液中加入有效的沉积抑制量的非烯醇化羰基化合物。优选的不可烯化羰基化合物是甲醛，乙二醛，苯甲醛，对茴香醛，甲酸，乙二醛酸和多聚甲醛。

3. 发明授权

US5770041A Non-enolizable oxygenates as antifoulants 失效
标题翻译：不可烯化的含氧化合物作为防污剂
公开(公告)号：US5770041A
公开(公告)日：1998-06-23
申请号：US804050
申请日：1997-02-21
申请人： Vincent E. Lewis , Robert D. McClain , Michael K. Poindexter
发明人： Vincent E. Lewis , Robert D. McClain , Michael K. Poindexter
IPC分类号： C07C17/42 , C10G19/02 , C10G75/04 , C10G9/16
CPC分类号： C10G75/04 , C07C17/42 , C10G19/02 , Y10S585/95
摘要： The invention is a method of inhibiting the formation of fouling deposits occurring on the surface of an alkaline scrubber used to remove acid gases, such as hydrogen sulfide, carbon dioxide and mercaptans, from hydrocarbon streams. These deposits are formed during the scrubbing of pyrolytically produced hydrocarbons contaminated with oxygen-containing compounds with a caustic solution having a pH>7 which comprises adding an effective deposit-inhibiting amount of a non-enolizable carbonyl compound to the caustic solution. The invention is also a method of inhibiting the formation of fouling deposits occurring in spent caustic wash/stripper systems used for hydrocarbon manufacturing processes. Fouling occurs in these systems when they are in contact with hydrocarbon processing streams contaminated with oxygen-containing compounds, such as aldehydes. These deposits are formed in hydrocarbon processing streams contaminated with oxygen-containing compounds while in contact with a caustic solution having a pH>7. The invention comprises adding an effective deposit-inhibiting amount of a non-enolizable carbonyl compound to the caustic solution. Preferred non-enolizable carbonyl compounds are formaldehyde, glyoxal, benzaldehyde, p-anisaldehyde, formic acid, glyoxalic acid and paraformaldehyde.
摘要翻译：本发明是一种抑制在用于从烃流中除去酸性气体如硫化氢，二氧化碳和硫醇的碱性洗涤器表面上发生的结垢沉积物形成的方法。这些沉积物是在用含有氢的化合物污染的热解生成的碳氢化合物的洗涤过程中形成的，所述氢氧化物溶液具有pH> 7的苛性碱溶液，其包括向苛性碱溶液中加入有效的沉积物抑制量的不可烯化的羰基化合物。本发明还是抑制在用于烃制造过程的废碱洗涤/汽提器系统中发生的结垢沉积物的形成的方法。当它们与含氧化合物如醛类污染的烃加工流接触时，这些系统中会发生结垢。这些沉积物在与含氧化合物污染的烃加工流中形成，同时与pH> 7的苛性碱溶液接触。本发明包括向苛性碱溶液中加入有效的沉积抑制量的非烯醇化羰基化合物。优选的不可烯化羰基化合物是甲醛，乙二醛，苯甲醛，对茴香醛，甲酸，乙二醛酸和多聚甲醛。

4. 发明授权

US5779881A Phosphonate/thiophosphonate coking inhibitors 失效
标题翻译：膦酸盐/硫代膦酸盐焦化抑制剂
公开(公告)号：US5779881A
公开(公告)日：1998-07-14
申请号：US778995
申请日：1997-01-06
申请人： Youdong Tong , Michael K. Poindexter
发明人： Youdong Tong , Michael K. Poindexter
IPC分类号： C07C4/02 , C07C7/20 , C07C11/04 , C09K3/00 , C10B43/14 , C10B57/12 , C10G9/16 , C10G75/04 , C10G9/12
CPC分类号： C10G75/04 , C07C7/20 , C10G9/16 , Y10S585/95
摘要： A method to inhibit coke formation on heat transfer surfaces used to heat or cool a petroleum feedstock at coke-forming conditions is disclosed. The heat transfer surfaces are treated with an effective amount of phosphonate to inhibit coke formation on the heat transfer surfaces. The phosphonate is essentially free from contributing to corrosion and from producing detrimental by-products.
摘要翻译：公开了一种在焦炭形成条件下用于加热或冷却石油原料的传热表面上抑制焦炭形成的方法。用有效量的膦酸盐处理传热表面以抑制传热表面上的焦炭形成。膦酸盐基本上不会有助于腐蚀和产生有害副产物。

