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1. 发明授权

US08802740B2 Environmentally friendly demulsifiers for crude oil emulsions 有权
标题翻译：用于原油乳液的环保破乳剂
公开(公告)号：US08802740B2
公开(公告)日：2014-08-12
申请号：US12489079
申请日：2009-06-22
申请人： Steven P. Newman , Carl Hahn , Robert D. McClain
发明人： Steven P. Newman , Carl Hahn , Robert D. McClain
IPC分类号： C08G65/28 , C08G65/26 , B01D17/05 , C08G69/44
CPC分类号： B01D17/047 , C08G65/20 , C08L71/02 , C08L2666/22
摘要： The present invention provides environmentally friendly demulsifiers for the breakdown of petroleum oil applications. The demulsification formulations of the present invention are biodegradable and are low in toxicity. The demulsifiers include a poly(tetramethylene glycol) and an alkylene glycol copolymer linked to the poly(tetramethylene glycol) by a difunctional coupling agent.
摘要翻译：本发明提供了用于石油应用破坏的环境友好的破乳剂。本发明的破乳剂可生物降解，毒性低。破乳剂包括通过双官能偶联剂与聚（四亚甲基二醇）连接的聚（四亚甲基二醇）和亚烷基二醇共聚物。

2. 发明授权

US06183882B2 In plane deflection coupon for monitoring and controlling of laser shock peening 失效
标题翻译：用于监测和控制激光冲击喷丸的平面偏转试样
公开(公告)号：US06183882B2
公开(公告)日：2001-02-06
申请号：US09106320
申请日：1998-06-29
申请人： Seetharamaiah Mannava , William D. Cowie , P. Kennard Wright, III , Robert D. McClain
发明人： Seetharamaiah Mannava , William D. Cowie , P. Kennard Wright, III , Robert D. McClain
IPC分类号： B23K2600
CPC分类号： C21D10/005 , Y10S148/903 , Y10T428/12486
摘要： A test coupon is formed from a metallic strip having opposite first and second sides that generally define a plane of the strip and the strip includes a laser shock peened patch of the strip that has first and second laser shock peened surfaces on the first and second sides, respectively, first and second laser shocked regions having deep compressive residual stresses imparted by the laser shock peening extending into the strip from the first and second laser shock peened surfaces, respectively, and a deflection of a portion of the strip from a position of the portion before the laser shock peening. The deflection is formed by the laser shock peening such that at least a part and preferably substantially all of the deflection lies in the plane and the test coupon preferably includes an indicating means to indicate the deflection.
摘要翻译：测试试样由具有相反的第一和第二侧的金属带形成，其通常限定条带的平面，并且条带包括条带的激光冲击喷丸贴片，其在第一和第二侧上具有第一和第二激光冲击喷丸表面分别具有由激光冲击喷丸赋予的深压缩残余应力的第一激光冲击区域和第二激光冲击区域分别从第一和第二激光冲击喷丸表面延伸到条带中，并且一部分条带从激光冲击硬化之前的部分。通过激光冲击喷丸形成偏转，使得至少一部分，优选基本上全部的偏转位于平面中，并且测试试样优选地包括指示装置以指示偏转。

3. 发明授权

US5951790A Method of monitoring and controlling laser shock peening using an in plane deflection test coupon 失效
标题翻译：使用平面偏转测试试样监测和控制激光冲击喷丸的方法
公开(公告)号：US5951790A
公开(公告)日：1999-09-14
申请号：US107196
申请日：1998-06-26
申请人： Seetharamaiah Mannava , William D. Cowie , P. Kennard Wright, III , Robert D. McClain
发明人： Seetharamaiah Mannava , William D. Cowie , P. Kennard Wright, III , Robert D. McClain
IPC分类号： C21D10/00 , C21D1/54
CPC分类号： C21D10/005 , Y10S148/90 , Y10S148/903
摘要： A method for quality assurance of a laser process and more particularly a laser shock peening process that uses a test coupon having a deflection formed by a laser firing. The test coupon is from a metallic strip having opposite first and second sides that generally define a plane of the strip and the strip includes a laser shock peened patch of the strip that has first and second laser shock peened surfaces on the first and second sides, respectively, first and second laser shocked regions having deep compressive residual stresses imparted by the laser shock peening extending into the strip from the first and second laser shock peened surfaces, respectively, and a deflection of a portion of the strip from a position of the portion before the laser shock peening. The deflection is formed by the laser shock peening such that at least a part and preferably substantially all of the deflection lies in the plane of the strip and the test coupon preferably includes an indicating means to indicate the deflection. The quality assurance process of the present invention may further include correlating high cycle fatigue to the deflection.
摘要翻译：一种用于激光工艺的质量保证的方法，更具体地说是使用具有通过激光烧制形成的偏转的试样的激光冲击硬化工艺。试样来自具有相反的第一和第二侧的金属条，其通常限定条带的平面，并且条带包括条的激光冲击喷丸补片，其在第一和第二侧上具有第一和第二激光冲击硬化表面，分别具有由激光冲击喷丸赋予的深压缩残余应力的第一和第二激光冲击区域分别从第一和第二激光冲击喷丸表面延伸到条带中，并且一部分条带从该部分的位置偏转之前激光冲击硬化。通过激光冲击喷丸形成偏转，使得至少一部分并且优选地基本上全部的偏转位于条的平面中，并且试样优选地包括指示装置以指示偏转。本发明的质量保证过程还可以包括将高循环疲劳与偏转相关联。

