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1. 发明授权

US4371674A Water soluble crosslinked ethyleneimine grafted polyamidoamine 失效
标题翻译：水溶性交联乙烯亚胺接枝聚酰胺胺
公开(公告)号：US4371674A
公开(公告)日：1983-02-01
申请号：US173479
申请日：1980-07-30
申请人： Otto Hertel , Emil Scharf , Jaroslav Melzer , Rolf Fikentscher
发明人： Otto Hertel , Emil Scharf , Jaroslav Melzer , Rolf Fikentscher
IPC分类号： C08G81/00 , C08G69/48 , D21H17/55 , D21H17/56
CPC分类号： C08G69/48
摘要： Process for the production of water-soluble auxiliaries for the papermaking industry by reacting(a) 1 part by weight of a polyamidoamine obtained by condensing 1 mole of a dicarboxylic acid having from 4 to 10 carbon atoms with from 0.8 to 1.4 moles of a polyalkylene polyamine having from 3 to 10 alkyleneamine units and containing up to 8 ethyleneimine units per basic nitrogen atom with (b) 0.1 to 4 parts by weight of an .alpha.,.omega.-dichloro polyalkylene oxide obtained by reacting a polyalkylene oxide having from 8 to 100 alkylene oxide units with a compound selected from the group consisting of a thionyl chloride and phosgene and then cleaving the reaction products by heating them to a temperature of from 70.degree. to 150.degree. C. in the presence of a tertiary amine as catalyst,as crosslinking agent, at a temperature above 20.degree. C. in aqueous solution or in a water-soluble organic solvent, the reaction being carried out to a point at which the viscosity of an aqueous solution containing 20% by weight of auxiliary is from 300 to 2,500 mPas.
摘要翻译：通过使（a）通过将1重量份通过将1摩尔具有4至10个碳原子的二羧酸缩合得到的聚酰胺胺与0.8至1.4摩尔聚亚烷基二醇来制备用于造纸工业的水溶性助剂的方法多胺具有3至10个亚烷基胺单元并且每个碱性氮原子含有至多8个亚乙基亚胺单元，和（b）0.1至4重量份通过使具有8至100个亚烷基的聚环氧烷反应获得的α，ω-二氯聚环氧烷氧化物单元与选自亚硫酰氯和光气的化合物反应，然后在作为催化剂的叔胺的存在下将反应产物加热至70℃至150℃的温度，作为交联剂在水溶液或水溶性有机溶剂中在20℃以上的温度下进行反应，直至水溶液的粘度为 20重量％的助剂为300至2,500mPas。

2. 发明授权

US4328142A Preparation of water-soluble condensates and their use as crosslinking agents for the preparation of papermaking aids 失效
标题翻译：水溶性缩合物的制备及其作为造纸助剂制备交联剂的用途
公开(公告)号：US4328142A
公开(公告)日：1982-05-04
申请号：US225241
申请日：1981-01-15
申请人： Otto Hertel , Emil Scharf , Jaroslav Melzer
发明人： Otto Hertel , Emil Scharf , Jaroslav Melzer
IPC分类号： C08G81/00 , C08G69/48 , C08G73/02 , D21H17/46 , D21H17/54 , D21H21/10 , C08L63/00
CPC分类号： C08G73/0286 , C08G69/48 , D21H17/54 , D21H21/10
摘要： A process for the preparation of water-soluble polymeric crosslinking agents by a two-stage reaction of di-secondary diamines with epichlorohydrin and/or dichlorohydrin, wherein, in the first stage, di-secondary diamines are condensed with epichlorohydrin and/or dichlorohydrin in a molar ratio of from 1:0.5 to 1:1 at a pH of from 9 to 12, and in the second stage the condensates obtained in the first stage are reacted with additional epichlorohydrin and/or dichlorohydrin at a pH of from 4 to 8.5. The water-soluble condensates thus obtained are crosslinking agents for polyamines, polyamidoamines, ethyleneimine-modified polyamidoamines and polyether-amines. The crosslinking reaction gives water-soluble condensates, which possess a high cation activity and may be used as retention aids, drainage aids and flocculants in the manufacture of paper.
摘要翻译：通过二次二胺与表氯醇和/或二氯丙醇的两步反应制备水溶性聚合物交联剂的方法，其中在第一阶段中将二仲二胺与表氯醇和/或二氯代丙醇缩合在pH为9至12时的摩尔比为1:0.5至1:1，在第二阶段中，将第一阶段中获得的缩合物与附加的表氯醇和/或二氯丙醇在pH为4至8.5 。由此获得的水溶性缩合物是多胺，聚酰胺胺，乙烯亚胺改性的聚酰胺胺和聚醚胺的交联剂。交联反应产生具有高阳离子活性的水溶性缩合物，并可用作纸的制造中的助留剂，助滤剂和絮凝剂。