5. 发明授权

US5556575A Corrosion inhibition in refineries using the reaction product of hydrocarbyl succinic anhydride and an amine 失效
标题翻译：使用烃基琥珀酸酐和胺的反应产物在炼油厂中进行腐蚀抑制
公开(公告)号：US5556575A
公开(公告)日：1996-09-17
申请号：US413340
申请日：1995-03-30
申请人： Elizabeth Babaian-Kibala , Veronica K. Braden , Michael K. Poindexter , Christopher J. Murphy
发明人： Elizabeth Babaian-Kibala , Veronica K. Braden , Michael K. Poindexter , Christopher J. Murphy
IPC分类号： C07D307/60 , C10G7/10 , C23F11/14
CPC分类号： C10G7/10 , C23F11/04 , C23F11/145
摘要： Disclosed are a method for inhibiting corrosion in crude oil distillation towers, an improvement in crude oil fractionation, a method for dispersing iron sulfide in a hydrocarbon stream and a hydrocarbon dispersion using the reaction product of hydrocarbyl succinic anhydride and an amine. The reaction product has a molecular weight of from 500-800, the hydrocarbyl substituent has 6-20 carbon atoms, and the amine is selected from EDA, DETA, TETA, TEPA, PEHA, AEP, piperazine, 1,2-PDA, 1,3-PDA, IBPA, MDA or HMDA. The imide product is a filming inhibitor used to treat metal surfaces subject to mineral acid corrosion and disperse iron sulfide particles by adding 3 to 24 ppm to sweet or sour crude contacting the metal surfaces.
摘要翻译：公开了一种抑制原油蒸馏塔腐蚀的方法，原油分馏的改进，烃流中硫化铁的分散方法和使用烃基琥珀酸酐与胺的反应产物的烃分散体。反应产物的分子量为500-800，烃基取代基具有6-20个碳原子，胺选自EDA，DETA，TETA，TEPA，PEHA，AEP，哌嗪，1,2-PDA，1 ，3-PDA，IBPA，MDA或HMDA。酰亚胺产品是一种用于处理无机酸腐蚀的金属表面的成膜抑制剂，通过向接触金属表面的甜或酸粗品加入3至24ppm来分散硫化铁颗粒。

6. 发明授权

US08911615B2 Recovery and separation of crude oil and water from emulsions 有权
标题翻译：从乳液中回收和分离原油和水
公开(公告)号：US08911615B2
公开(公告)日：2014-12-16
申请号：US12757008
申请日：2010-04-08
申请人： Olina G. Raney , John Hera, Jr. , Duy T. Nguyen , Michael K. Poindexter , George J. Hirasaki , Clarence A. Miller
发明人： Olina G. Raney , John Hera, Jr. , Duy T. Nguyen , Michael K. Poindexter , George J. Hirasaki , Clarence A. Miller
IPC分类号： C10G33/04 , B01D17/05 , B01D17/04 , B01D17/02
CPC分类号： C10G33/04 , B01D17/0202 , B01D17/047 , C10G2300/44
摘要： A composition and method demulsify a produced emulsion from anionic surfactants and polymer (SP) and alkali, surfactants, and polymer (ASP). The produced emulsion is demulsified into oil and water. In one embodiment, the composition includes a surfactant. The surfactant comprises a cationic surfactant, an amphoteric surfactant, or any combinations thereof.
摘要翻译：组合物和方法从阴离子表面活性剂和聚合物（SP）和碱，表面活性剂和聚合物（ASP）中破乳产生的乳液。所生产的乳液被破乳成油和水。在一个实施方案中，组合物包括表面活性剂。表面活性剂包括阳离子表面活性剂，两性表面活性剂或其任何组合。

7. 发明授权

US5360531A Phosphoric triamide coking inhibitors 失效
标题翻译：磷酸三酰胺焦化抑制剂
公开(公告)号：US5360531A
公开(公告)日：1994-11-01
申请号：US71458
申请日：1993-06-02
申请人： Youdong Tong , Michael K. Poindexter
发明人： Youdong Tong , Michael K. Poindexter
IPC分类号： C07C4/04 , C07C11/04 , C07F9/59 , C10G9/16
CPC分类号： C10G9/16 , Y10S585/95
摘要： Inhibiting coke formation on heat transfer surfaces used to heat or cool a petroleum feedstock at coke-forming conditions. The heat transfer surfaces are treated with an effective amount of tripiperidinophosphine oxide to inhibit coke formation on the heat transfer surfaces. The tripiperidinophosphine oxide is essentially free from contributing to corrosion and from producing catalyst-impairing by-products.
摘要翻译：在焦炭形成条件下用于加热或冷却石油原料的传热表面上抑制焦炭形成。传热表面用有效量的三哌啶基氧化膦处理以抑制传热表面上的焦炭形成。三哌啶基氧化膦基本上不会有助于腐蚀和产生催化剂损害副产物。