4. 发明授权

US5302681A Polymerization inhibition by fullerenes 失效
标题翻译：富勒烯的聚合抑制作用
公开(公告)号：US5302681A
公开(公告)日：1994-04-12
申请号：US989933
申请日：1992-12-10
申请人： Robert D. McClain
发明人： Robert D. McClain
IPC分类号： C07B63/04 , C07C7/20 , C07C67/62 , C07C253/32 , C08F36/08 , C08F12/08
CPC分类号： C07C253/32 , C07B63/04 , C07C67/62 , C07C7/20 , C07C2104/00 , Y10S977/753
摘要： The premature free-radical polymerization of a non-linear, readily polymerizable organic monomer under conditions where the monomer would otherwise polymerize is inhibited by incorporating within the non-linear, readily polymerizable monomer a polymerization inhibiting amount of a fullerene or a derivative thereof.
摘要翻译：通过在非线性易聚合单体内引入聚合抑制量的富勒烯或其衍生物，可以抑制非线性易于聚合的有机单体在单体另外聚合的条件下的过早自由基聚合。

5. 发明授权

US06372121B1 Reducing undesired polymerization in the basic wash unit of hydrocarbon cracking process 有权
标题翻译：在烃裂解过程中减少不希望的聚合
公开(公告)号：US06372121B1
公开(公告)日：2002-04-16
申请号：US09703108
申请日：2000-10-31
申请人： Robert D. McClain , Natu R. Patel , Raymond M. Glath
发明人： Robert D. McClain , Natu R. Patel , Raymond M. Glath
IPC分类号： C10G916
CPC分类号： C10G75/04 , C10G9/00 , C10G19/02 , C10G70/06 , Y02P30/464 , Y10S585/95
摘要： This invention is a method to inhibit the polymerization of carbonyl compounds in a basic wash unit operation in a hydrocarbon cracking process, wherein a compound selected from the group consisting of alpha-amino acids and esters thereof and amides thereof and salts thereof and mixtures thereof or Mercaptoacetic acid and alkyl esters thereof, is added either to a stream comprising a carbonyl compound or to the basic wash unit operation; wherein the compound is selected such that it remains water-soluble and base-soluble and does not flocculate in the stream or in the basic wash unit operation; and wherein the stream is contacted with the compound either before or at the same time as the stream enters the basic wash unit operation; or wherein the compound is added to the basic wash unit operation before or while the stream enters the basic wash unit operation.
摘要翻译：本发明是在烃裂解方法中碱性洗涤单元操作中抑制羰基化合物的聚合的方法，其中选自α-氨基酸及其酯及其酰胺及其盐及其混合物的化合物或将巯基乙酸及其烷基酯加入到包含羰基化合物的流或基本洗涤单元操作中;其中选择该化合物使其保持水溶性和碱溶性，并且不会在流中或基本洗衣机操作; 并且其中所述物流在所述物流进入所述基本洗涤单元操作之前或同时与所述化合物接触; 或其中在流进入基本洗涤单元操作之前或期间将化合物加入基本洗涤单元操作中。