3. 发明授权

US4567303A Process and apparatus for preparing or reacting alkanolamines 失效
标题翻译：制备或反应链烷醇胺的方法和设备
公开(公告)号：US4567303A
公开(公告)日：1986-01-28
申请号：US638522
申请日：1984-08-06
申请人： Guenter Boettger , Hans Hammer , Otto Hertel , Gerhard Jeschek , Herbert Mueller , Emil Scharf , Willibald Schoenleben
发明人： Guenter Boettger , Hans Hammer , Otto Hertel , Gerhard Jeschek , Herbert Mueller , Emil Scharf , Willibald Schoenleben
IPC分类号： C07C211/10 , C07C67/00 , C07C209/00 , C07C209/16 , C07C211/09 , C07C211/65 , C07C213/00 , C07C213/04 , C07C215/08 , C07C215/14 , C07D295/088 , C07C65/01
CPC分类号： C07D295/088
摘要： In preparing or reacting alkanolamines, especially at high temperatures, the use of substantially nickel-free alloy steels prevents corrosion and discoloration.
摘要翻译：在制备或反应链烷醇胺时，特别是在高温下，使用基本上不含镍的合金钢可防止腐蚀和变色。

4. 发明授权

US4450045A Preparation of water-soluble, nitrogen-containing condensates and their use in papermaking 失效
标题翻译：制备水溶性含氮缩合物及其在造纸中的应用
公开(公告)号：US4450045A
公开(公告)日：1984-05-22
申请号：US416614
申请日：1982-09-10
申请人： Otto Hertel , Friedrich Linhart , Emil Scharf
发明人： Otto Hertel , Friedrich Linhart , Emil Scharf
IPC分类号： C08G69/00 , C08G69/48 , C08G73/02 , D21H17/55 , D21H21/10 , D21H3/58
CPC分类号： C08G73/0286 , C08G69/48 , C08G73/022 , C08G73/024 , D21H17/55 , D21H21/10
摘要： Water-soluble, nitrogen-containing condensates are prepared by reacting a cross-linking agent, obtained by(a) condensing 1 mole of a dicarboxylic acid of 4 to 10 carbon atoms with from 1 to 2 moles of a polyalkylenepolyamine, having 3-10 basic nitrogen atoms in the molecule, to give a polyamidoamine and(b) reacting the polyamidoamine with epichlorohydrin and/or dichlorohydrin in aqueous solution at a pH of from 4.5 to 8.5 and at below 100.degree. C., from 1 to 130 parts by weight of epichlorohydrin and/or dichlorohydrin being employed per 100 parts by weight of the polyamidoamine from (a),with ammonia, a primary amine, a polyamine containing 2 to 4 N atoms, a polyether-amine or a polyamidoamine in aqueous solution at below 100.degree. C.The condensates are used as retention aids, flocculants and drainage aids in papermaking.
摘要翻译：通过使（a）将1摩尔4〜10个碳原子的二羧酸与1〜2摩尔的聚亚烷基多胺缩合得到的交联剂，使3-10 分子中的碱性氮原子，得到聚酰胺胺和（b）使聚酰胺胺与环氧氯丙烷和/或二氯丙醇在pH 4.5至8.5和低于100℃，水溶液中的1-13重量份的水溶液中反应每100重量份来自（a）的聚酰胺胺与氨，伯胺，含2至4个N原子的聚胺，聚醚胺或聚酰氨胺在水溶液中的含量低于100时使用的表氯醇和/或二氯丙醇冷凝物用作造纸中的助留剂，絮凝剂和排水辅助剂。