8. 发明授权

US5324393A Fouling prevention in ethylene dichloride distillation units 失效
标题翻译：二氯乙烷蒸馏装置防污
公开(公告)号：US5324393A
公开(公告)日：1994-06-28
申请号：US48337
申请日：1993-04-15
申请人： Michael K. Poindexter
发明人： Michael K. Poindexter
IPC分类号： C07C17/383 , C07C17/386 , C23F11/00 , C07C17/00 , C23F14/00
CPC分类号： C07C17/386 , C07C17/383
摘要： A method for preventing fouling of ethylene dichloride distillation units which comprises treating the feed to such unit with a fouling preventing amount of a composition comprising (a) 2-15 weight % of an oil soluble polyacrylate ester or methacrylate ester with alcohol radical of the ester group containing from C.sub.4 -C.sub.22 carbon atoms which contains between 0.1-25 mole % of amino alcohol ester groups; (b) 20-40 weight % a phenylene diamine compound having the formula ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, and R.sub.4 are the same or different and are hydrogen, C.sub.1 -C.sub.20 alkyl, C.sub.1 -C.sub.20 aryl, C.sub.1 -C.sub.20 alkaryl or C.sub.1 -C.sub.20 aralkyl, with the proviso that at least one of R.sub.1, R.sub.2, R.sub.3 or R.sub.4 is hydrogen; and (c) the balance is a heavy aromatic solvent.
摘要翻译：一种用于防止二氯乙烯蒸馏单元结垢的方法，其包括用防污垢量的组合物处理进料至该单元，所述组合物包含（a）2-15重量％的油溶性聚丙烯酸酯或甲基丙烯酸酯与酯的醇基含有0.1-25摩尔％氨基醇酯基的C 4 -C 22碳原子的基团; （b）20-40重量％的具有式“IMAGE”的苯二胺化合物，其中R 1，R 2，R 3和R 4相同或不同，为氢，C 1 -C 20烷基，C 1 -C 20芳基，C 1 -C 20烷芳基或C 1 -C 20芳烷基，条件是R 1，R 2，R 3或R 4中的至少一个为氢; 和（c）余量为重芳族溶剂。

9. 发明授权

US5288925A Method for inhibiting the deposition of ethylene-vinyl alcohol copolymer 失效
标题翻译：抑制乙烯 - 乙烯醇共聚物沉积的方法
公开(公告)号：US5288925A
公开(公告)日：1994-02-22
申请号：US983202
申请日：1992-11-30
申请人： Michael K. Poindexter
发明人： Michael K. Poindexter
IPC分类号： C07C29/80 , C07C29/94 , C08J3/03 , C07C27/26
CPC分类号： C08J3/03 , C07C29/80 , C07C29/94 , C08J2329/04
摘要： A method for preventing the precipitation of ethylene-vinyl alcohol copolymers in a distillation vessel. The vessel contains water, methanol, and ethylene-vinyl alcohol copolymers. The method includes the step of adding to the distillation vessel from 1 to about 1,000 ppm of at least one surfactant selected from the group consisting of alkyl, aryl, alkylaryl and arylalkyl sulfonic acids having a carbon length of from 4 to about 30 carbons. Preferably, the surfactant is dodecylbenzenesulfonic acid.
摘要翻译：一种用于防止乙烯 - 乙烯醇共聚物在蒸馏容器中析出的方法。该容器含有水，甲醇和乙烯 - 乙烯醇共聚物。该方法包括向蒸馏容器中加入1至约1,000ppm的至少一种选自碳原子数为4至约30个碳原子的烷基，芳基，烷基芳基和芳基烷基磺酸的表面活性剂的步骤。优选地，表面活性剂是十二烷基苯磺酸。

10. 发明授权

US09688899B2 Curable composition for use as lost circulation material 有权
公开(公告)号：US09688899B2
公开(公告)日：2017-06-27
申请号：US14004819
申请日：2012-05-03
申请人： Phillip S. Athey , Bernard E. Obi , Michael K. Poindexter
发明人： Phillip S. Athey , Bernard E. Obi , Michael K. Poindexter
IPC分类号： C09K8/035 , C09K8/508 , C08G18/67 , C09D175/16
CPC分类号： C09K8/035 , C08G18/672 , C09D175/16 , C09K8/5086 , C08G18/48
摘要： The present invention relates to compositions and methods for reducing or preventing the loss of drilling fluids and other well servicing fluids into a subterranean formation during drilling or construction of boreholes in said formation. Specifically, this invention comprises a curable composition capable of free radical polymerization for creating lost circulation material in-situ. The curable composition comprises an organic compound capable of free radical (co)polymerization represented by the formula (I): wherein x is an integer from 1 to 8; Fp comprises one or more moiety comprising a free radical polymerizable group; L is an organic moiety comprising a (substituted) aromatic or (substituted) aliphatic group comprising one or more O, N, S, or combinations thereof; and Q comprises a substituted or unsubstituted mono- or polyvalent organic radical comprising one or one or more moiety selected from alkyl, alkylene, alkenyl, cycloalkyl, cycloalkylene, aryl, aralkyl, alkaryl, poly(oxyalkylene), poly(carboalkoxyalkylene), a substituted heterocyclic radical, or an unsubstituted heterocyclic radical.

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