6. 发明授权

US5879534A Non-enolizable oxygenates as anti foulants in ethylene dichloride manufacture 失效
标题翻译：不可烯化的含氧化合物作为二氯乙烷中的防污剂制造
公开(公告)号：US5879534A
公开(公告)日：1999-03-09
申请号：US102483
申请日：1998-06-22
申请人： Vincent E. Lewis , Robert D. McClain , Michael K. Poindexter
发明人： Vincent E. Lewis , Robert D. McClain , Michael K. Poindexter
IPC分类号： C07C17/42 , C10G19/02 , C10G75/04 , C10G9/16
CPC分类号： C07C17/42 , C10G19/02 , C10G75/04 , Y10S585/95
摘要： A method of inhibiting the formation of fouling deposits occurring in spent caustic wash systems used for ethylene dichloride (EDC) manufacturing processes. Fouling occurs in these systems when they are in contact with EDC processing streams contaminated with oxygen-containing compounds, such as aldehydes. These deposits are formed in EDC processing streams contaminated with oxygen-containing compounds while in contact with a caustic solution having a pH>7. The invention comprises adding an effective deposit-inhibiting amount of a non-enolizable carbonyl compound to the caustic solution. Preferred non-enolizable carbonyl compounds are formaldehyde, glyoxal, benzaldehyde, p-anisaldehyde, formic acid, glyoxalic acid and paraformaldehyde.
摘要翻译：一种抑制在用于二氯乙烷（EDC）制造过程的废碱洗涤系统中发生的结垢沉积物形成的方法。当这些系统与含氧化合物（如醛）污染的EDC处理流接触时，会在这些系统中发生结垢。这些沉积物在与含氧化合物污染的EDC处理流中形成，同时与pH> 7的苛性碱溶液接触。本发明包括向苛性碱溶液中加入有效的沉积抑制量的非烯醇化羰基化合物。优选的不可烯化羰基化合物是甲醛，乙二醛，苯甲醛，对茴香醛，甲酸，乙二醛酸和多聚甲醛。

7. 发明授权

US5770041A Non-enolizable oxygenates as antifoulants 失效
标题翻译：不可烯化的含氧化合物作为防污剂
公开(公告)号：US5770041A
公开(公告)日：1998-06-23
申请号：US804050
申请日：1997-02-21
申请人： Vincent E. Lewis , Robert D. McClain , Michael K. Poindexter
发明人： Vincent E. Lewis , Robert D. McClain , Michael K. Poindexter
IPC分类号： C07C17/42 , C10G19/02 , C10G75/04 , C10G9/16
CPC分类号： C10G75/04 , C07C17/42 , C10G19/02 , Y10S585/95
摘要： The invention is a method of inhibiting the formation of fouling deposits occurring on the surface of an alkaline scrubber used to remove acid gases, such as hydrogen sulfide, carbon dioxide and mercaptans, from hydrocarbon streams. These deposits are formed during the scrubbing of pyrolytically produced hydrocarbons contaminated with oxygen-containing compounds with a caustic solution having a pH>7 which comprises adding an effective deposit-inhibiting amount of a non-enolizable carbonyl compound to the caustic solution. The invention is also a method of inhibiting the formation of fouling deposits occurring in spent caustic wash/stripper systems used for hydrocarbon manufacturing processes. Fouling occurs in these systems when they are in contact with hydrocarbon processing streams contaminated with oxygen-containing compounds, such as aldehydes. These deposits are formed in hydrocarbon processing streams contaminated with oxygen-containing compounds while in contact with a caustic solution having a pH>7. The invention comprises adding an effective deposit-inhibiting amount of a non-enolizable carbonyl compound to the caustic solution. Preferred non-enolizable carbonyl compounds are formaldehyde, glyoxal, benzaldehyde, p-anisaldehyde, formic acid, glyoxalic acid and paraformaldehyde.
摘要翻译：本发明是一种抑制在用于从烃流中除去酸性气体如硫化氢，二氧化碳和硫醇的碱性洗涤器表面上发生的结垢沉积物形成的方法。这些沉积物是在用含有氢的化合物污染的热解生成的碳氢化合物的洗涤过程中形成的，所述氢氧化物溶液具有pH> 7的苛性碱溶液，其包括向苛性碱溶液中加入有效的沉积物抑制量的不可烯化的羰基化合物。本发明还是抑制在用于烃制造过程的废碱洗涤/汽提器系统中发生的结垢沉积物的形成的方法。当它们与含氧化合物如醛类污染的烃加工流接触时，这些系统中会发生结垢。这些沉积物在与含氧化合物污染的烃加工流中形成，同时与pH> 7的苛性碱溶液接触。本发明包括向苛性碱溶液中加入有效的沉积抑制量的非烯醇化羰基化合物。优选的不可烯化羰基化合物是甲醛，乙二醛，苯甲醛，对茴香醛，甲酸，乙二醛酸和多聚甲醛。