5. 发明授权

US3973904A Water-soluble synthetic tanning agents 失效
标题翻译：水溶性合成鞣剂
公开(公告)号：US3973904A
公开(公告)日：1976-08-10
申请号：US233755
申请日：1972-03-10
申请人： Horst Endres , Otto Hertel , Franz-Friedrich Miller
发明人： Horst Endres , Otto Hertel , Franz-Friedrich Miller
IPC分类号： C14C3/18 , C14C3/20
CPC分类号： C14C3/18 , C14C3/20
摘要： Water-soluble synthetic tanning agents composed of formaldehyde condensation products of non-sulfonated aromatic hydroxy compounds or the sulfomethylation products thereof with aromatic sulfonic acids or with the formaldehyde condensation products of said sulfonic acids.
摘要翻译：由非磺化芳族羟基化合物的甲醛缩合产物或其磺基甲基化产物与芳族磺酸或与所述磺酸的甲醛缩合产物组成的水溶性合成鞣剂。

6. 发明授权

US4775540A Preparation of pourable choline chloride/silica powders 失效
标题翻译：可浇注氯化胆碱/二氧化硅粉末的制备
公开(公告)号：US4775540A
公开(公告)日：1988-10-04
申请号：US33849
申请日：1987-04-03
申请人： Otto Hertel , Gerhard Jeschek , Walter Klink , Wolfgang Koernig , Theodor Weber , Fritz Rateike
发明人： Otto Hertel , Gerhard Jeschek , Walter Klink , Wolfgang Koernig , Theodor Weber , Fritz Rateike
IPC分类号： A23K1/00 , A23K1/16 , A61K9/14 , A23K1/175
CPC分类号： A61K9/143 , A23K20/174 , A23K40/10 , A61K9/145 , Y10S426/807
摘要： A process for the preparation of pourable choline chloride/silica powders by mixing silica with choline chloride and, where appropriate, drying this mixture, wherein spray-dried or fluidized bed-dried silica which has a particle size of from 30 to 250 .mu.m is mixed with an aqueous choline chloride solution which contains from 70 to 80% by weight, based on the solution, of choline chloride and is at from 40.degree. to 80.degree. C., thereafter from 0.05 to 0.4% by weight, based on the mixture, of magnesium stearate or calcium stearate is added and, if appropriate, the resulting mixture is dried.
摘要翻译：通过将二氧化硅与氯化胆碱混合并适当地干燥该混合物来制备可倾倒的氯化胆碱/二氧化硅粉末的方法，其中具有30至250μm的粒度的喷雾干燥或流化床干燥的二氧化硅是与氯化胆碱氯化物溶液混合，该溶液含有70至80重量％的氯化胆碱溶液，为40-80℃，其后为0.05至0.4重量％，基于混合物，硬脂酸镁或硬脂酸钙，如果合适，将所得混合物干燥。

7. 发明授权

US4330480A Preparation of aminoalkyl half-esters of sulfuric acid 失效
标题翻译：制备硫酸氨基烷基半酯
公开(公告)号：US4330480A
公开(公告)日：1982-05-18
申请号：US231322
申请日：1981-02-04
申请人： Otto Hertel , Karl-Heinz Beyer , Albrecht H. Wallis , Klaus Wulz , Kamuran Izi
发明人： Otto Hertel , Karl-Heinz Beyer , Albrecht H. Wallis , Klaus Wulz , Kamuran Izi
IPC分类号： C07C305/06 , C07C141/02
CPC分类号： C07C305/06
摘要： A process for the preparation of an aminoalkyl half-ester of sulfuric acid by simultaneously adding an aminoalkanol and sulfuric acid to a suspending medium, boiling at 70.degree.-150.degree. C., with vigorous mixing, distilling off the water formed during the reaction, and any water introduced with the starting materials, together with a part of the suspending medium, as an azeotrope, separating off the water from the condensed azeotrope and recycling the suspending medium, as a gas, to the reaction mixture.
摘要翻译：通过同时向悬浮介质中加入氨基烷基半酯的硫酸制备方法，在剧烈混合下，在70-150℃沸腾，蒸除反应中形成的水，和引入原料的任何水以及悬浮介质的一部分作为共沸物，将水与冷凝的共沸物分离出来，并将悬浮介质作为气体再循环到反应混合物中。