8. 发明授权

US5734098A Method to monitor and control chemical treatment of petroleum, petrochemical and processes with on-line quartz crystal microbalance sensors 失效
标题翻译：使用在线石英晶体微量天平传感器监测和控制石油，石化和工艺化学处理的方法
公开(公告)号：US5734098A
公开(公告)日：1998-03-31
申请号：US621402
申请日：1996-03-25
申请人： Paul R. Kraus , Robert D. McClain , Michael K. Poindexter
发明人： Paul R. Kraus , Robert D. McClain , Michael K. Poindexter
IPC分类号： C02F1/00 , C07B61/00 , C07C7/00 , C07C11/02 , C07C253/34 , C07C255/08 , C10G15/00 , G01N5/02 , G01N9/00 , G01N9/36 , G01N11/10 , G01N11/16 , G01N27/00 , G01N29/02 , G01N29/036 , G01N33/00 , G01N33/18 , G01N33/28 , G05D21/00
CPC分类号： G01N29/022 , G01N17/008 , G01N29/036 , G01N11/10 , G01N2291/0256 , G01N2291/02818 , G01N2291/0422 , G01N2291/0426 , G01N9/002
摘要： Thickness-shear mode resonators which simultaneously measure mass deposition and fluid properties can be utilized to monitor petroleum processing, petrochemical and water treatment systems. Specialty chemical additive materials can be accurately and instantaneously added to control conditions detected by the thickness-shear mode resonators. The thickness-shear mode resonators are piezoelectric crystals used in conjunction with oscillator circuitry that can determine mass as well as viscosity and/or density of a fluid in contact with the piezoelectric surface.
摘要翻译：同时测量质量沉积和流体性质的厚度剪切模式谐振器可用于监测石油加工，石化和水处理系统。专门的化学添加剂材料可以精确和即时添加，以控制由厚度 - 剪切模式谐振器检测到的条件。厚度 - 剪切模式谐振器是与振荡器电路结合使用的压电晶体，其可以确定与压电表面接触的流体的质量以及粘度和/或密度。

9. 发明授权

US5362652A Spectrophotometric detection of hydroperoxides in hydrocarbons 失效
标题翻译：分光光度法检测碳氢化合物中的氢过氧化物
公开(公告)号：US5362652A
公开(公告)日：1994-11-08
申请号：US156374
申请日：1993-11-22
申请人： Robert D. McClain
发明人： Robert D. McClain
IPC分类号： G01N31/22 , G01N33/28 , G01N21/00 , G01N33/00
CPC分类号： G01N31/228 , G01N33/2835 , Y10T436/206664
摘要： A method for the determination of organic hydroperoxides in a hydrocarbon which has been subjected to oxidative polymerization conditions is disclosed. The steps employed in the invention include mixing an organic cupric salt such as cupric acetate and a phenanthroline such as 2,9-dimethyl-1,10-phenanthroline with a sample of the hydrocarbon in an organic solvent such as acetonitrile, measuring the color change after a fixed period of time for cuprous complex formation, and comparing the measurement to the color change of a standard reference to determine the relative quantity of organic hydroperoxide in the sample.
摘要翻译：公开了一种测定已经经历氧化聚合条件的烃中的有机氢过氧化物的方法。本发明中采用的步骤包括将有机铜盐如乙酸铜和菲咯啉如2,9-二甲基-1,10-菲咯啉与有机溶剂如乙腈中的烃样品混合，测量颜色变化在一定时间后形成亚铜络合物，并将测量与标准参考的颜色变化进行比较，以确定样品中有机氢过氧化物的相对量。

10. 发明申请

US20090259004A1 ENVIRONMENTALLY FRIENDLY DEMULSIFIERS FOR CRUDE OIL EMULSIONS 有权
标题翻译：环境友好的乳化剂乳化剂
公开(公告)号：US20090259004A1
公开(公告)日：2009-10-15
申请号：US12489079
申请日：2009-06-22
申请人： Steven P. Newman , Carl Hahn , Robert D. McClain
发明人： Steven P. Newman , Carl Hahn , Robert D. McClain
IPC分类号： C08L53/00 , C08G65/34
CPC分类号： B01D17/047 , C08G65/20 , C08L71/02 , C08L2666/22
摘要： The present invention provides environmentally friendly demulsifiers for the breakdown of petroleum oil applications. The demulsification formulations of the present invention are biodegradable and are low in toxicity. The demulsifiers include a poly(tetramethylene glycol) and an alkylene glycol copolymer linked to the poly(tetramethylene glycol) by a difunctional coupling agent.
摘要翻译：本发明提供了用于石油应用破坏的环境友好的破乳剂。本发明的破乳剂可生物降解，毒性低。破乳剂包括通过双官能偶联剂与聚（四亚甲基二醇）连接的聚（四亚甲基二醇）和亚烷基二醇共聚物。

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