8. 发明授权

US5132471A Purification of .alpha.-bisabolol 失效
标题翻译：（ALPHA） - 双酚A的纯化
公开(公告)号：US5132471A
公开(公告)日：1992-07-21
申请号：US690617
申请日：1991-04-24
申请人： Gerald Lauterbach , Otto Hertel , Klaus Euler
发明人： Gerald Lauterbach , Otto Hertel , Klaus Euler
IPC分类号： C07C29/80 , C07C33/14
CPC分类号： C07C33/14
摘要： .alpha.-Bisabolol is purified by distilling a plant extract containing .alpha.-bisabolol under reduced pressure and drawing off the purified .alpha.-bisabolol in the lower half of a distillation column as side product, and feeding in the extract above the side outlet.
摘要翻译：通过在减压下蒸馏含有α-对映体的植物提取物，并将作为副产物的蒸馏塔的下半部分中的纯化的α-对映体产物抽出，并将侧面出口上方的提取物进料进行纯化，来纯化α-对照。

9. 发明授权

US4806679A Isomerization of diacyloxybutenes 失效
标题翻译：二酰氧基丁烯异构化
公开(公告)号：US4806679A
公开(公告)日：1989-02-21
申请号：US633279
申请日：1984-07-23
申请人： Wolfgang Hoelderich , Rolf Fischer , Otto Hertel , Wolf D. Mross , Hans-Martin Weitz
发明人： Wolfgang Hoelderich , Rolf Fischer , Otto Hertel , Wolf D. Mross , Hans-Martin Weitz
IPC分类号： C07C67/34 , B01J29/00 , B01J29/04 , C07B61/00 , C07C67/00 , C07C69/025 , C07C69/16 , C07C67/293 , C07C69/28
CPC分类号： C07C67/00
摘要： 1,4-Diacyloxybut-2-enes and 3,4-diacyloxybut-1-enes are converted into one another in the gas phase or liquid phase at from 100.degree. to 350.degree. C. under atmospheric or superatmospheric pressure in the presence of a zeolite as a catalyst.
摘要翻译： 1,4-二酰氧基丁-2-烯和3,4-二酰氧基丁-1-烯在气相或液相中在大气压或超大气压下在100-350℃下，在沸石作为催化剂。

10. 发明授权

US4739051A Preparation of morpholine 失效
标题翻译：吗啉的制备
公开(公告)号：US4739051A
公开(公告)日：1988-04-19
申请号：US16484
申请日：1987-02-17
申请人： Wolfgang Schroeder , Wolfgang Lengsfeld , Gerd Heilen , Otto Hertel , Guenter Boettger
发明人： Wolfgang Schroeder , Wolfgang Lengsfeld , Gerd Heilen , Otto Hertel , Guenter Boettger
IPC分类号： B01J23/75 , B01J23/755 , C07D295/023 , C07D295/02
CPC分类号： C07D295/023 , B01J23/75 , B01J23/755
摘要： Morpholine and other cyclic imines are obtained by reacting diethylene glycol and other appropriate diols with ammonia under hydrogenating conditions in the gas phase in the presence of a catalyst which contains copper, a smaller amount of nickel and alumina.
摘要翻译：在含有铜，较少量的镍和氧化铝的催化剂的存在下，在气相中，在氢化条件下，使二甘醇和其它合适的二醇与氨反应，得到吗啉等环状亚胺。

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